Final Programme book is uploaded

Transcription

Contents
Welcome Message
4
Sponsors, Media Partners, Supporting Organisations
6
Committees, Organisers
14
Symposium History
16
Awards
19
The Eponyms of the Lecture Halls
21
Scientific Programme – Short Courses
25
Legend of the Congress Level
26
Lecture Programme
Sunday,
19
Monday,
20
Tuesday,
21
Wednesday, 22
Thursday,
23
27
27
29
36
45
54
June
June
June
June
June
2011
2011
2011
2011
2011
Final List of Posters
61
Vendor Seminars
182
Technical Information for Speakers and Poster Presenters
184
List of Exhibitors
189
Social Events
194
General Information
197
Welcome Message
Dear Participants of the HPLC 2011 Budapest Symposium,
It is our great pleasure to welcome you to Budapest and the 36th International Symposium
on High-Performance Liquid Phase Separations and Related Techniques: the HPLC 2011
Budapest Symposium. It is for the first time that the most prestigious and largest meeting
in the world dedicated to liquid-phase separations takes place in Hungary. The HPLC 2011
Budapest Symposium is proudly organised by the Hungarian Society for Separation Sciences that was established 15 years ago.
We often think of chromatography as a Hungarian science. It is often recalled how strongly
the Hungarian ‘mafia’ influenced the development of chromatography. We will remember
the achievements of famous Hungarian separation scientists during this week in a number
of ways. The plenary and the parallel oral sessions will take place in lecture halls named
after Csaba Horváth, István Halász, and Szabolcs Nyiredy. During the symposium, the
Halász Medal Award and the Csaba Horváth Memorial Award will be presented to honour
prominent separation scientists. Furthermore, a day-long scientific session will reunite the
former students and co-workers of Csaba Horváth to present research results based on
ideas that Csaba initiated.
During the five days of the symposium, a total of 134 oral presentations and about 800
posters will be presented. Short courses and tutorial lectures will constitute an integral
part of the scientific programme, which are planned as educational lectures for students
and others new to various separation disciplines, and to provide opportunities to broaden
one’s understanding of separation science. Moreover, the short courses will give a chance
to meet and discuss separation problems with the real experts. Nine tutorial lectures will
provide in-depth introduction and overview of current topics. Newcomers and senior researchers are also welcome to attend the tutorial lectures.
Exhibition and 13 vendor seminars are intended to inform the participants about the latest
developments in the field in terms of instrumentation, technology, and applications. Fiftyseven exhibitors will present their latest innovations in the field of separation science.
The social programme will offer opportunity to experience the Hungarian culture, food,
customs, and to discover Budapest and its surroundings. The 200th anniversary of the
birth of Ferenc Liszt – the Hungarian composer and virtuoso pianist – is celebrated this
year. The programme of the organ concert in the St. Stephen Basilica will feature his
works. The highlight of the social programme will be the symposium dinner in the Lázár
Equestrian Park, where you can enjoy the Hungarian cuisine, hospitality, and entertainment.
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Many people need to be thanked for making the HPLC 2011 Budapest Symposium a
success. We would like to thank all the members of the Scientific and Organising Committees for their ideas and work. We also thank our sponsors and exhibitors for providing
generous financial support. Special thanks go to all the people who submitted excellent
abstracts from many areas of liquid-phase separations.
We wish all participants of HPLC 2011 an intellectually stimulating and rewarding meeting
as well as a pleasant and unforgettable week in Budapest.
Attila Felinger
Chairman
HPLC 2011 Budapest
László Szepesy
Honorary Chairman
HPLC 2011 Budapest
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Sponsors, Media Partners, Supporting Organisations
PLATINUM SPONSORS
Agilent Technologies, Inc.
Agilent Technologies’ Bio-Analytical Measurement Solutions business is a leading global
provider of scientific tools for measuring the composition of the environment, foods,
pharmaceuticals, industrial processes, and biological samples. Bio-Analytical Measurement, combining Agilent’s life sciences and chemical analysis solutions units, produced
revenues of USD $5.4 billion in 2010. Agilent manufactures the world’s most popular gas
chromatography systems and holds market leadership positions in liquid chromatography,
mass spectrometry, consumables, software, genomic microarrays, sequencing target
enrichment, reagents, lab automation, support and compliance services. Agilent products
are found in academic, government and private labs throughout the world.
E-mail info_agilent@agilent.com
Website: www.agilent.com/chem
Thermo Scientific (part of Thermo Fisher Scientific)
Thermo Fisher Scientific is the world leader in serving science. We enable our customers
to make the world healthier, cleaner and safer by providing analytical instruments, equipment, reagents and consumables, software and services for research, analysis, discovery
and diagnostics. With revenues of nearly $11 billion, we have approximately 37,000
employees and serve customers within pharmaceutical and biotech companies, hospitals
and clinical diagnostic labs, universities, research institutions and government agencies, as
well as in environmental and process control industries.
With our recent acquisition of Dionex we have strengthened our position in chromatography to deliver the industry’s broadest selection of HPLC/UHPLC, Nano-LC, IC, CDS
columns, consumables, and vials.Our growing portfolio of products includes innovative
technologies for mass spectrometry, gas chromatography, sample preparation, and in-
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formatics. We also give our customers the most convenient purchasing choices, including a direct sales force of 7,500 professionals, catalogs, e-commerce and distribution
partners.
Contact Person: Andy Altman (Director of Liquid Chromatography)
Address: 355 River Oaks Parkway, San Jose, CA 95134, USA
Phone: +1 408 965 6389
E-mail: andy.altman@thermofisher.com
Website: www.thermoscientific.com
Waters
Waters Corporation, the premium brand in the analytical instruments industry, creates
business advantages for laboratory-dependent organizations by delivering practical and
sustainable scientific innovation to enable significant advancements in healthcare delivery,
environmental management, food safety, and water quality worldwide. Bringing keen understanding and deep experience to those responsible for laboratory infrastructure and performance, Waters helps customers make profound discoveries, optimize laboratory operations, deliver product performance, and ensure regulatory compliance. Pioneering a connected portfolio of separations and analytical science, laboratory informatics, mass spectrometry, as well as thermal analysis, Waters’ technology breakthroughs and laboratory
solutions provide an enduring platform for customer success.
Contact Person: Laurence Dufau, Waters European Headquarters
Address: BP 608, 78056 Saint-Quentin-en Yvelines Cedex, France
Phone: + 33 1 30 48 75 66, Fax: +33 1 30 48 72 11
E-mail: laurence_dufau@waters.com
Website: www.waters.com/hplc2011
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GOLD SPONSORS
Dionex, now part of Thermo Fisher Scientific
Dionex, now part of Thermo Fisher Scientific, is empowering scientists to quickly separate,
isolate, and identify chemical components – from simple ions in water to complex molecules in human tissue. Our UHPLC+ solutions and market-leading ion chromatography
systems enable customers to:
• Do things faster and more efficiently
• Simplify processes
• Deliver answers to tough questions
Dionex systems increase productivity and deliver faster results with fewer resources. The
simplicity of the Chromeleon® chromatography data software makes workflow integration
easy. Our advanced array of IC and LC column chemistries deliver unrivaled separations.
Speed and Simplicity – all come together in the Dionex applications-based solutions. By
combining our leadership in chromatography with Thermo Fisher Scientific’s leadership in
mass spectrometry and other techniques, a new range of powerful and simplified workflow
solutions now becomes possible. Our solutions are used by the environmental, life sciences, pharmaceutical, food and beverage, chemicals, power generation, and electronics
industries.
Contact Person: Phillip DeLand
Address: 1228 Titan Way, P.O. Box 3603, Sunnyvale, CA 94088-3603, USA
Phone: +1 408 737 0700, Fax: +1 408 730 9403
E-mail: hplc2011@dionex.com
Website: www.dionex.com
Merck Millipore, a division of Merck KGaA
Merck Millipore, a division of the Merck Group, offers solutions that enable scientists to
conduct life science research easily, efficiently and economically. With a range of more
than 40,000 products, Merck Millipore is one of the top three suppliers of tools to the
life science industry and is also advancing the development of analytical separation
technologies.
Address: Frankfurter Straße 250, 64293 Darmstadt, Germany
Phone: 800 645 5476, Fax: 800 645 5493
Website: www.merck-millipore.com
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National Innovation Office
The National Innovation Office (NIH) is the research, development and innovation organization of the Hungarian Government. NIH provides professional support for private and
government initiatives aiming to exploit and promote the market access of national R&D
results. To this end NIH has a team of analysts and information management experts, and
supports national and international cooperation, and incents the formation of innovation
networks. The National Innovation Office represents Hungary at the EU and at international
organisations in issues relating to research and innovation.
Gedeon Richter Plc.
Gedeon Richter Plc. is a major pharmaceutical company in Hungary and one of the largest
in Central Eastern Europe, with an expanding direct presence in Western Europe. Richter’s
consolidated sales amounted to 1 billion EUR in 2010. The product portfolio of the Company covers almost all important therapeutic areas, such as cardiovascular, central nervous
system, gynecology, etc. The Company has the largest R&D unit in Central Eastern Europe. Original research activity focuses exclusively on CNS disorders with main clinical
targets being schizophrenia, anxiety, chronic pain and depression. With its widely acknowledged steroid chemistry expertise Richter is a significant player in the female healthcare
field worldwide.
Contact Person: Ms. Zsuzsa Beke
Head of Public Relations and Public Affairs
E-mail: posta@richter.hu
Website: www.richter.hu
Shimadzu Europa GmbH
Shimadzu European Operations: Shimadzu is one of the worldwide leading manufacturers
of analytical instrumentation. Its equipment and systems are used as essential tools for
quality control of consumer goods and articles of daily use, in health care as well as in all
areas of environmental and consumer protection. Spectroscopy, chromatography, environ-
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mental analysis, balances, biotechnology and material testing make up a homogeneous yet
versatile offering. Along with many “industry first” technologies and products Shimadzu has
created and invented since 1875, there has also been the exceptional awarding of the
2002 Nobel Prize for Chemistry to Shimadzu engineer Koichi Tanaka for his outstanding
contributions in the field of mass spectrometry.
Markets Served: Shimadzu’s analyzers and equipment are applied in the chemical, petrochemical and pharmaceutical industry, life sciences and biotech, cosmetics, semiconductor and nutrition industry as well as in the flavors and fragrances business. Research
institutes, privately run laboratories, administrations and universities complete the list of
clients. The systems are used in routine and high-end applications, process and quality
control as well as R&D.
Contact Person: Dr. Björn-Thoralf Erxleben
Address: Albert-Hahn-Str. 6–10, 47269 Duisburg, Germany
Phone: +49 203 7687 0, Fax: +49 203 766625
E-mail: shimadzu@shimadzu.eu
Website: www.shimadzu.eu
Sigma-Aldrich
Sigma-Aldrich is a leading Life Science and High Technology company committed to enabling Science to improve the quality of Life.
Supelco and Fluka are the Analytical brands of Sigma-Aldrich. Supelco’s innovative Chromatography products together with Fluka’s high quality analytical reagents and standards are
used for research and control in Pharmaceutical, Food, Environmental, Clinical and many
others areas.
Sigma-Aldrich operates in 40 countries and has over 7,600 employees providing excellent
service worldwide. For more information about Sigma-Aldrich, please visit its award winning
Web site at http://www.sigma-aldrich.com.
Contact Person: Denise de Voogd
Sigma-Aldrich Chemie GmbH
Address: Industriestrasse 25, CH-9471 BUCHS SG
Phone: +41 81 755 2511, Fax: +41 81 756 5449
Website: sigma-aldrich.com
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SILVER SPONSORS
Beckman Coulter
Beckman Coulter is the leading provider of capillary electrophoresis solutions that separate
and characterize molecules, including counter-ions, nucleic acids, basic drugs, enantiomers, proteins and carbohydrates, with high efficiency and reproducibility.
Contact Person: Stacey Winters,
Supervisor, Marketing, North America Commercial Operations
Address: Beckman Coulter, Inc, 250 S. Kraemer Blvd., M-363, Brea, CA 92821, USA
Phone: +1 714 961 3883, Fax: +1 714 578 4207
KNAUER – Wissenschaftliche Gerätebau Dr. Ing. Herbert Knauer GmbH
KNAUER offers instrumentation, accessories and software as well as complete solutions
for both analytical and preparative liquid chromatography applications. The KNAUER product range includes UHPLC/MS systems, biochromatography systems, and sample preparation systems. Solutions for value product purification range from semi-preparative HPLC
to simulated moving bed chromatography.
KNAUER is continuously enhancing products and overall company processes for more
efficiency and sustainability. At HPLC we will present a life cycle assessment according to
ISO 14040 and 14044:2006.
Contact Person: Dr. Alexander Bünz
Address: Hegauer Weg 38, 14163 Berlin, Germany
Phone: +49 30 809 72 7 0, Fax: +49 30 801 50 10
E-mail: info@knauer.net
Website: www.knauer.net
Pfizer
At Pfizer, we apply science and our global resources to improve health and well-being at
every stage of life. We strive to set the standard for quality, safety and value in the discovery, development and manufacturing of medicines for people and animals. Our diversified
global health care portfolio includes human and animal biologic and small molecule medicines and vaccines, as well as nutritional products and many of the world’s best-known
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consumer products. Every day, Pfizer colleagues work across developed and emerging
markets to advance wellness, prevention, treatments and cures that challenge the most
feared diseases of our time.
Contact Person: Dr. Roman Szucs
Senior Research Fellow
Address: Pfizer Limited, Sandwich, Kent CT13 9NJ, United Kingdom
E-mail: roman.szucs@pfizer.com
OFFICIAL MEDIA PARTNERS
SUPPORTING ORGANISATIONS
American Chemical Society, Hungary Chapter
Austrian Society of Analytical Chemistry
Chinese American Chromatography Association (CACA)
CASSS
Central European Group for Separation Sciences
Chromatography and Electrophoresis Group of the Czech Chemical Society
Connecticut Separation Sciences Council
Division of Analytical Chemistry of the Swiss Chemical Society
European Society for Separation Science
Hungarian Academy of Sciences
Interdivisional Group of Separation Science (IGSS) of the Italian Chemical Society
Polish Chemical Society
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Committees, Organisers
Chairman
Attila Felinger (president of HSSS), University of Pécs, Pécs, Hungary
Honorary Chairman
László Szepesy (honorary president of HSSS), Budapest, Hungary
COMMITTEES
Scientific Committee
Günther Bonn
Francesco Dondi
Attila Felinger*
John Frenz*
Georges Guiochon*
William Hancock*
Barry Karger*
Ferenc Kilár
Wolfgang Lindner*
Michel Martin
Pat Sandra
Peter Schoenmakers*
Mark R. Schure
Frantisek Svec
Nobuo Tanaka*
Gyula Vigh
Douglas Westerlund*
Guowang Xu*
Ed Yeung*
University of Innsbruck, Austria
University of Ferrara, Italy
University of Pécs, Hungary
Globelmmune, USA
University of Tennessee, USA
Northeastern University, USA
Northeastern University, USA
University of Vienna, Austria
ESPCI, France
University of Ghent, Belgium
University of Amsterdam, The Netherlands
The Dow Chemical Company, USA
Lawrence Berkeley National Laboratory, USA
Kyoto Institute of Techology, Japan
Texas A&M University, USA
Uppsala University, Sweden
Dalian Institute of Chemical Physics, China
Iowa State University, USA
* indicates Permanent Scientific Committee member
Organising Committee
Attila Felinger
Mária Gazdag
Mónika Babják
László Drahos
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Gedeon Richter Plc., Hungary
Gedeon Richter Plc., Hungary
HAS Chemical Research Center, Hungary
János Harangi
Tamás Janáky
Márton Káldor
Imre Klebovich
Imre Molnár
Róbert Ohmacht
University of Pannonia, Hungary
University of Szeged, Hungary
Simkon Ltd., Hungary
Semmelweis University, Hungary
Molnár-Institute, Germany
Symposium Secretariat
Diamond Congress Ltd.
H-1255 Budapest, P.O.B 48, Hungary
Phone: +36 1 225 0210
Fax: +36 1 201 2680
E-mail: diamond@diamond-congress.hu
Website: www.diamond-congress.hu
ORGANISED BY
Hungarian Society for Separation Sciences, HSSS
c/o Chemistry Institute, University of Pécs
H-7624 Pécs, Ifjúság útja 6., Hungary
Phone: +36 72 501 500 x 24582
E-mail: info@mett.hu
Website: www.mett.hu
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Symposium History
The series of HPLC Symposia started in 1973 and currently the symposium is held at least
annually. It is organised in alternating years in locations in North America and in Europe. In
addition, meetings are held in places outside of these territories, especially in Asia.
The International Symposium on High Performance Liquid Phase Separations and Related
Techniques is an international forum for scientific discussion of the methods of high performance liquid chromatography in its various forms, along with the complementary separation techniques such as electrophoresis, electrochromatography, field-flow fractionation,
supercritical fluid chromatography and hyphenated techniques, such as LC-MS and CZE-MS.
The field of microfluidics or lab-on-a-chip is also included.
1st
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Year
1973
1975
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Location
Interlaken, Switzerland
Wilmington, USA
Salzburg, Austria
Boston, USA
Avignon, France
Cherry Hill, USA
Baden-Baden, Germany
New York City, USA
Edinburgh, UK
San Francisco, USA
Amsterdam, The Netherlands
Washington, USA
Stockholm, Sweden
Boston, USA
Basel, Switzerland
Baltimore, USA
Hamburg, Germany
Minneapolis, USA
Innsbruck, Austria
San Francisco, USA
Birmingham, UK
St. Louis, USA
Granada, Spain
Seattle, USA
Maastricht, The Netherlands
Kyoto, Japan
Montreal, Canada
Nice, France
Chair(s)
Professor Simon
Dr. Kirkland
Professor Huber
Professor Karger
Professor Guiochon
Dr. Bardford
Dr. Hupe
Professor Horváth
Professor Knox
Dr. Majors
Professor Poppe
Professor Guiochon
Professor Westerlund
Professor Karger
Professor Erni
Professor Regnier
Professor Unger
Professors Bowers and Carr
Professor Lindner
Dr. Hancock
Professor Fell
Professor Armstrong
Professor Gelpi
Professor Yeung
Professor Poppe and Dr. Lingeman
Professors Tanaka and Terabe
Professor Wainer
Professor Siouffi
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2004
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2006
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2011
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2013
Philadelphia, USA
Stockholm, Sweden
San Francisco, USA
Ghent, Belgium
Baltimore, USA
Kyoto, Japan
Dresden, Germany
Boston, USA
Budapest, Hungary
Dalian, China
Anaheim, USA
Amsterdam, The Netherlands
Dr. Schure
Professor Westerlund
Dr. Frenz
Professors Crommen and Sandra
Professors Guiochon and Jacobson
Professors Otsuka and Tanaka
Professor Huber
Dr. Cohen
Professor Attila Felinger
Professor Xu
Dr. Svec
Professor Schoenmakers
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Awards
HPLC 2011 Best Poster Award
Sponsored by
Posters presented at HPLC 2011 are reviewed by an international panel of scientists
chaired by Gerard Rozing and Peter Schoenmakers. All presented posters are evaluated
based on three selection criteria:
• Inspiration – creativity, newness, uniqueness, originality
• Transpiration – experimental execution, completeness of the work
• Presentation – overall readability of the poster, visual impression, author’s explanations
Posters will be up for two days. Nominated posters from the first two days will also be
displayed the following two days. Poster presenters who made it into the final round are
asked to stay till the Best Poster Award ceremony on Thursday.
First prize:
1000 EUR
Second prize: 600 EUR
Third prize:
300 EUR
and 6 x 100 EUR, for outstanding posters.
In addition to the 9 prize winners, the remaining nominated posters are awarded with a
certificate. The awards are presented at the closing ceremony.
Csaba Horváth Young Scientist Award
The purpose of the Csaba Horváth Young Scientist Award is to honour the memory of
Professor Csaba Horváth as a father of HPLC and mentor of young scientists in chromatography, furthermore to encourage the participation of young scientists in the HPLC
Symposium series and their visibility as key contributors to the meeting. The award is a
cash grant of $1000–$1500 US and a trophy engraved with the winner’s name. The
winner will also be invited to give an oral presentation at the subsequent HPLC symposium.
This competition is held annually. The award is sponsored by HPLC, Inc.
Eligibility Criteria
Scientists under the age of 35 at the time of the lecture at the HPLC 2011 Budapest
Symposium are eligible. Candidates will be required to provide evidence of eligibility (e. g.,
passport, driver’s license).
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Selection of the winning presentation
The jury will include 6–8 prominent scientists identified by the Permanent Scientific
Committee. The winner will be chosen by the jury, and be announced at the closing
ceremony.
Grant Recipients
HPLC Inc. Student Travel Grant
– Miriam Beneito-Cambra, University of Valencia, Spain
– Elena Chernetsova, Kurchatov Institute, Russia
– Eva Cífková, University of Pardubice, Czech Republic
– Martin Enmark, Karlstad University, Sweden
– Astrid Gjelstad, University of Oslo, Norway
– Vanesa Guillén-Casla, Complutense University of Madrid, Spain
– Nathaly Henry, Institut de Chimie Organique et Analytique, France
– Oswaldo Hernández-Hernández, Organic Chemistry Institute, Spain
– Stefan Mittermayr, Horváth Laboratory of Bioseparation Sciences, Hungary
– Tiziana Pacchiarotta, Leiden University Medical Center, The Netherlands
– Ana Vemić, Faculty of Pharmacy, Serbia
– Katarzyna Wrzosek, Slovak University of Technology in Bratislava, Slovakia
CASSS Student Travel Grants
– Javier Gotta, Universidad Nacional La Plata, Argentina
– Carla Grazieli, University of Campinas, Brazil
– Anna Nordborg, ACROSS, University of Tasmania, Australia
– Tomoyuki Okada, Kyoto Institute of Technology, Japan
– Jing Zhao, University of Macau, China
Pfizer Student Travel Grants
– Tiffany Anne Goodie, Deakin University, Australia
– Clésio Soldateli Paim, Universidade Federal do Rio Grande do Sul, Brazil
– Maria Rambla-Alegre, University Jaume I, Spain
Hungarian Society for Separation Sciences Grants
– Zsuzsanna Darula, HAS Biological Research Centre, Hungary
– Szabolcs Fekete, Budapest University of Technology and Economics, Hungary
– István Ilisz, University of Szeged, Hungary
– Vilmos Kertész, Széchenyi István University, Hungary
– Árpád Könczöl, Gedeon Richter Plc., Hungary
– Ágnes Móricz, HAS Plant Protection Institute, Hungary
– Lilla Turiák, HAS Chemical Research Center, Hungary
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The Eponyms of the Lecture Halls
István Halász
István Halász (1922–1988) was born and educated in Hungary. He received his doctoral degree at the University of Szeged, in 1949. For the next seven years he was on the staff of
the Institute of Physical Chemistry of the Technical University,
Budapest, working closely with Professor Géza Schay.
In 1954, he was one of the first members of the newly
organized Central Research Institute for Chemistry of the
Hungarian Academy of Sciences, Budapest, where he
served as the head of the Department of Gas Adsorption
and Catalysis.
After moving to Germany, he joined in 1957 the Institute of
Physical Chemistry of the Johann Wolfgang Goethe University, in Frankfurt am Main. In 1958, he received the venia
legendi for physical chemistry as a Privatdozent at this University. In the next three
years he simultaneously had positions at the University and in industry, as the head of
the Gas Laboratory of Scholven Chemie AG, in Gelsenkirchen-Buer. In 1961, he was
appointed a full-time Dozent at the University in Frankfurt and in 1964 he received the
title of professor.
In 1970 and 1971 he was visiting professor at Northeastern University, Boston, MA,
USA, and the University of Nice, France. In 1971 he was appointed to the Chair for Applied Physical Chemistry at the University of the Saarland in Saarbrücken.
In the late 1950s and during the 1960s he was involved in a number of important investigations, mainly in the field of open tubular (capillary) columns and in the development of
brush-type bonded-phase packing materials. At the end of the 1960s, he extended his
interest to the field of liquid chromatography and he was one of the pioneers who made
the development of modem high-performance, liquid chromatography possible. He had
important results in almost every aspect of HPLC, both in the theory and practice, analysis
of very small amounts and in preparative work, high and low pressures, packed and opentube columns, and in the preparation and investigation of high-efficiency column packing
materials.
Recognizing his significant contribution to chromatography, István Halász was awarded in
1978 with the Chromatography Commemorative Medal of the U.S.S.R. Academy of Sciences, and in 1980 he received the Tswett Chromatography Award. His scientific works
comprised more than 130 publications. He supervised more than 50 diploma and postgraduate students in the course of his teaching career.
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Csaba Horváth
Csaba Horváth (1930–2004) was born in Szolnok, Hungary
and graduated as a chemical engineer from the Technical
University in Budapest in 1952. Then he worked for 4 years
the Department of Organic Chemical Technology at the same
university. In 1956, Csaba Horváth left Hungary and for the
following 4 years, he worked at Farbwerke Hoechst AG in
Frankfurt am Main in Germany. In 1961 he joined the group
of Professor István Halász under whose supervision he did
doctoral research on open-tubular columns for gas chromatography at the Johann Wolfgang Goethe University in Frankfurt am Main in Germany. Having received a PhD in 1963, he
emigrated to the United States and started research at the
Harvard Medical School in Boston. In the following year, he
moved to Yale University. He chaired the Department of Chemical Engineering at Yale from
1987 to 1993 and was appointed as Roberto C. Goizueta Professor of Chemical Engineering in 1998. He held that chair until his death in 2004.
From the beginning, he focused his interests on the separation of samples of biological
origin, thus Csaba Horváth is the pioneer of modern bioanalytical chemistry. Csaba Horváth designed and built the first HPLC instrument with microbore HPLC columns. He
later pioneered the new technique of reversed-phase chromatography (RPC) and developed the solvophobic theory of RPC retention. He worked on the entropy–enthalpy compensation in the study of RPC retention mechanism, established the modern use of
displacement chromatography in biotechnology, and developed the fundamentals of
electrochromatography.
Among the numerous honors bestowed upon Csaba Horváth are the Stephen Dal Nogare
Award of the Forum of the Delaware Valley (1978), the Anniversary Tswett Medal of the
USSR Academy of Sciences (1979), the Tswett Chromatography Award (1980), the
Humboldt Award for Senior American Scientists (1982), the Chromatography Awards of
the American Chemical Society (1983) and of Eastern Analytical Symposium (1986), the
Merit Award of NIH (1993), the A. J. P. Martin Gold Medal of the Chromatographic Society (1994), the Halász Medal Award of the Hungarian Society for Separation Sciences
(1997), the Golay Award (1999), the Michael Widmer Award of the Swiss Chemical Society (2000), the Austrian Cross for Science and Arts, first class (2002), the Torbern
Bergman Medal of the Swedish Chemical Society (2003). He was an external member of
the Hungarian Academy of Sciences (1990), a member of the Connecticut Academy of
Sciences and Engineering (1992), a Founding Fellow of the American Institute for Medical
and Biomedical Engineering (1992), a Fellow of the American Institute of Chemical Engineers (1994) and of the California Separation Sciences Society (1998). In January 2004,
Csaba was elected a member of the US National Academy of Engineering.
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Szabolcs Nyiredy
Szabolcs Nyiredy (1950–2006) graduated in pharmacy from
the Semmelweis University (Budapest) in 1975. In 1976 he
received the Doctor of Pharmacy degree, then in 1978 the
Diploma of Professional Pharmacist of Pharmaceutical Technology. Working in the Institute of Medicinal Plants and Drugs
of the Semmelweis University he became a Professional Pharmacist for Pharmacognosy and Phytochemistry in 1983. In
1984 he obtained the CSc degree and in 1991 the DSc degree
from the Hungarian Academy of Sciences. In 2004 he was
elected as a member of the Hungarian Academy of Sciences.
He contributed to the introduction of the forced flow planar
chromatographic technique, overpressure planar liquid chromatography (OPLC) developed in Hungary. In 1983 he started
to work at the Department of Pharmacy at the ETH in Zürich as a research fellow. In
1984 he was promoted to associate professor.
His research activity was focused around the analysis and preparative isolation of various
groups of components with similar structures of medicinal plants. He developed the
PRISMA system for selection and optimization of operating parameters in TLC and HPLC.
In order to improve the extraction and separation techniques he developed and applied a
number of off-line forced flow analytical and micropreparative methods as well as on-line
preparative operations. He developed a new rotation planar chromatograph for the implementation of various centrifugal planar chromatographic techniques.
After his return from Switzerland to Hungary, in 1990 he became the General Director
and Chairman of the Board of the Research Institute for Medicinal Plants in Budakalász.
He held that position until his untimely death in 2006. He developed new strategies and
methods for determination and isolation of valuable compounds from medicinal plants.
He was board member of the European Federation of Pharmaceutical Societies, the European Society for Separation Sciences, and the Central European Group for Separation
Sciences.
He was the founding president of the Hungarian Society for Separation Sciences (1996),
the president of the Hungarian Society for Pharmaceutical Sciences (2004). He founded
the Journal of Planar Chromatography – Modern TLC (JPC) and was until his death its
Editor-in-Chief.
Szabolcs Nyiredy organized a large number of international conferences. He launched an
international series of symposia, the Balaton Symposium on High-Performance Separation
Methods, which has grown to one of the most important European separation science events.
He was recognised and honoured with numerous awards and titles. Some of the most notable were the Waksmundzki medal, the Koritsánszky medal, the Medical Academy of Lublin
Award, the Societies Pharmaceutica Hungarica medal, the Schulek medal, the Tswett medal,
the Dabis medal and the Dénes Gábor Award. Posthumously he received the Csaba Horváth
Memorial Award from the Hungarian Society for Separation Sciences in 2007.
23
12:15
13:00
13:45
14:00
14:15
14:30
14:45
15:00
15:15
15:30
15:45
16:00
16:15
16:30
16:45
17:00
17:15
17:30
17:45
18:00
18:15
18:30
18:45
19:45
20:00
20–21
24
OPENING
CEREMONY
AWARD
PRESENTATIONS
WELCOME
RECEPTION
LUNCH
19:15
19:30
ORGAN
CONCERT
VENDOR
SEMINARS
LUNCH
VENDOR
SEMINARS
LUNCH
VENDOR
SEMINARS
COFFEE BREAK
COFFEE BREAK
COFFEE BREAK
TUTORIAL
LECTURES
TUTORIAL
LECTURES
TUTORIAL
LECTURES
SYMPOSIUM
DINNER
Detection in
microfluidics
Szabolcs Nyiredy Hall
Stationary phases
István Halász Hall
COFFEE BREAK
Proteomics
Chiral separations
Advances in separation technology
Csaba Horváth Hall
Biomarkers
Biopharmaceuticals
Retention mechanism
Csaba Horváth Hall
Pharmaceutical
analysis
Metabolomics
In memory of
Csaba Horváth
Csaba Horváth Hall
22 June, Wed
Multidimensional
Separations
Csaba Horváth Hall
HPLC-MS
Ion chromatography,
ionic liquids
Fundamental aspects
of separations...
Csaba Horváth Hall
Proteomics
Column technology
In memory of
Csaba Horváth
Csaba Horváth Hall
Proteomics
12:30
COFFEE BREAK
Industrial
separations
Multidimensional and
planar chromatography
12:00
COFFEE BREAK
21 June, Tue
Fundamental aspects
of separations...
Csaba Horváth Hall
11:45
PLENARY
LECTURES
Chemometrics
11:30
DNA & Biopharmaceuticals
9:15
Microfluidics
11:15
20 June, Mon
In memory of
Csaba Horváth
Csaba Horváth Hall
11:00
Electrodriven methods
10:45
Particle technology
Csaba Horváth Hall
9:30
Stationary phases for
sample preparation
10:30
#1 #2 #3
19 June, Sun
In memory of
Uwe Neue
Csaba Horváth Hall
10:15
SHORT COURSES
10:00
#4 #5 #6
9:45
SHORT COURSES
REGISTRATION
9:00
23 June, Thu
COFFEE BREAK
12:45
13:15
LUNCH
13:30
VENDOR
SEMINARS
POSTER SESSION POSTER SESSION POSTER SESSION
EXHIBITION
COFFEE BREAK
EXHIBITION
EXHIBITION
EXHIBITION
POSTER SESSION
PLENARY
LECTURES
CLOSING
CEREMONY
FAREWELL
RECEPTION
PLENARY
LECTURES
19:00
Scientific Programme Short Courses
Sunday, 19 June 2011, 9:00–12:00
SC #1
Nyiredy Hall
Enantioselective Liquid Chromatography: Concepts, Column Technology and
Practical Aspects
Michael Lämmerhofer, Wolfgang Lindner
University of Vienna, Vienna, A
SC #2
Mass Spectrometry and its Chromatography Coupling
Michal Holčapek
University of Pardubice, Pardubice, CZ
Liszt Hall
SC #3
Mozart Hall
Supercritical Fluid chromatography in the Pharmaceutical Industry
Larry Miller1, Larry Taylor2
1
Amgen, Cambridge, MA, USA; 2Virginia Tech University, Blacksburg, VA, USA
Sunday, 19 June 2011, 13:00–16:00
SC #4
Liszt Hall
Current Trends in Liquid Chromatography: Understanding the Theory behind the
Practice
Torgny Fornstedt1, Alberto Cavazzini2, Jörgen Samuelsson1
1
Karlstad University, Karlstad, S; 2Ferrara University, Ferrara, I
SC #5
Pretreatment of Biofluids for LC-MS/MS Analysis of Small Molecules
Karl-Siegfried Boos
University of Munich, Munich, D
Mozart Hall
SC #6
Nyiredy Hall
Recent Developments in Pharmaceutical and Bio-Pharmaceutical Analysis
Pat Sandra1, Frédéric Lynen1, Roman Szucs2, Claudio Brunelli2, Koen Sandra3
1
Pfizer Analytical Research Centre, Ghent Universty, Ghent, B;
2
Pfizer Global R&D, Analytical R&D, Sandwich, Kent, UK;
3
Metablys, Research Institute for Chromatography, Kortrijk, B
Advance registration was required for the short courses.
25
26
Lecture Programme
Sunday, 19 June 2011
17:00–17:30
OPENING CEREMONY
17:30–18:00
Halász Medal Award Ceremony
Csaba Horváth Memorial Award Ceremony
18:00–19:00
PLENARY LECTURES
Chair: László Szepesy
Csaba Horváth Hall
18:00–18:30
PL01
Recent Progress in Column Technology Begets Progress in our Understanding
of Column Efficiency
Georges Guiochon1, Fabrice Gritti2
1
University of Tennessee, Knoxville, TN, USA;
2
Oak Ridge National Laboratory, Oak Ridge, TN, USA
18:30–19:00
PL02
Dynamical Structure Activity Relationship of Peptides and Proteins
András Perczel
Eötvös University, Budapest, H
19:00–21:00
WELCOME RECEPTION
27
28
Lecture Programme
Monday, 20 June 2011
9:00–10:30
PLENARY LECTURES
Chair: Peter Schoenmakers
Csaba Horváth Hall
9:00– 9:30
PL03
A New Preparative-Scale Isoelectrophoretic Trapping Device: Design,
Construction and First Characterization
Robert Y. North, Gyula Vigh
Texas A&M University, College Station, TX, USA
9:30–10:00
PL04
Novel Enrichment and Separation Methods as Fundamental Tools in
Bioanalysis
G. K. Bonn, R. Bakry, M. Rainer, C. W. Huck
Leopold-Franzens University Innsbruck, Innsbruck, A
10:00–10:30
PL05
Continuous Chromatography (MCSGP) for the Purification of Therapeutic
Proteins
Massimo Morbidelli
ETH, Zürich, CH
EXHIBITION
10:30–11:00
Coffee Break /
11:00–12:30
PARTICLE TECHNOLOGY
Chair: Mark R. Schure
Csaba Horváth Hall
11:00–11:30
KN01
Toward Higher Chromatographic Efficiency: Future Challenges in Column and
Instrument Technologies
Fabrice Gritti
The University of Tennessee, Knoxville, TN, USA; Oak Ridge National Laboratory,
Oak Ridge, TN, USA
29
11:30–11:50
L01
On the Finite Band Width of Particle Size Distribution of Core-Shell Particles
and the Relationship to their Chromatography Mass Transfer Mechanism
Jesse O. Omamogho1, Jeremy D. Glennon1, Georges Guiochon2,
presented by Joseph Stankovich2
1
Irish Separation Science Cluster (ISSC) and Analytical and Biological Research
Facility (ABCRF), University College Cork, IRL;
2
University of Tennessee, Knoxville, TN, USA
11:50–12:10
L02
Novel Hydrophilic Bonded-Phase Fused-Core Particles Demonstrating Highly
Efficient HILIC Separations
Barry E. Boyes, Timothy Langlois, Joseph J. DeStefano, Joseph J. Kirkland
Advanced Materials Technologies, Inc., Wilmington, DE, USA
12:10–12:30
L03
Current Levels of Performance of Commercial HPLC Columns Made with CoreShell Sorbent Particles and Further Advancements in the Field
Tivadar Farkas, Jason Anspach, Carl Sanchez, Mike Chitty
Phenomenex Inc., Torrance, CA, USA
11:00–12:30
DNA, BIOPHARMACEUTICALS, QbD
Chair: Klára Valkó
11:00–11:30
KN02
Electromigration of Single Protein and DNA Molecules in Nanopores
Edward S. Yeung, C. Ma, R. Han, S. Qi
Iowa State University Ames, IA, USA
11:30–11:50
L04
Biointeraction Analysis by High Performance Frontal Affinity Chromatography:
Immobilized PPAR-γγ Receptor
Temporini Caterina1, Calleri Enrica1, Fracchiolla Giuseppe2, Montanari Roberta3,
Pochetti Giorgio3, Lavecchia Antonio4, Loiodice Fulvio2, Novellino Ettore4,
Caccialanza Gabriele1, Massolini Gabriella1
1
Università degli Studi di Pavia, Pavia, I;
2
Università degli Studi di Bari “Aldo Moro”, Bari, I;
3
Istituto di Cristallografia, Consiglio Nazionale delle Ricerche, Rome, I;
4
Università degli Studi di Napoli “Federico II”, Naples, I
30
11:50–12:10
L05
New Separation Media and Methods for Plasmid DNA Analysis
Michael Lämmerhofer, Marek Mahut, Elisabeth Haller, Andrea Gargano,
Wolfgang Lindner
12:10–12:30
L06
Quality by Design (QbD) in the Development of an Analytical Chromatographic
Method
Frank Hu, Karthik Jayaraman, Frank Tomasella
Bristol Myers Squibb Company, New Brunswick, NJ, USA
11:00–12:30
PROTEOMICS
Chair: Robert Kennedy
11:00–11:30
KN03
Ultratrace Proteomic Analysis of 10,000 Laser Capture Microdissection
Breast Cancer Cells using 2D/LC/MS with a Porous Layer Open Tubular
(PLOT) Column
Barry L. Karger
Northeastern University, Boston, MA, USA
11:30–11:50
L07
The Long Way to a Global Foodomics Approach
Clara Ibañez, Carolina Simo, Virginia Garcia-Cañas, Miguel Herrero, Elena Ibañez,
Alejandro Cifuentes
Institute of Food Science Research (CSIC), Madrid, E
11:50–12:10
L08
The Potential of Polymer Monolithic Column Technology in Combination with
High-Resolution Mass Spectrometry for the Analysis of Proteins Isoforms
Sebastiaan Eeltink1, Bert Wouters1, Achim Treumann2
1
Vrije Universiteit Brussel, Brussels, B;
2
North East Proteome Analysis Facility, Newcastle upon Tyne, UK
12:10–12:30
L09
A Challenge for nanoUPLC-MS/MS: Determination of Glycosylation Patterns
Olivér Ozohanics, Lilla Turiák, Ádám Lengyel, Károly Vékey, László Drahos
Chemical Research Center, HAS, Budapest, H
12:30–13:30
Lunch
31
13:30–14:30
VENDOR SEMINARS
13:30–15:30
POSTER SESSION / EXHIBITION
14:30–15:15
Coffee break
15:30–16:15
TUTORIAL LECTURES
Chair: Michael Lämmerhofer
Csaba Horváth Hall
T01
Hydrophilic Interaction Chromatography: is it a Viable Complimentary Method
to Reversed-Phase for the Separation of Polar or Ionisable Compounds?
David V. McCalley
University of the West of England, Bristol, UK
Chair: Tibor Kremmer
T02
SPME for Liquid Phase Separations
Janusz Pawliszyn
University of Waterloo, Waterloo, CDN
Chair: Andrew Shalliker
T03
The Requirements for High Reproducibility, High Recovery and High Resolution
in Electrophoresis, Chromatography, Centrifugation, Diffusion…
Stellan Hjertén
Uppsala University, Uppsala, S
16:15–17:45
IN MEMORY OF UWE NEUE
Chair: Gyula Vigh
Csaba Horváth Hall
16:15–16:45
KN04
Novel HILIC and HILIC-Mixed Mode Stationary Phases: Potentials and Pitfalls
Wolfgang Lindner, Georg Schuster, Anna Bletsou, Michal Kohout
16:45–17:05
L10
Uwe Neue’s Contributions to HPLC Column Technology
Thomas H. Walter
Waters Corportaion, Milford, MA, USA
32
17:05–17:25
L11
Illustration of Peptide Retention Behavior in HILIC with Retention Prediction
Model
Martin Gilar1, Aleksander Jaworski2
1
Waters Corporation, Milford, MA, USA;
2
Waters Corporation, Franklin, MA, USA
17:25–17:45
L12
New Test Method for Chromatographic Characterization of Hydrophilic
Interaction Chromatography (HILIC) Stationary Phases
Tohru Ikegami1, Yusuke Kawachi1, Hirotaka Takubo1, Masatoshi Miyamoto1,
Nobuo Tanaka1,2
1
Kyoto Institute of Technology, Kyoto, J;
2
GL Science Inc., Saitama, J
16:15–17:45
STATIONARY PHASES FOR SAMPLE PREPARATION
Chair: Günther Bonn
16:15–16:45
KN05
Chromatographic Adsorbents and their Application in Therapy
Karl-Siegfried Boos
University of Munich, Munich, D
16:45–17:05
L13
New Selective Extraction Tool Based on Aptamers for the Sample
Pretreatment. Comparison with Immunosorbents and Molecularly Imprinted
Polymers
Valérie Pichon, Sonia Lordel, Valérie Thibert, Florence Chapuis-Hugon
LSABM, ESPCI, Paris, F
17:05–17:25
L14
New Observations on the Isotherm and Kinetics of Molecularly Imprinted
Polymers
Bettina Lorántffy, Blanka Tóth, George Horvai
Budapest University of Technology and Economics, Budapest, H
17:25–17:45
L15
Monodispersed Molecularly Imprinted Polymer for Selective Extraction of
Active Compounds and their Analogues
Jun Haginaka, Noriko Funaya, Tomoko Kitabatake
Mukogawa Women’s University, Nishinomiya, J
33
16:15–17:45
ELECTRODRIVEN METHODS
Chair: Marja-Liisa Riekkola
16:15–16:45
KN06
Highly Sensitive Microscale Electrophoretic Analysis of Biogenic Compounds
using On-Line Sample Concentration
Takayuki Kawai, Saeko Kinami, Hiroshi Koino, Kenji Sueyoshi, Fumihiko Kitagawa,
Koji Otsuka
Kyoto University, Kyoto, J
16:45–17:05
L16
Capillary Isoelectric Focusing Combined with MS Detection
Ferenc Kilár1, Csilla Páger1, Andrea Vargová1, Anna Takácsi-Nagy1,
Wolfgang Thormann2
1
University of Pécs, Pécs, H;
2
University of Bern, Bern, CH
17:05–17:25
L17
Application of Capillary Electrophoresis for the Characterization of Chemically
Modified Allergens
S. Gusenkov, C. Ackaert, G. J. Oostingh, H. Stutz
University of Salzburg, Salzburg, A
17:25–17:45
L18
Csaba Horváth Young Scientist Award Nominee
An Interface for High Speed Multidimensional Capillary Electrophoresis
Separations
John D. Chin, Cameron D. Skinner
Concordia University, Montréal, CDN
19:30
34
ORGAN CONCERT
35
Lecture Programme
Tuesday, 21 June 2011
9:00–10:30
IN MEMORY OF CSABA HORVÁTH
Chair: Georges Guiochon
Csaba Horváth Hall
9:00– 9:30
KN07
Csaba Horváth, the Revolutionizer of Life Science
Imre Molnár
Molnár-Institute, Berlin, D
9:30– 9:50
L19
Highly Hydrophilic Monolith for Affinity Chromatography at Reduced
Nonspecific Interactions
Ziad El Rassi, Dilani N. Gunasena
Oklahoma State University, Stillwater, OK, USA
9:50–10:10
L20
Modulation of Migration Behaviour of Biological Molecules in Capillary
Electrodriven Separation Systems
Danilo Corradini, Antonella De Rossi, Isabella Nicoletti
CNR, Institute of Chemical Methodologies, Rome, I
10:10–10:30
L21
Analysis of Peptides and Proteins with Fused Core and UHPLC Technologies
A. Staub, D. Zurlino, J. Ruta, S. Rudaz, J. L. Veuthey, D. Guillarme
University of Geneva, University of Lausanne, Geneva, CH
9:00–10:30
METABOLOMICS
Chair: Károly Vékey
9:00– 9:30
KN08
Insights to Cellular Function using Microfluidics and LC-MS Based
Metabolomics
Robert T. Kennedy, Matt Lorenz, Ting Zhang, Chunhai Ruan
University of Michigan, Ann Arbor, MI, USA
36
9:30– 9:50
L22
New CE-MS Systems for Analysis of Biopharmaceuticals
G. J. de Jong, R. Haselberg, G. W. Somsen
Utrecht University, Utrecht, NL
9:50–10:10
L23
Lipidomic Profiling of Biological Tissues and Human Plasma using Off-Line
2D-LC-MS/MS
Michal Holčapek, Eva Cífková, Miroslav Lísa
10:10–10:30
L24
A Comprehensive Metabolomics Approach: Applicability to Urinary Tract
Infection
Tiziana Pacchiarotta, Cees van Niewkoop, Ekaterina Nevedomskaya, Rico Derks,
Artem Artemov, Bart Schoenmaker, Paul Hensbergen, Manfred Wuhrer,
Jaap van Dissel, André Deelder, Oleg Mayboroda
Leiden University Medical Center, Leiden, NL
9:00–10:30
PHARMACEUTICAL ANALYSIS
Chair: William Hancock
9:00– 9:30
KN09
Advanced Applications of Separation Science in Pharmaceutical and
Biomedical Analysis
Douglas Westerlund
Uppsala University, Uppsala, S
9:30– 9:50
L25
Electro Membrane Extraction – a Novel Invention for Rapid Bioanalytical
Sample Preparation
Astrid Gjelstad, Stig Pedersen-Bjergaard
University of Oslo, Oslo, N
9:50–10:10
L26
Applications of Multi-Dimensional Chromatography in the Pharmaceutical
Industry
Rudy Sneyers, Jeroen Peeters, Luc van Grieken, Gaby Török
Janssen Pharmaceutical Companies of Johnson & Johnson, Beerse, B
37
10:10–10:30
L27
Comparison of Off-Line, On-Line and Stop-Flow Comprehensive-2-Dimensional
Liquid Chromatographic Methods for the Analysis of Phenolic Compounds
André de Villiers, Kathithileni M. Kalili
Stellenbosch University, Matieland, ZA
EXHIBITION
10:30–11:00
Coffee Break /
11:00–12:30
Chair: Imre Molnár
Csaba Horváth Hall
11:00–11:30
KN10
Next-Generation Biologics: Development Challenges for Recombinant Yeast as
a Therapeutic Biopharmaceutical
John Frenz
GlobeImmune, Inc., Louisville, CO, USA
11:30–11:50
L28
Inspirations from Cs. Horváth in Biotechnology
Ann L. Lee
Genentech Inc. a Member of the Roche Group, San Francisco, CA, USA
11:50–12:10
L29
siRNA Analysis by UPLC and MS Related Techniques
Rong Xiang, Sarah Young, Huimin Yuan, Bing Mao
Merck & Co., Inc., Rahway, NJ, USA
12:10–12:30
L30
Characterization of PEGs and PEGylated Biotherapeutics by Electrospray
Ion-Mobility Time-of-Flight Mass Spectrometry Coupled with Ion-Molecule
Reactions
Isabelle Gusev1, Asish B. Chakraborty2, Weibin Chen2, StJohn Skilton2,
Jeff Mazzeo2, Jesse Z. Dong1
1
IPSEN/Biomeasure Inc., Milford, MA, USA;
2
Waters Corporation, Milford, MA, USA
38
11:00–12:30
COLUMN TECHNOLOGY
Chair: Steven A. Cohen
11:00–11:30
KN11
New Functionalized Metal Oxide Materials and Ionic Liquid Modified Silica
Materials for Solid Phase Extraction, Capillary Liquid Chromatography and
Capillary Electrochromatography
Marja-Liisa Riekkola1, Lorena Vidal1,2, Clara Baños-Pérez1, Giovanni D’Orazio1,3,
Jan-Henrik Smatt4, Susanne K. Wiedmer1, Salvatore Fanali3
1
University of Helsinki, Helsinki, FIN;
2
Universidad de Alicante, Alicante, E;
3
Institute of Chemical Methodologies, Rome, I;
4
Abo Akademi University, Abo, FIN
11:30–11:50
L31
Capillary Titania (TiO2) Monoliths for Micro-Extraction of Phosphorylated
Compounds
Maguy Abi Jaoudé, Jérôme Randon
Université de Lyon, Villeurbanne, F
11:50–12:10
L32
Structural Approaches to Improved Performance of Monolithic HPLC
Columns
Kazuki Nakanishi1, Risako Ito1, Kei Morisato1,2, Shota Miyazaki2,
Masayoshi Ohira2, Masahiro Furuno2, Nobuo Tanaka2
1
Kyoto University, Kyoto, J;
2
GL Sciences Inc., Saitama, J
12:10–12:30
L33
Porous Polymer Monoliths for Small Molecule Separations: Advancements and
Limitations
Ivo Nischang, Ian Teasdale, Oliver Brüggemann
Johannes Kepler University Linz, Leonding, A
39
11:00–12:30
PROTEOMICS
Chair: Barry Karger
11:00–11:30
KN12
A New Challenge for Separation Science: The Specification of the Parts Lists
of the Human Proteome, the Study of Chromosome 17, Human Proteome
Project (HPP)
W. Hancock1, G. Omenn2, M. Snyder3, R. Beavis4
1
Northeastern University, Boston, MA, USA;
2
University of Michigan, USA;
3
Stanford University, USA;
4
University of British Columbia, CDN
11:30–11:50
L34
New Separation and Identification Techniques for Proteome Analysis
Yukui Zhang
Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian, PRC
11:50–12:10
L35
LC-MS Based Label-Free Quantification of Proteins Separated by 1D and 2D
Gel Electrophoresis
Zoltán Szabó, István Földi, Judit Szeliné Szomor, Tamás Janáky
University of Szeged, Szeged, H
12:10–12:30
L36
A Proteomic Snapshot of Breast Cancer Cell Cycle: The G1/S Transition Point
Iulia M. Lazar, Milagros J. Tenga
Virginia Polytechnic Institute and State University, Blacksburg, VA, USA
12:30–13:30
Lunch Sponsored by
13:30–14:30
VENDOR SEMINARS
13:30–15:30
14:30–15:15
Coffee break
40
15:30–16:15
TUTORIAL LECTURES
Chair: Karl-Siegfried Boos
T04
HPLC-MS: A Big Challenge or a Perfect Solution?
Olivér Ozohanics, Lilla Turiák, László Drahos, Károly Vékey
Csaba Horváth Hall
Chair: Ulrich Tallarek
T05
Transport, Sensing and Separations in Nanofluidic Devices
Stephen C. Jacobson
Indiana University, Bloomington, IN, USA
Chair: Janusz Pawliszyn
T06
Chemometrics and Chromatographic Fingerprints
Beata Walczak
University of Silesia, Katowice, PL
16:15–17:45
Chair: Ernő Tyihák
Csaba Horváth Hall
16:15–16:45
KN13
Applications of Bio-Mimetic HPLC for the Estimation of In Vivo Distribution of
Drug Discovery Compounds
Klara Valko
GlaxoSmithKline, Stevenage, UK
16:45–17:05
L37
Rapid Ultra-Performance Size-Based Separations of Biomolecules
Edouard S. P. Bouvier, Susan Serpa, Kevin D. Wyndham, Nicole L. Lawrence,
Paula Hong, Thomas H. Walter
17:05–17:25
L38
Using UHPLC and Design of Experiments (DOE) to Develop High-Throughput
Charge Heterogeneity Analysis of Monoclonal Antibodies
Dell Farnan, Jennifer Wang, Tony G. Moreno, Toby Reichenberg
Genentech Inc. A Member of the Roche Group, San Francisco, CA, USA
17:25–17:45
L39
Hungarians in the Separation Sciences
Tibor Kremmer
41
16:15–17:45
MICROFLUIDICS
Chair: František Foret
16:15–16:45
KN14
Microfabricated Carbon Nanotube Based Separation Columns for Microchip
Electrochromatography
Klaus B. Mogensen, Miaoxiang Chen, Kristian Molhave, Peter Boggild,
Jörg P. Kutter
Technical University of Denmark, Lyngby, DK
16:45–17:05
L40
Usefulness of Monolithic Frits, Obtained with UV-LED Polymerization, for
Applications in nano-LC and CEC
Salvatore Fanali, Zeineb Aturki, Giovanni D’Orazio, Anna Rocco
Institute of Chemical Methodologies, Rome, I
17:05–17:25
L41
Development of Pressure-Driven Chromatography in Extended Nanochannels:
Toward High Resolution Separation
Ryo Ishibashi, Kazuma Mawatari, Takehiko Kitamori
The University of Tokyo, Tokyo, J
17:25–17:45
L42
Structural Analysis of Endotoxins by Microchip and Mass Spectrometry
Anikó Kilár, Lilla Makszin, Ágnes Dörnyei, Béla Kocsis, Ferenc Kilár
University of Pécs, Pécs, H
16:15–17:45
CHEMOMETRICS
Chair: Paul R. Haddad
16:15–16:45
KN15
Experimental Design-Based Method Development and its Translation to
Chromatographic Methods
Yvan Vander Heyden1, B. Dejaegher1, M. Dumarey1, R. Sneyers2, W. Janssens2,
I. Somers2
1
2
Johnson & Johnson Pharmaceutical Research & Development, Beerse, B
16:45–17:05
L43
Smart Peak Detection in Comprehensive Two-Dimensional Chromatography
Gabriel Vivó-Truyols, Peter J. Schoenmakers
University of Amsterdam, Amsterdam, NL
42
17:05–17:25
L44
A Metabolomic Approach to Extend the Steroid Profile Monitoring for Doping
Control Analysis
Julien Boccard1,2, Flavia Badoud1,2,3, Elia Grata2,3, Jean-Luc Veuthey1,2,
Martial Saugy2,3, Serge Rudaz1,2
1
University of Lausanne, Geneva, CH;
2
University of Geneva, Geneva, CH;
3
University Center of Legal Medicine, Epalinges, CH
17:25–17:45
L45
HPLC Retention as an Ancillary Tool for Compound Identification: Easy and
Accurate Cross-Platform Retention Prediction by Back-Calculation of Gradient
and Flow Rate Profiles
Paul G. Boswell, Jonathan R. Schellenberg, Peter W. Carr, Jerry D. Cohen,
Adrian D. Hegeman
University of Minnesota, Minnesota, MN, USA
43
44
Lecture Programme
Wednesday, 22 June 2011
9:00–10:30
RETENTION MECHANISM
Chair: Alberto Cavazzini
Csaba Horváth Hall
9:00– 9:30
KN16
The Effect of Pressure on Solute Retention in Reversed-Phase Liquid
Chromatography
Kensuke Okusa1, Yuki Suita Iwasaki1, Hideyuki Uzu1, Kyo Miyaki1, Mineo Tahara2,
Tohru Ikegami3, Nobuo Tanaka1,3, Masakazu Takahashi1, Masayoshi Ohira1
1
GL Sciences Inc., Saitama, J; 2GL Sciences Inc., Fukushima, J;
3
Kyoto Institute of Technology, Kyoto, J
9:30– 9:50
L46
Residual Silanols – the Old Problem and the New Facts in Chromatographic Elution
Bogusław Buszewski, Szymon Bocian
Nicolaus Copernicus University, Torun, PL
9:50–10:10
L47
Use of Computational Fluid Dynamics to Establish and Validate Novel B-term
Diffusion Expressions for Packed Bed and Monolithic Columns
Gert Desmet, Sander Deridder
Vrije Universiteit Brussel, Brussels, B
10:10–10:30
L48
Physical Reconstruction of Packed Beds and their Morphological Analysis
Stefan Bruns, Ulrich Tallarek
Philipps-Universität Marburg, Marburg, D
9:00–10:30
BIOPHARMACEUTICALS
Chair: Douglas Westerlund
9:00– 9:30
KN17
Purification and Characterisation of Large Biomolecular Assemblies by
Monolithic Columns
Alois Jungbauer
University of Natural Resources and Life Sciences, Vienna, A
45
9:30– 9:50
L49
Analysis of Proteomes by 2D-LC-MS Applying Displacement Chromatography
Maria Trusch1, Kati Tillack2, Mireia Sospedra2, Roland Martin2,
Oliver Kohlbacher3, Hartmut Schlüter1
1
University Medical Center Hamburg-Eppendorf, Hamburg, D;
2
Center for Molecular Neurobiology Hamburg, Hamburg, D;
3
Eberhard-Karls-Universität Tübingen, Tübingen, D
9:50–10:10
L50
Using LC Separation Techniques for Mass Balance and Characterization of
Recombinant Protein Vaccine Candidates and Process Intermediates During
Development and cGMP Manufacture
Jordan Plieskatt, Wanderson Rezende, Maria Elena Bottazzi, Peter J. Hotez
The George Washington University and Sabin Vaccine Development, Washington
DC, USA
10:10–10:30
L51
Application of Various Modes of High Performance Liquid Chromatography for
Protein Analysis
Sandra Grotefend, Lukas Kaminski, Stefanie Wroblewitz, Hermann Wätzig
Technische Universität Braunschweig, Braunschweig, D
9:00–10:30
BIOMARKERS
Chair: John Frenz
9:00– 9:30
KN18
Biomarker Discovery for Multiple Sclerosis in Cerebrospinal Fluid by
Microfluidics-HPLC MS
Therese Rosenling1, Marcel Stoop2, Amos Attali3, Hans van Aken3,
Ernst Suidgeest3, Christin Christin1, Christoph Stingl2, Frank Suits4,
Peter Horvatovich1, Rogier Hintzen2, Tinka Tuinstra3, Theo Luider2,
Rainer Bischoff1
1
University of Groningen, Groningen, NL;
2
Erasmus University Medical Center, Rotterdam, NL;
3
Abbott Healthcare Products B.V., Weesp, NL;
4
IBM TJ Watson Research Centre, Yorktown Heights, NY, USA
9:30– 9:50
L52
Glycoproteomic Markers of Glioblastoma Cancer Stem Cells
David M. Lubman, Jintang He, Yashu Liu, Nancy Lan Dai, Xing Fan
University of Michigan Medical Center, Ann Arbor, MI, USA
46
9:50–10:10
L53
Quantitative Glycan Profiling and Oligosaccharide Identification in Cancer
Diagnostic and Prognostic Measurements
Milos V. Novotny, William R. Alley, Jr., Jacqueline Vasseur, John A. Goetz
10:10–10:30
L54
Novel Derivatization Strategies for the LC-MS Based Determination of
Biomarkers and Cellular Metabolites
Martin Giera1, Dick Paul Kloos1,2, Henk Lingeman1, Oleg Mayboroda2,
Hubertus Irth1, Wilfried M. A. Niessen1
1
VU University Amsterdam, Amsterdam, NL; 2LUMC Leiden, Leiden, NL
EXHIBITION
10:30–11:00
Coffee Break /
11:00–12:30
FUNDAMENTAL ASPECTS OF SEPARATIONS:
HONOURING GEORGES GUIOCHON
Chair: Stephen Jacobson
Csaba Horváth Hall
11:00–11:30
KN19
Introduction
Francisco Farre Rius1, Attila Felinger2
1
Spanish National Research Council, Barcelona, E; 2University of Pécs, Pécs, H
11:30–11:50
L55
Different Approaches to Complexity in Stochastic Theory of Chromatography
Francesco Dondi, Alberto Cavazzini, Luisa Pasti
University of Ferrara, Ferrara, I
11:50–12:10
L56
Renewal of an Old Method: Taylor Dispersion Analysis for Size
Characterization of Nanomaterials
Michel Martin1, Jean-Philippe Biron2, Hervé Cottet2
1
Ecole Supérieure de Physique et de Chimie Industrielles (ESPCI), Paris, F;
2
Universités de Montpellier 1 et 2, Montpellier, F
12:10–12:30
L57
Moment Equations for Chromatography using Superficially Porous Spherical
Particles
Kanji Miyabe
University of Toyama, Toyama, J
47
11:00–12:30
ION CHROMATOGRAPHY, IONIC LIQUIDS
Chair: Nobuo Tanaka
11:00–11:30
KN20
Recent Advances in Ion Chromatography
Paul R. Haddad, Greg W. Dicinoski, Robert A. Shellie, Boon K. Ng,
Emily F. Hilder, Pavel N. Nesterenko, Philip Zakaria, Viktor Drgan
University of Tasmania, Hobart, AUS
11:30–11:50
L58
Integrated Chemical Systems for High Performance Ion Chromatography using
Chelating, Macrocyclic and Dipolar Ligands
Péter Hajós
University of Pannonia, Veszprém, H
11:50–12:10
L59
Silanol Suppression Potency of Alkyl-Imidazolium Ionic Liquids on C18
Stationary Phases
María José Ruiz-Ángel, Juan José Fernández-Navarro,
María Celia García-Álvarez-Coque
Universitat de València, Burjassot, E
12:10–12:30
L60
Novel Chromatographic Systems to Prevent Acts of Terrorism
Greg W. Dicinoski, Joseph P. Hutchinson, Cameron A. Johns, Eadaoin Tyrrell,
Emily F. Hilder, Michael C. Breadmore, Robert A. Shellie, Rosanne M. Guijt,
Pavel N. Nesterenko, Kara-Lea Angoy, Gustavo Blanco Heras, Paul R. Haddad
11:00–12:30
HPLC-MS
Chair: Christian Huber
11:00–11:30
KN21
High Resolution Liquid Chromatography and Fast Acquisition Mass
Spectrometry for Simultaneous Qualitative and Quantitative Analysis
Gérard Hopfgartner, Emmanuel Varesio
48
11:30–11:50
L61
High Performance Liquid Chromatography Coupled to Direct Analysis in Real
Time Mass Spectrometry: A New Hyphenated Method
Christian W. Klampfl1, Susanne Beismann1, Walter Eberherr1,
Wolfgang Buchberger1, Robert Hertsens2
1
Johannes Kepler University, Linz, A;
2
JEOL (Europe) BV, Zaventem, B
11:50–12:10
L62
Liquid Microjunction and Laser Ablation/Liquid Phase Collection Surface
Sampling Coupled with HPLC/Electrospray Ionization-Mass Spectrometry for
Analysis of Drugs and Metabolites in Whole-Body Thin Tissue Sections
Vilmos Kertész1, Olga S. Ovchinnikova1,2, Gary J. Van Berkel1,2
1
Organic and Biological Mass Spectrometry Group, Oak Ridge, TN, USA;
2
12:10–12:30
L63
Method Development for the Selective Isolation of Secreted O-Glycopeptides
Zsuzsanna Darula1, Katalin F. Medzihradszky1,2
1
Biological Research Centre, Szeged, H;
2
Mass Spectrometry Facility, UCSF, San Francisco, CA, USA
12:30–13:30
Lunch
13:30–14:30
VENDOR SEMINARS
13:30–15:30
14:30–15:15
Coffee break
49
15:30–16:15
TUTORIAL LECTURES
Chair: Francesco Dondi
Csaba Horváth Hall
T07
Characterizing Chromatograms by Dimensionality: A Comparison of Estimation
Techniques using a Gallery of Single and Multidimensional Chromatograms
Mark R. Schure
The Dow Chemical Company, Springhouse, PA, USA
Chair: Fabrice Gritti
T08
Supercritical Fluid Chromatography: Past, Present and Future
Pat Sandra1,2
1
Research Institute for Chromatography, Kortrijk, B;
2
Ghent University, Ghent, B
Chair: Imre Klebovich
T09
Overpressured-Layer Chromatography (OPLC) – from the Pressurized
Ultramicro Chamber to BioArena System
Ernő Tyihák1, Emil Mincsovics2, Ágnes M. Móricz1
1
Plant Protection Institute, HAS, Budapest, H;
2
OPLC-NIT Engineering Co. Ltd., Budapest, H
16:15–17:25
FUNDAMENTAL ASPECTS OF SEPARATIONS:
HONOURING GEORGES GUIOCHON
Chair: Pavel Jandera
Csaba Horváth Hall
16:15–16:45
KN22
Reconstruction and Statistical Analysis of Chromatographic Media: From
Metric Properties to Structural Descriptors of Diffusion and Dispersion
Ulrich Tallarek
16:45–17:05
L64
Visualization of Chromatographic Surprises – The Helfferich Paradox Revisited
Torgny Fornstedt
Karlstad University, Karlstad, S
17:05–17:25
L65
Reaction Chromatography: Design and Characterization of New Stationary
Phases for Flow-Chemistry Applications
Alberto Cavazzini, Alessandro Massi, Luisa Pasti, Francesco Dondi
50
16:15–17:25
INDUSTRIAL SEPARATIONS
Chair: Ziad El Rassi
16:15–16:45
KN23
Evaluation of Flash SFC for Pharmaceutical Medicinal Chemistry Purifications
Larry Miller
Amgen, Cambridge, MA, USA
16:45–17:05
L66
Ion Pair Supercritical Fluid Chromatography of Isomeric Protected and
Unprotected Polypeptide Pairs
M. A. Patel1, F. Riley1, J. Wang1, M. Lovdahl, M. Ashraf-Khorassani2,
L. T. Taylor2
1
Pfizer Inc., Groton, CT, USA;
2
Virginia Tech, Blacksburg, VA, USA
17:05–17:25
L67
A Powerful Preparative Technique: Modern Countercurrent Chromatography
Alain Berthod
16:15–17:25
MULTIDIMENSIONAL AND PLANAR
CHROMATOGRAPHY
Chair: Teresa Kowalska
16:15–16:45
KN24
New Developments in the use of Comprehensive LC for the Analysis of Natural
Products
Paola Dugo1,2, Paola Donato1,2, Francesco Cacciola1, Luigi Mondello1,2
1
University of Messina, Messina, I;
2
University Campus Bio-Medico, Rome, I
16:45–17:05
L68
Theory and Modelling of a New Analytical Technique: Comprehensive Online
Multidimensional Fast Fourier Transform Separations
Mark J. E. Trudgett1,2, Georges Guiochon3, R. Andrew Shalliker1,2
1
Australian Centre for Research on Separation Science (ACROSS), Sydney, AUS;
2
Nanoscale Organisation and Dynamics Group, Sydney, AUS;
3
51
17:05–17:25
L69
Silica Based Thin-Layer Chromatography Plates Templated through Carbon
Nanotubes
David Scott Jensen1, Supriya Kanyal1, Andrew Dadson2, Michael Vail2,
Matthew R. Linford1
1
Brigham Young University, Provo, UT, USA;
2
US Synthetic Corporation, Orem, UT, USA
18:00–
52
SYMPOSIUM DINNER
53
Lecture Programme
Thursday, 23 June 2011
9:00–10:30
ADVANCES IN SEPARATION TECHNOLOGY
Chair: Edward S. Yeung
Csaba Horváth Hall
9:00– 9:30
KN25
Novel Monolithic Cryopolymers for Efficient Capillary Chromatography of
Biomolecules
Emily F. Hilder, Dario Arrua, Anna Nordborg
9:30– 9:50
L70
Two-Dimensional LC-MS/MS of Complex Peptide Samples: The Utility of
Porous Graphitic Carbon as the First Dimension Stationary Phase
John R. Griffiths1, Simon Perkins1, Yvonne Connolly1, Lu Zhang1,
Valeria Barattini2, Luisa Pereira2, Anthony Edge2, Harald Ritchie2,
Duncan L. Smith1
1
Paterson Institute for Cancer Research, Manchester, UK;
2
Thermo Fisher Scientific, Cheshire, UK
9:50–10:10
L71
Fast and Efficient Comprehensive Two-Dimensional UHPLC for Separations of
Polymers
Elena Uliyanchenko, Peter Schoenmakers, Sjoerd van der Wal
10:10–10:30
L72
Volume Based HPLC – A Paradigm Change in Liquid Chromatography
Konstantin Choikhet1, Klaus Witt1, Monika Dittmann1, Philip Herzog2,
Herbert Anderer1, Gert Desmet2, Matthias Verstraeten2, Ken Broeckhoven2
1
Agilent Technologies, Waldbronn, D;
2
Free University of Brussels, Brussels, B
54
9:00–10:30
CHIRAL SEPARATIONS
Chair: Danilo Corradini
9:00– 9:30
KN26
New Insights on Separation Mechanism of Enantiomers in Aqueous and
Non-Aqueous Capillary Electrophoresis
Bezhan Chankvetadze
Tbilisi State University, Tbilisi, GE
9:30– 9:50
L73
Mechanism of Enantioseparation on Macrocyclic Antibiotic Phases
Shengli Ma1, Sherry Shen1, Heewon Lee1, Dheleepkumar Krishmamurthy1,
Chris Senanayake1, Nelu Grinberg1, David Bell2
1
Boehringer Ingelheim Pharmaceuticals Inc., Ridgefield, CT, USA;
2
Sigma Aldrich, Bellefonte, PA, USA
9:50–10:10
L74
Simultaneous Enantioselective Analysis of all Proteinogenic Amino Acids in
Mice Lacking Enzymes Metabolizing D-amino Acids
Kenji Hamase1, Kyoko Ueno1, Yurika Miyoshi1, Masashi Mita2, Ryuichi Konno3,
Wolfgang Lindner4
1
Kyushu University, Fukuoka, J; 2Shiseido Co., Ltd., Tokyo, J;
3
International University of Health and Welfare, Tochigi, J;
4
10:10–10:30
L75
Novel Immobilised Polysaccharide-Derived Chiral Stationary Phases to Enhance
Success Rate in the Resolution of Enantiomers
P. Franco, D. Nguyen, T. Zhang
Chiral Technologies Europe, Illkirch, F
9:00–10:30
PROTEOMICS
Chair: Gérard Hopfgartner
9:00– 9:30
KN27
High-Efficiency HPLC – High-Resolution Orbitrap-MS for Top-Down Analysis of
Intact Proteins
Martin Samonig1, Jens H. Mohr1, Remco Swart2, Günter Böhm3,
Christian G. Huber1
1
University of Salzburg, Salzburg, A;
2
Dionex Benelux B.V., Amsterdam, NL;
3
ThermoFisher Scientific, Reinach, CH
55
9:30– 9:50
L76
Enrichment-Enabled “Bottom-Up” Exploration of the Nitroproteome by Liquid
Chromatography–Tandem Mass Spectrometry
Laszlo Prokai, Jia Guo, Katalin Prokai-Tatrai
University of North Texas Health Science Center, Fort Worth, TX, USA
9:50–10:10
L77
Multidimensional Lipid Analysis using Novel Workflows Based on High
Resolution Mass Spectrometry or High Chromatographic Peak Capacity
Markus Himmelsbach, Emmanuel Varesio, Gérard Hopfgartner
10:10–10:30
L78
Analytical Variability Reduction in Complex Sample Analysis using One and Two
Dimensional Liquid Chromatography Mass Spectrometry
Robert E. Murphy, Ryan Preston
CovX, Pfizer’s Biotherapeutics Research and Development, San Diego, CA, USA
EXHIBITION
10:30–11:00
Coffee Break /
11:00–12:30
MULTIDIMENSIONAL SEPARATIONS
Chair: Pat Sandra
Csaba Horváth Hall
11:00–11:30
KN28
Optimization of Selectivity, Peak Capacity and Separation Time in
Two-Dimensional HPLC by Matching Separation Systems and Adjusting
Gradient Conditions in the Two Dimensions
Pavel Jandera, Tomáš Hájek, Petr Cesla
11:30–11:50
L79
Using Multidimensional Liquid Chromatography for Solving Difficult Separation
Problems in the Life Sciences and Pharmaceutical Analysis
Steven A. Cohen, Peter Claise, Sean McCarthy, Catalin Doneanu
56
11:50–12:10
L80
Novel Thermal Modulation for Multi-Dimensional Liquid Chromatography
Separations using Low-Thermal-Mass LC
Matthias Verstraeten1, Matthias Pursch2, Patric Eckerle2, Jim Luong3,
Gert Desmet1
1
Vrije Universiteit Brussel, Elsene, B; 2Dow Deutschland GmbH, Rheinmunster, D;
3
Dow Canada, Fort Saskatchewan, CDN
12:10–12:30
L81
Sample Dilution and Eluent Compatibility in Two-Dimensional Liquid
Chromatography
Krisztián Horváth1, Jacob Fairchild2, Péter Hajós1, Georges Guiochon3
1
University of Pannonia, Veszprém, H; 2Waters Corporation, Milford, MA, USA;
3
11:00–12:30
STATIONARY PHASES
Chair: Frantisek Svec
11:00–11:30
KN29
Understanding Column Bed Heterogeneity in the Quest for Improved
Separation Efficiency
H. Ritchie1, M. Camenzuli2, G. R. Dennis2, R. A. Shalliker2
1
Thermo Fisher Scientific, Runcorn, UK;
2
University of Western Sydney, Sydney, AUS
11:30–11:50
L82
Second Generation of Porous Polymer Monoliths: From High Surface Area to
Endless Number of Applications
Jiri Urban1,2, Pavel Jandera1, Frantisek Svec2
1
University of Pardubice, Pardubice, CZ;
2
University of California, Berkeley, CA, USA
11:50–12:10
L83
A Deeper Understanding of a Complex Adsorption Behavior in a Common
Chiral, Separation System
Martin Enmark, Jörgen Samuelsson, Torgny Fornstedt
12:10–12:30
L84
About the Performance of 2nd Generation Monolithic HPLC Columns
K. Cabrera, P. Knoell, G. Jung, A. Piper, K. Kreher, E. Machtejevas
Merck KGaA, Darmstadt, D
57
11:00–12:30
DETECTION IN MICROFLUIDICS
Chair: Nelu Grinberg
11:00–11:30
KN30
On-Column Surface-Enhanced Raman Spectrometry Detection in Capillary
Separations
Jan Prikryl, Karel Kleparnik, František Foret
Institute of Analytical Chemistry of the ASCR, Brno, CZ
11:30–11:50
L85
Microfluidic Electrophoresis with LIF and LED Fluorescence Detection for
Biomedical Diagnostics and On-Site Analysis: How Flexible Can a Fixed-Design
Chip-CE System Be?
Petr Smejkal1,2,3, Nantana Nuchtachvorn4, Yi Sing Gee1, Yi Nai1,
Michael C. Breadmore1, Shane Powell5, František Foret2, Rosanne M. Guijt1,
Leena Suntornsuk4, Fritz Bek6, Mirek Macka1
1
University of Tasmania, Hobart, AUS;
2
Institute of Analytical Chemistry of the ASCR, Brno, CZ;
3
University of Pardubice, Pardubice, CZ;
4
Mahidol University, Bangkok, T;
5
6
Agilent Technologies, Waldbronn, D
11:50–12:10
L86
Native Time-Resolved Fluorescence Detection – a Powerful Tool in Chip-Based
Total Analysis Systems
Reinhild Beyreiss, Stefan Ohla, Detlev Belder
University of Leipzig, Leipzig, D
12:10–12:30
L87
Advancements in the HDC Separation of Nanoparticles in Ordered Micro-Pillar
Array Columns
Jeff Op De Beeck1, Wim Demalsche1,2, Gert Desmet1
1
2
Imec, Leuven, B
12:30–13:30
Lunch
13:30–14:30
VENDOR SEMINARS
58
13:30–15:00
14:30–15:00
Coffee break
15:00–16:30
PLENARY LECTURES
Chair: Wolfgang Lindner
15:00
Csaba Horváth Hall
Martin Gold Medal Award Ceremony
15:00–15:30
PL06
High-Performance Separations of Macromolecules
Peter Schoenmakers
15:30–16:00
PL07
Imaging Flow and Chromatographic Separation in Monolithic Capillaries using
Remote NMR Detection
Frantisek Svec, Thomas Z. Teisseyre, Jiri Urban, Nicholas W. Halpern-Manners,
Stuart D. Chambers, Vikram S. Bajaj, Alexander Pines
Lawrence Berkeley National Laboratory, Berkeley and University of California at
Berkeley, Berkeley, CA, USA
16:00–16:30
PL08
LC-MS Based Metabolomics for Disease Biomarker Discovery and
Confirmation
Guowang Xu, Xinjie Zhao, Peiyuan Yin, Qiang Huang, Lina Zhou, Xin Lu
Dalian Institute of Chemical Physics, Dalian, PRC
16:30–17:00
POSTER AWARDS,
CSABA HORVÁTH YOUNG SCIENTIST AWARD,
INVITATIONS, AND CLOSING CEREMONY
17:00–18:00
FAREWELL RECEPTION
59
60
Final List of Posters
Advances in Separation Techniques
P1-G-001-MO
A Critical Evaluation of Sub-2 μm Particles for Packed Column Supercritical Fluid
Chromatography
Michael Jones1,2, Norman Smith1, Cristina Legido-Quigley1, Andrew Aubin2
1
King’s College London, UK;
2
P1-G-002-TU
A Highly Automated Multi-Pump, Multi-Detector, Super-Critical Fluid Chromatography
(SFC) System for Purification in Drug Discovery
Xu Zhang, Qing Ping Han, Mark J. Hayward
Lundbeck Research, Paramus, NJ, USA
P1-G-003-MO
Applications of a New HILIC Stationary Phase
Ken Butchart, Mark Woodruff
Fortis Technologies Ltd, Neston, Cheshire, UK
P1-G-004-TU
Basic Study of Macroporous Spongy Monolith on HPLC Separation and its Application
for Effective Concentration of PAHs
Takuya Kubo1, Tetsuya Tanigawa1,2, Keita Kato1, Yoshiyuki Watabe3, Yoshitomo Tanaka4,
Ken Hosoya1
1
Tohoku University, Sendai, J; 2Chemco Scientific Co., Ltd., Osaka, J;
3
Shimadzu Corporation, Kyoto, J; 4Glory Industry Co., Ltd., Osaka, J
P1-G-005-MO
Design of Linear Peptidic Affinity Ligands Based on Single-Chain Antibody Fragment
Sequence Information
Katrin Kurz, Frank Hilbrig, Ruth Freitag
University of Bayreuth, Bayreuth, D
P1-G-006-TU
Development of a Comprehensive Two-Dimensional Liquid Chromatography / Mass
Spectrometry System and its Applications in Analyzing Triglycerides
Qin Yang, Xiaoli Hou, Xianzhe Shi, Yuanhong Shan, Guowang Xu
61
P1-G-007-MO
Electrospun Nanofibers as Sorbent Material for Miniaturized Solid Phase Extraction
Devices
Nelson Torto, Samuel Chigome
Rhodes University, Grahamstown, ZA
P1-G-008-TU
Evaluation of Diol and Polyethylene Glycol Columns for the Analysis of Ionisable
Solutes by Different Chromatographic Modes
Alberto dos Santos Pereira1, Nobukazu Higashi2, Kazuhisa Mitsui2, Hirooki Kanda3,
Frank David1, Pat Sandra1
1
2
Japan Tobacco Inc., Yokohama, J;
3
Gerstel K.K. Tokyo, J
P1-G-009-MO
Evaluation of New UHPLC Mixed-Mode Hybrid Stationary Phases in Pharmaceutical
Analysis
Lucie Nováková, Hana Vlčkova
Charles University, Hradec Králové, CZ
P1-G-010-TU
Evaluation of UHPLC and Core-Shell Particles
P1-G-011-MO
Fast Method Development of Rooibos Tea Phenolics using a Variable Column Length
Strategy
Deirdre Cabooter1,2, Andre de Villiers2, Martha Kallili2, Gert Desmet1
1
2
P1-G-012-TU
Injection Sequence for Optimizing Performance in UHPLC Separations
Jason A. Anspach, A. Carl Sanchez, Tivadar Farkas
Phenomenex, Torrance, CA, USA
P1-G-013-MO
Ion Chromatography – Analysis of Aqueous Solutions of Amines
Maciej Chrubasik, Ewa Micek, Justyna Tarnowska
Institute for Chemical Processing of Coal, Zabrze, PL
62
P1-G-014-TU
Maximizing Peak Capacity with UHPLC
Siji Joseph1, Edgar Naegele2, Syed Lateef1, Christian Gotenfels2
1
Agilent Technologies India Pvt Ltd, Bangalore, IND; 2Agilent Technologies, Waldbronn, D
P1-G-015-MO
Multidimensional HPLC+GC Coupling System for Automated On-Line Clean-Up,
Derivatization and Analysis of Complex Samples
Josep Ma Gibert1, Nieves Sarrión1, Ariadna Galve1, Roger Gibert1, David Alonso1,
Jesús Villén2, José Manuel Cortés2, Lorena Colmenero Fernández1
1
KONIK-Tech S.A., Barcelona, E; 2Universidad de Castilla-La Mancha, Albacete, E
P1-G-016-TU
Multidimensional Orthogonal High Performance Liquid Chromatography with Backward
Elution (Eluent Back-Flush) as a New Solution for General Elution Problems
Marian Kamiński, Grzegorz Boczkaj, Maciej Trznadel, Mariusz Jaszczołt,
Sebastian Zalewski
Gdansk University of Technology, Gdansk, PL
P1-G-017-MO
Optimized Supercritical Fluid Chromatography (SFC) Separation of Organic Light
Emitting Diode (OLED) Materials
Dennis Lorenzen, Axel Thomasberger, Bernhard Schubach
P1-G-018-TU
Robustness Criterion vs. Experimental Design in Robustness Testing of RP-HPLC
Method for Ramipril and its Impurities Determination
Biljana Jančić-Stojanović, Tijana Rakić, Sava Vemić, Nad– a Kostić, Ana Vemić,
And– elija Malenović
University of Belgrade, Belgrade, SRB
P1-G-019-MO
Search of Suitable Two-Dimensional Chromatographic Systems for the Separation of
Biomass Compounds
David Angot1, Agnes Fonverne1, Amelie Dechenaux2, Sabine Heinisch2
1
IFP Energies Nouvelles – Lyon, Solaize, F; 2Université de Lyon, Villeurbanne Cedex, F
P1-G-020-TU
Sensitive Analysis of Trace Metal Ions in a Saline Sample Combining Online Dye
Complexation and Transient Isotachophoresis
Kihwan Choi, Asif Riaz, Sunyoung Cho, Jihye Kim, Doo Soo Chung
Seoul National University, Seoul, ROK
63
P1-G-021-MO
Separation Modes in Ice Chromatography
Tetsuo Okada, Yuiko Tasaki, Taiki Shamoto, Yuji Miyazaki, Satsuki Takahashi
Tokyo Institute of Technology, Tokyo, J
P1-G-022-TU
Separation of Monosaccharides by Ionic Liquid-Immobilized Microporous Polymers
Minglei Tian, Kyung Ho Row
Inha University, Incheon, ROK
P1-G-023-MO
Simple Separation and Detection Techniques for the Analysis of Carbohydrates
Ian N. Acworth, Bruce Bailey, Marc Plante, Christopher Crafts
ESA – A Dionex Company, Chelmsford, MA, USA
P1-G-024-TU
Simultaneous Analysis of Metal-Chelate Complexes and their Ligands using High
Performance Ion Chromatography
Renáta Tófalvi, Annamária Sepsey, Krisztián Horváth, Péter Hajós
P1-G-025-MO
Size Exclusion Chromatography of Silica-Based Nanoparticles
Marcell Pálmai1, Tibor Kremmer1, Lívia Nagyné Naszályi1, Judith Mihály1,
Imola Szigyárto1, Péter Németh2
1,2
P1-G-026-TU
Study of Axial Dispersion with Peak Parking in Different Columns
Nándor Lambert, Attila Felinger
P1-G-027-MO
Switching from Constant Flow Rate to Constant Pressure Elution Mode
Matthias Verstraeten1, Ken Broeckhoven1, Frederic Lynen2, Konstantin Choikhet3,
Monika Dittmann3, Klaus Witt3, Klaus Landt3, Pat Sandra2,4, Gert Desmet1
1
Vrije Universiteit Brussel, Elsene, B;
2
Pfizer Analytical Research Centre (PARC), Gent, B;
3
Agilent Technologies, Waldbronn, D;
4
Research Institute for Chromatography (RIC), Kortrijk, B
64
P1-G-028-TU
The HPLC Study on Spontaneous Peptidization of Phenylglycine, Phenylalanine, and
Phenylglycine – Phenylalanine Systems
Mieczysław Sajewicz, Monika Gontarska, Teresa Kowalska
Silesian University, Katowice, PL
P1-G-029-MO
The Retention Behaviour of Acidic Polar Compounds on Zirconia-Based Stationary
Phases
Radim Kučera, Petra Kovařikova, Michal Klivický, Jiří Klimeš
Charles University in Prague, Hradec Králové, CZ
P1-G-030-TU
TLC / HPTLC / MS / LT-ELSD Coupling: New Development and Optimization
François Bretin1, Francis Maquin1, Pierre Bernard-Savary2, Eric Verette3,
Henry Gangloff3, Véronique de Nailly4
1
SANOFI-AVENTIS, Research Center, Vitry sur Seine, F; 2CHROMACIM-CAMAG, Pommiers
la Placette, F; 3SEDERE SAS, Alfortville Cedex, F 4BCP INSTRUMENTS, Irigny, F
P1-G-031-MO
Towards the Comprehensive Two-Dimensional LCxMEKC Separations using On-Line
Preconcentration and Programmed Separation Conditions
Petr Česla, Jan Fischer, Pavel Jandera
Chip Based Separations, Microfluidics, Microscale Detection Systems
P1-G-032-TU
A Novel Economic Approach towards Free-Flow-Electrophoresis Chips
Stefan Jezierski, Leonid Gitlin, Detlev Belder
P1-G-033-MO
A Novel Microfluidic-Based Chip Device for Rapid and Automated Characterization of
N-linked Glycans from Monoclonal Antibodies
Stephan Buckenmaier, Michael Frank, Tom van de Goor, Lukas Trojer
P1-G-034-TU
A Novel NMR Chip for Chemical Reaction Analysis in Extended-Nano Space
Shota Yoshioka, Kazuma Mawatari, Takehiko Kitamori
The University of Tokyo, J
65
P1-G-035-MO
Application of the HPLC-Chip LC-MS Technology for Global and Targeted Investigations
of Proteomes
Hartmut Schlüter1, Steffen Ehlert2, Ullrich Tallarek2, Verena Richter1, Diana Hildebrand1,
Maria Trusch1
1
University Medicine Hamburg-Eppendorf, Hamburg, D;
2
Philipps University, Marburg, D
P1-G-036-TU
Bead-Based Liquid Chromatography in Microfluidic Devices
Sebastian Thurmann, Detlev Belder
P1-G-037-MO
Comparison of Glycan Distribution in Therapeutic Monoclonal Antibodies by LC-MS
using mAb-Glyco-Chip and CE-LIF
Shiaw-Lin Wu1, Yi Wang1, Sam Tep2, Zoran Sosic2, Yelena Lyubarskaya2, Ning Tang3,
William S. Hancock1, Barry Karger1
1
Barnett Institute, Boston, MA, USA;
2
Biogen Idec Inc., Cambridge, MA, USA;
3
Agilent Technologies, Santa Clara, CA, USA
P1-G-038-TU
Determination of Low-Molecular-Mass Amines using Microchip Electrophoresis and
Contactless Conductivity Detector
Ahmed O. Alnajjar
King Faisal University, Hofuf, SA
P1-G-039-MO
Development and Prevalidation of a Nano-LC-Chip-MS/MS Method for High Sensitivity
Hepcidin Quantitation
Virginie Houbart, Frederic Lecomte, Gaël Cobraiville, Anne-Catherine Servais,
Philippe Hubert, Marianne Fillet
University of Liège, Liège, B
P1-G-040-TU
Development of a Micro-Pillar Array Separation Device for Commercially Available
Micro-HPLC Systems
Hiroshi Kobayashi, Hiroo Wada
Shinwa Chemical Industries Ltd., Kyoto, J
66
P1-G-041-MO
Development of Laplace Pressure Valve for Chromatography System in
Extended-Nano Space
Shogo Kubota, Kazuma Mawatari, Xu Yan, Takehiko Kitamori
The University of Tokyo, Tokyo J
P1-G-042-TU
Development of Polymer-Modification Method for Novel Separation Device on
Extended-Nano Space
Junpei Katagiri, Tatsuhiro Yamamoto, Kazuma Mawatari, Takehiko Kitamori
The University of Tokyo, Tokyo, J
P1-G-043-MO
Electrochromatographic Properties of Monoliths Prepared by Radiation-Induced Free
Radical Polymerization for Lab-on-a-Chip Applications
Claudia Ernst, Detlev Belder
P1-G-044-TU
Evaluation of Microfluidic Chip Chromatography-Mass Spectrometry of N- and
O-Glycans using Porous Graphitised Carbon, Hydrophilic Interaction Media and Online
Anion Exchange Fractionation
Oscar G. Potter1, Rudolf Grimm2, Pauline M Rudd1
1
National Institute for Bioprocessing Research and Training, Dublin, IRL;
2
P1-G-045-MO
Evolution of Nano-Scale Chemistries for Information-Rich UPLC-Based MS Analyses
Martin Gilar, Jim Murphy, Geoff Gerhardt
P1-G-046-TU
From Ordered Pillars to Random Packings: Effect of Confinement on Transcolumn
Velocity Bias and Separation Efficiency
Anton Daneyko, Siarhei Khirevich, Alexandra Höltzel, Ulrich Tallarek
P1-G-047-MO
High Sensitivity Characterization of Propanolol and Associated Metabolites Utilizing
Intergrated Microfluidic LC/MS/MS
Paul D. Rainville1,2, Michael Tomany1, Norman W. Smith2, David Cowan2,
Robert S. Plumb1,2
1
Waters Corporation, Milford, MA, USA; 2Kings College London, London, UK
67
P1-G-048-TU
HPLC on a Compact Disc: Fabrication and Feasibility
Phillip Morgan1, Dominic Banks2, Robert Flanagan1, Peter Myers3
1
King’s College Hospital, London, UK;
2,3
University of Liverpool, Liverpool, UK
P1-G-049-MO
Integration of Ground Aerogel Particles into PDMS Microchip as a New
Chromatographic Stationary Phase
Andrea Nagy, Attila Gáspár, István Lázár
University of Debrecen, Debrecen, H
P1-G-050-TU
Method of Development for Toner-Based Microchips
Una Crowley1, Mark Naussbaum1,2, Jeremy D. Glennon1
1
University College Cork, Cork, IRL;
2
Hillsdale College, Hillsdale, MI, USA
P1-G-051-MO
Microfluidic Liquid Junction System for CE/MS
Jakub Grym, František Foret
Institute of Analytical Chemistry ASCR v.v.i., Brno, CZ
P1-G-052-TU
Micro-Scaled High Throughput Screening of Digestion Conditions for Insulin Analog
Precursor
Lidia Gurba, Michał Odrowa˛ż-Sypniewski, Anna Bierczyńska-Krzysik, Grażyna Płucienniczak,
Bożena Tejchman-Małecka, Dorota Stadnik
Institute of Biotechnology and Antibiotics, Warsaw, PL
P1-G-053-MO
On-Line Analysis of Cocaine and its Metabolite from Biological Fluids using a
Chip-SPE-LC-MS System
Valérie Thibert, Florence Chapuis-Hugon, Valérie Pichon
ESPCI ParisTech, Paris, F
P1-G-054-TU
Poly(ethylene Glycol) Coated Microfluidic Devices for Microchip Electrophoresis
Marcel Schulze, Detlev Belder
68
P1-G-056-TU
The Challenge of Hyphenating a Continuous Flow System with Capillary Liquid
Chromatography for Detection of Enzymatic Regulation in House Dust
Katja Oeste1,2, Paul Ermisch1, Christoph Portner1, Thorsten Teutenberg1,
Thomas Letzel2
1
Institut für Energie- und Umwelttechnik e. V., Duisburg, D;
2
Technische Universität München, Freising-Weihenstephan, D
P1-G-057-MO
UHPLC-MS with High Pressure Microfluidic Metal Chips
Faizy Ahmed1, Greg Staples2, Reid Brennen1, Karen Seaward2, Jon James2,
Hongfeng Yin1, Lynette Martinez1, Liz Carr1, Sue Post1, Qing Bai1, John Mannion1,
Kevin Killeen1
1
Agilent Technologies, Santa Clara, CA, USA;
2
Agilent Technologies, Santa Rosa, CA, USA
P1-G-058-TU
Using 200 μm ID cHiPLC Columns for Increased Sample Throughput in Peptide
Quantitation
Remco van Soest, Nicole Hebert, Erika Lin
Eksigent, division of AB Sciex, Dublin, CA, USA
Chiral Separations
P1-G-059-MO
Analysis of Chiral Amino Acids in Cerebrospinal Fluid Samples Linked to Different
Stages of Alzheimer Disease
Shorena Samakashvili1, Clara Ibáñez2, Carolina Simó2, Francisco J. Gil-Bea3,
Bengt Winblad3, Angel Cedazo-Mínguez3, Alejandro Cifuentes2
1
Tbilisi State University, Tbilisi, GE;
2
Institute of Food Science Research (CSIC), Madrid, E;
3
Karolinska Institute, Stockholm, S
P1-G-060-TU
Capillary Electrophoretic Enantioseparation of Aminonaphthol Analogs
I. Ilisz1, G. Fodor1, Z. Pataj1, I. Szatmári2, F. Fülöp2, L. Szente3, A. Péter1
1,2
University of Szeged, Szeged, H;
3
CycloLab R&D Ltd, Budapest, H
69
P1-G-061-MO
Chiral HPLC Determination of Nabumetone and its Phase I Metabolites In
Vitro. Application to Study of Stereospecificity of Carbonyl Reductases Involved in
Nabumetone Biotransformation
Milan Nobilis1,2, Veronika Holmanová2, Barbora Szotáková2, Chamseddin Chamseddin3,
Thomas Jira3, Eliška Matoušová2, Jiří Kuneš2, Milan Pour2
1
Joint Research Center of PRO. MED. CS Praha a.s.and Academy of Sciences of the
Czech Republic, Hradec Králové, CZ;
2
Charles University, Hradec Králové, CZ;
3
Ernst-Moritz-Arndt-University, Greifswald, D
P1-G-062-TU
Chiral HPLC-FD Method Validation for Determination of Several Beta-Blockers and
Fluoxetine in Biodegradation Assays
Ana Rita Lado Ribeiro1,2, Paula Maria Lima Castro2, Carlos Magalhães Afonso3,
Maria Elizabeth Tiritan1,3
1
Centro de Investigacao em Ciencias da Saude (CICS), Gandra, P;
2
Universidade Catolica Portuguesa, Porto, P; 3Universidade do Porto, Porto, P
P1-G-063-MO
Chiral Separation of Binaphthyl Catalysts using New HPLC Chiral Stationary Phases
Based on Derivatized Cyclofructans
Lucie Janečková1, Květa Kalíková2, Jiři Vozka2, Zuzana Bosáková1, Daniel W. Armstrong3,
Eva Tesařová2
1,2
Charles University in Prague, Prague, CZ;
3
University of Texas at Arlington, Arlington, TX, USA
P1-G-064-TU
Chiral Separation of Citalopram by Capillary Electrophoresis
Xiaolan Deng, Erwin Adams, Ann Van Schepdael
Katholieke Universiteit Leuven, Leuven, B
P1-G-065-MO
Chiral Separation of Clinically Important Compounds using CE – Determination of the
Most Effective Chiral Selector
Christoforos A. Hadjistasi, Constantina P. Kapnissi-Christodoulou
University of Cyprus, Nicosia, CY
P1-G-066-TU
Chiral Separation of Huperzine A using CE – Method Validation and Application in
Pharmaceutical Formulations
Despina Tsioupi, Constantina P. Kapnissi-Christodoulou
70
P1-G-067-MO
Chiral Separations of Un-Derivatized Peptides on Chiral Zwitterionic Stationary Phases
Stefanie Wernisch, Reinhard Pell, Wolfgang Lindner
P1-G-068-TU
Chiral Stationary Phases Based on Derivatized Cyclofructan for Chiral HPLC
Separation
Květa Kalíková1, Lucie Janečková2, Radim Geryk2, Daniel W. Armstrong3, Eva Tesařová1
1,2
Charles University in Prague, Prague, CZ;
3
P1-G-069-MO
Combination of Capillary Electrophoresis, Molecular Modelling and Nuclear Magnetic
Resonance to Study the Interaction Mechanisms between Single-Isomer Anionic CD
Derivatives and Basic Drug Enantiomers in a Methanolic Background Electrolyte
Anne-Catherine Servais, Anne Rousseau, Georges Dive, Michel Frederich,
Jacques Crommen, Marianne Fillet
P1-G-070-TU
Comparison of the Charge State Distribution in Commercially Available Sulfated
Cyclodextrins used as Chiral Resolving Agents in CE
Roy Estrada1,2, Gyula Vigh1
1
Texas A&M University, College Station, TX, USA;
2
TX Molecular LLP, Deer Park, TX, USA
P1-G-071-MO
Cyclodextrin Based Cation-Exchanger Chiral Columns
Julianna Szemán1, Júlia Visy2, Éva Jámbor3, Gábor Fodor4, Róbert Ohmacht3,
Gábor Varga5
1
CycloLab R&D Ltd, Budapest, H; 2Chemical Research Center, HAS, Budapest, H;
3
University of Pécs, Pécs, H; 4University of Szeged, Szeged, H;
5
ChiroQuest Ltd, Budapest, H
P1-G-072-TU
Direct Chiral Determination of Salbutamol, Salmeterol and Atenolol by Two
Dimensional (LC-LC) High Performance Liquid Chromatography
Yun Yang1,2, Noelia Rosales-Conrado1, Vanesa Guillén-Casla1,
María Eugenia de León González1, Luis Vicente Pérez-Arribas1, Luis María Polo-Díez1
1
Complutense University of Madrid, Madrid, E;
2
Northwest University, Xi’an, PRC
71
P1-G-074-TU
Enantioselective 2D-HPLC Determination of N-Methylaspartic Acid and
N-Methylglutamic Acid in Mammals and Bivalves
Reiko Koga1, Yurika Miyoshi1, Kyoko Ueno1, Masashi Mita2, Wolfgang Lindner3,
Kenji Hamase1
1
Kyushu University, Fukuoka, J; 2Shiseido Co., Ltd., Tokyo, J;
3
P1-G-075-MO
Enantioseparation of Amino Acids by Molecularly Imprinted Electrochromatography
with Electrochemical Detection
Fengjun Shang1, John, H. T. Loung2, Mila Pravda1, Jeremy D. Glennon1
1
2
National Research Council, Canada, Montreal, Quebec, CDN
P1-G-076-TU
High Performance Chiral Columns for Efficient Enantioseparation
Yong Wang, Feng Ai, Siu-Choon Ng, Timothy T. Y. Tan
Nanyang Technological University, Singapore, SGP
P1-G-077-MO
High Throughput Chiral Screening: A Comparison between LC and SFC
Melissa Dunkle1, Gerd Vanhoenacker1, Alberto dos Santos Pereira1, William Farrell2,
Frank David1, Pat Sandra1
1
Research Institute for Chromatography, Kortrijk, B; 2Pfizer Global R&D, La Jolla, CA, USA
P1-G-078-TU
Highly Sensitive Chiral Analysis in Microscale Electrophoresis using Large-Volume
Sample Stacking with Electroosmotic Flow Pump
Takayuki Kawai, Jun Ito, Kenji Sueyoshi, Fumihiko Kitagawa, Koji Otsuka
P1-G-079-MO
High-Performance Liquid Chromatographic Enantioseparation of Isoxazoline-Fused
Cispentacin Derivatives on Chiral Stationary Phases
László Sipos1, Melinda Nonn1, Ferenc Fülöp1, Daniel W. Armstrong2, Antal Péter1
1
University of Szeged, Szeged, H; 2University of Texas at Arlington, Arlington, TX, USA
P1-G-080-TU
HPLC Enantioseparation and a Temperature-Induced Inversion of the Elution Sequence
of 1-(Phenylethylamino)- or 1-(Naphthylethylamino)methyl-2-Naphthol Analogs
Anita Aranyi, István Ilisz, Zoltán Pataj, István Szatmári, Ferenc Fülöp, Antal Péter
University of Szeged, Szeged, H
72
P1-G-081-MO
HPLC Enantioseparation and Chiral Recognition Mechanism of Novel Xanthone
Derivatives on Macrocyclic Antibiotic Chiral Stationary Phases
Carla Fernandes1,2, Maria Elizabeth Tiritan1,3, Quezia Cass4, Miguel Fernandes5,
Madalena Pinto1,2
1,2
Universidade do Porto, Porto, P;
3
Instituto Superior de Ciencias da Saude-Norte, Gandra, P;
4
Universidade Federal de São Carlos, SP, BR;
5
Universidade da Madeira, Madeira, P
P1-G-082-TU
Hydroxyethylcellulose as a Dynamic Coating Agent in Chiral Capillary Electrophoresis
Tímea Czipó-Takács, Mónika Babják, Mária Gazdag
Gedeon Richter Plc., Budapest, H
P1-G-083-MO
LC Method for the Enantiomeric Purity Determination of S-amlodipine with Special
Emphasis on Reversal of Enantiomer Elution Order using Chlorinated Cellulose-Based
Chiral Stationary Phases and Polar Non-Aqueous Mobile Phases
Katina S.S. Dossou1, Patrick A. Edorh2, Patrice Chiap3, Bezhan Chankvetadze4,
Anne-Catherine Servais1, Marianne Fillet1, Jacques Crommen1
1
University of Liège, Liège, B; 2University of Abomey-Calavi, Cotonou, DY;
3
University Hospital of Liège, Liège, B; 4Tbilisi State University, Tbilisi, GE
P1-G-084-TU
Research on the Metabolism of 4-(Methylnitrosamino)-1-(3-Pyridyl)-1-Butanone to the
Enantiomers of 4-(Methylnitrosamino)-1-(3-Pyridyl)-1-Butanol In Vitro in Human
Bronchial Epithelial Cells using Chiral Capillary Electrophoresis
Youyou Yang1, Cong Yu1, Meng Zhou2, Ning Li2, Jie Liao2, Yu Bai1, Huwei Liu1
1
Peking University, Beijing, PRC; 2General Hospital of Chinese PLA, Beijing, PRC
P1-G-085-MO
Separation of Phenotropil on Polysaccharide Based Chiral Stationary Phases
Helena Kažoka1, Oksana Rotkaja1,2, Grigorij Veinberg1, Maksim Vorona1, Anton Lebedev1
1
Latvian Institute of Organic Synthesis, Rı̄ga, LT; 2Latvian University, Rı̄ga, LT
P1-G-086-TU
Simultaneous Discrimination of Jasmonic Acid Stereoisomers in Wounded Tobacco
Leaves by LC-QTOF-MS
Yehua Han, Yu Bai, Yuan Liang, Meiping Zhao, Huwei Liu
Peking University, Beijing, PRC
73
P1-G-087-MO
Simultaneous Enantioselective 2D-HPLC Analysis of Neuro-Active Amino Acids in
Mouse Central Nervous System using Various Pirkle-Type Chiral Stationary Phases
Yurika Miyoshi1, Kyoko Ueno1, Jumpei Sasabe2, Masashi Mita3, Sadakazu Aiso2,
Kenji Hamase1
1
Kyushu University, Fukuoka, J;
2
Keio University School of Medicine, Tokyo, J;
3
Shiseido Co., Ltd., Tokyo, J
P1-G-088-TU
Stereochemical Characterization of Fluorinated 2-Arylpropionic Acids by
Enantioselective HPLC Analysis and ECD Detection
Carlo Bertucci1, Marco Pistolozzi1, Daniele Tedesco1, Riccardo Zanasi2,
Renzo Ruzziconi3, Anna Maria Di Pietra1
1
University of Bologna, I; 2University of Salerno, I;
3
University of Perugia, I
P1-G-089-MO
Study of Tert-Butyl Calix[n]arene Derivatives and Molecularly Imprinted Polymers in
the Chiral Separation of Oral Anticoagulants and β-Blockers
Ioana Daria Tiuca, Bogdan Cezar Iacob, Ede Bodoki, Radu Oprean
“Iuliu Haţieganu” University of Medicine and Pharmacy, Cluj-Napoca, RO
P1-G-090-TU
The Application of a Newly Developed Isopropyl Carbamate-Cyclofructane6-Based
(IP-CF6) Chiral Stationary Phase for HPLC Enantioseparation of Betti Base Analogs
Zoltán Pataj1, István Ilisz1, István Szatmári1, Ferenc Fülöp1, Daniel W. Armstrong2,
Antal Péter1
1
2
P1-G-091-MO
Use of Chiral Ionic Liquids as Additives in Capillary Electrophoresis
Ioannis Stavrou, Constantina P. Kapnissi-Christodoulou
Clinical, Forensic, and Toxicological Analysis
P1-G-092-TU
A Novel Non-Card Based Format for Dried Blood Spots Analysis
Michel Wagner, Emmanuel Varesio, Gérard Hopfgartner
74
P1-G-093-MO
A Rapid Method for the Detection of Metabolite of Sulfur Mustard
1,1’-Sulfonylbis[2-S-(N-Acetylcysteinyl)Ethane] in Biofluids via LC-MS/MS
Igor Rodin1, Arkady Braun1, Oleg Shpigun1, Irina Ananieva1, Igor Rybalchenko2
1
Lomonosov Moscow State University, Moscow, RUS; 2“Lumex Ltd.”, Moscow, RUS
P1-G-094-TU
Analysis of 1α
α,25-Dihydroxyvitamin D3 (Calcitriol) in a Biological Fluid using
LC-MS/MS
Joanna Denbigh, Tony Edge, Joanne Gartland, Tim Liddicoat, Kim Phipps
ThermoFisher Scientific, Runcorn, Cheshire, UK
P1-G-095-MO
Analysis of 25-Hydroxy Vitamin D2 and D3 in Human Serum using UHPLC/SQ MS
with Field-Free APCI Ion Source
Avinash Dalmia1, Sean Daugherty2, Daniel Pentek1
1
PerkinElmer, Shelton, CT, USA; 2PerkinElmer, Beaconsfield, UK
P1-G-097-MO
Analysis of Triazophos Residue (Pesticide) in Tomato using High Performance Liquid
Chromatography
Chandra Mohineesh, Anupuma Raina, Jaya Raj, T.D. Dogra
A.I.I.M.S., New Delhi, IND
P1-G-098-TU
CE-LIF Assays Based on Boronic Acid Functionalized Dyes for Microbe Surface
Glycoprotein Targets
Christa L. Colyer1, Shingo Saito1,2, Tara L. Massie1, Xiuli Lin1, Takeshi Maeda3,
Hiroyuki Nakazumi3
1
Wake Forest University, Winston-Salem, NC, USA; 2Saitama University, Saitama, J;
3
Osaka Prefecture University, Osaka, J
P1-G-099-MO
Comparison of Different Commercial Sorbents for the In-Line Solid Phase Extraction in
Capillary Electrophoresis Determination of Barbiturate Drugs in Biological Samples
Igor Botello, Francesc Borrull, Marta Calull, Carme Aguilar
Rovira i Virgili University, Tarragona, E
P1-G-100-TU
Confirmatory Quanitation of Benzodiazepines in Post-Mortem Matrices using
HPLC/MS with Online Cleanup
Guifeng Jiang, Terry Zhang, Kathryn Preston
Thermo Fisher Scientific, San Jose, CA, USA
75
P1-G-101-MO
Determination of Antipshycotic Drugs in Brain Tissue by LC-ESI-MS-MS: Screening and
Quantitation of Samples of Forensic Interest
M. Carmen Sampedro, M. Aranzazu Goicolea, Ramón J. Barrio
University of the Basque Country, Vitoria-Gasteiz, E
P1-G-102-TU
Determination of Isomeric Synthetic Cannabinoid Metabolites in Hydrolyzed Urine by
LC/MS/MS
Ty Kahler1, Amanda Rigdon1, Paul Kennedy2, Rick Lake1, Steve Kozel1, Chris Denicola1
1
Restek, Bellefonte, PA, USA;
2
Cayman Chemical, Ann Arbor, MI, USA
P1-G-103-MO
Determination of Selenoaminoacids by HPLC Fluorescence in Plasma of Sheeps
Supplemented with Selenium
Claudia Valdez Flores, Erika F. Pérez Becerril, Alma L. Revilla Vázquez
Universidad Nacional Autónoma de México, Mexico, MEX
P1-G-104-TU
Determination of t,t-muconic Acid in Urine Samples
Silvia Marten, Mareike Naguschewski
Knauer GmbH, Berlin, D
P1-G-106-TU
Development of an Automated Ion-Trap MSn-Based Screening Method for Clinical and
Forensic Toxicology
Jürgen Kempf1, Susanne Vogt1, Anna Sandhaas1, Wolfgang Weinmann2,
Birgit Schneider3, Petra Decker3, Sebastian Götz3, Arnd Ingendoh3, Carsten Baessmann3
1
University Medical Center Freiburg, Freiburg, D;
2
Universität Bern, Bern, CH;
3
Bruker Daltonik GmbH, Bremen, D
P1-G-107-MO
Enantiomeric Resolution, Identification, and Quantitation of Chiral Illicit Drugs using
SFC APCI MS/MS
Lakshmi Subbarao1, John McCauley1, Harbaksh Sidhu2, Rui Chen1, Jacquelyn Runco1
1
Waters Corporation, New Castle, DE, USA; 2Waters Corporation, Pittsburgh, PA, USA
P1-G-108-TU
Fabrication of Hierarchically Porous TiO2 Monoliths for HPLC Columns
George Hasegawa1, Kei Morisato2, Kazuyoshi Kanamori1, Kazuki Nakanishi1
1
Kyoto University, Kyoto, J; 2GL Sciences Inc., J
76
P1-G-109-MO
Forensic Screening of Isobaric Compounds in Crude Samples by Ultrahigh-Resolution
UHPLC-QTOF Technology
Zoltan Czentnar1, Marcus Macht1, Anna Pelander2, Petra Decker1, Carsten Baessmann1
1
Bruker Daltonik GmbH, Bremen, D;
2
University of Helsinki, Helsinki, FIN
P1-G-110-TU
HPLC Determination of Benzodiazepines in Vitreous Humor using Microwave Assisted
Extraction
Purificación Fernandez1, Estrella Núñez1, Ana M. Bermejo1, Rosa A. Lorenzo2,
Antonia M. Carro2
1
Institute of Legal Medicine, C/ San Francisco, Santiago de Compostela, E;
2
Avda. de las Ciencias Santiago de Compostela, E
P1-G-111-MO
Lipidomic Profiling of Patients with Cardiovascular Diseases
Kateřina Netušilová, Miroslav Lísa, Michal Holčapek
P1-G-112-TU
Quantitative Analysis of Underivatized 1,25-Dihydroxyvitamin D3 and D2 in Blood by
UHPLC and Triple Quadrupole Mass Spectrometer Utilizing Ion Funnel Technology
Andre Szczesniewski, Monika Dittmann
P1-G-113-MO
Quantitative Profiling of Eicosanoids in Plasma by Liquid
Chromatography-Quadrupole/Time-of-Flight-Mass Spectrometry
Su Hyeon Lee1,2, Young Wan Ha1, Won-Yong Lee2, Bong Chul Chung1, Man Ho Choi1
1
Biomolecule Function Research Center, Seoul,ROK;
2
Yonsei University, Seoul, ROK
P1-G-114-TU
Rapid Screening of Derivatised Anabolic Steroids in Equine Urine using Ultra
Performance Liquid Chromatography – Tandem Mass Spectrometry
Colton H. F. Wong, David K. K. Leung, Francis P. W. Tang, Jenny K. Y. Wong,
Nola H. Yu, Terence S. M. Wan
The Hong Kong Jockey Club, Hong Kong, PRC
77
P1-G-115-MO
Rapid Selective Diagnosis of Bacillus Anthracis Infection by LC-MS Detection of
Endoproteinase Activity of Antibody Captured Anthrax Lethal Factor in Serum
Zsuzsanna Kuklenyik1, Anne E. Boyer1, Renato Lins2, Conrad P. Quinn1,
Maribel Gallegos-Candela1, John R. Barr1
1
Centers for Disease Control and Prevention, Atlanta, GA, USA;
2
Battelle Atlanta Analytical Services, Atlanta, GA, USA
P1-G-117-MO
The Development of the Method for the Analysis of Neopterin and its Derivatives by
Means of UHPLC-MS/MS and UHPLC-FD
Helena Tomšíková, Hana Vlčková, Lucie Nováková
P1-G-118-TU
Unambiguous Determination of Milk Phospholipids by HILIC Coupled to an Hybrid
Mass Analyzer
Filomena Cichello1, Francesco Cacciola1, Paola Donato2,1, Paola Dugo1,2,
Luigi Mondello1,2
1
2
Electrodriven Separations
P1-G-119-MO
Stability of Linear Polyacrylamide Coated Capillaries in Acidic Media in the Presence of
Organic Modifiers and Surfactants
Philippe Anres, Nathalie Delaunay, Pierre Gareil
Chimie ParisTech, Paris, F
P1-G-120-TU
A Sensitive Method for the Determination of Ochratoxin A by Capillary Zone
Electrophoresis using Fluorescence Detection and its Application to Certain Foods
Muzaffer Tuncel, Dilek Dogrukol-Ak, Rasime Demirel, Elif Mine Oncu, Ulku Dilek Uysal,
Merih Kivanc
Anadolu University, Eskişehir, TR
P1-G-121-MO
Application of Micellar Electrokinetic Chromatography Method for Determination of
Oxidized and Reduced Glutathione in Human Blood
Paulina Chyla, Dariusz Wideł, Ewelina Blonska, Zygfryd Witkiewicz
Jan Kochanowski University, Kielce, PL
78
P1-G-122-TU
Application of Microemulsion Electrokinetic Chromatography for Quantitative Analysis
of α-Tocopherol Acetate in Pharmaceutical Preparations
Dariusz Wideł, Jerzy Oszczudlowski, Zygfryd Witkiewicz
P1-G-123-MO
Capillary Electrophoresis Analysis of Carbohydrates in Post-Blast Residue Extracts
Cedric Sarazin1,2, Nathalie Delaunay2, Christine Costanza1, Veronique Eudes1,
Pierre Gareil1
1
Central Laboratory of the Prefecture de Police, Paris, F;
2
P1-G-124-TU
Capillary Zone Electrophoresis for Caco-2 Cell Cytotoxicity Analysis
Lu Zhang1, Feng Qu1, Meiling Hu1, Jinmei Ding2, Beilei Lou1
1
Beijing Institute of Technology, Beijing, PRC;
2
National Institute of Biological Sciences, Beijing, PRC
P1-G-125-MO
Covalent Binding of Phospholipids on Fused Silica Capillaries for
Electrochromatography
Jana Lokajova, Heidi Tiala, Tapani Viitala, Marja-Liisa Riekkola, Susanne K. Wiedmer
P1-G-126-TU
Determination of Acetylcholinesterase Inhibitors using Capillary Electrophoresis –
Mass Spectrometry
Irene N. Nicolaou, Constantina P. Kapnissi-Christodoulou
P1-G-127-MO
Determination of Acidity Constants by the CE Internal Standard Method: Polyprotic
Compounds
Joan Marc Cabot, Elisabet Fuguet, Clara Ràfols, Martí Rosés
Universitat de Barcelona, Barcelona, E
P1-G-128-TU
Determination of Alcaline Cation Mobility in Background Electrolytes Containing
Micelles
Ludmila Müllerová, Pavel Dubský, Jana Svobodová, Bohuslav Gaš
Charles University in Prague, Prague, CZ
79
P1-G-129-MO
Development of a Generic MEKC Method for the Separation of 15 Antimalarial Drugs
by a Design Space Approach
Caroline Lamalle, Roland Marini, Benjamin Debrus, Pierre Lebrun, Anne-Catherine Servais,
Jacques Crommen, Philippe Hubert, Marianne Fillet
P1-G-130-TU
Drug Quantification in the Presence of Matrix Proteins: A MEKC Method with Direct
Sample Injection
Sascha Kühne, Christopher Untucht, Michael Steinert, Hermann Wätzig
TU Braunschweig, Braunschweig, D
P1-G-131-MO
Electrochromatography Separation of Tryptic Digests of Enzymes using Lauryl
Methacrylate Monolithic Columns
Miriam Beneito-Cambra, Pascuala Vizcaino-Milla, Iván Esteve-Adell,
Guillermo Ramis-Ramos, José Manuel Herrero-Martínez
University of Valencia, Valencia, E
P1-G-132-TU
High Resolution Intact Glycoprotein Analysis by Sheathless Capillary Electrophoresis –
Electrospray Ionization-Mass Spectrometry
Hans Dewald, Scott Mack, Gina Donvito, Kimberly Kwong, Chitra Ratnayake Beckman
Discovery Solutions Business Center, Brea, CA, USA
P1-G-133-MO
Highly Emissive Metal Probes Suitable for Ultratrace Detection of Lanthanide and
Actinide Ions by Capillary Electrophoresis-Laser-Induced Fluorescence
Shingo Saito1, Tomoko Haraga2, Yuta Nakano1, Yoshiyuki Sato1, Yutaka Kameo2,
Kuniaki Takahashi2, Masami Shibukawa1
1
Saitama University, Saitama, J; 2Japan Atomic Energy Agency, Ibaraki, J
P1-G-134-TU
Highly-Sensitive Electrophoretic Analysis of Biomolecules by LVSEP
Saeko Kinami, Takayuki Kawai, Kenji Sueyoshi, Fumihiko Kitagawa, Koji Otsuka
P1-G-135-MO
Infrared-based Temperature Measurements for thorough Analytical Instrument
Qualification in Capillary Electrophoresis
Claudia Cianciulli, Hermann Wätzig
80
P1-G-136-TU
Investigation of Migration Behavior and Separation Mechanism of Coumarins in
Capillary Electrophoresis
Shu-Ping Wang, Ruo-Shuo Yang, Ying Yuan Chang
Providence University, Taichung, RC
P1-G-137-MO
Label-Free Electrophoretic Analysis of Sugars using Complexation with Aryl Boronic
Acids. 2
Risa Kusumoto1, Philip Britz-McKibbin2, Takayuki Kawai1, Kenji Sueyoshi1, Fumihiko Kitagawa1,
Koji Otsuka1
1
Kyoto University, Kyoto, J;
2
McMaster University, Hamilton, ON, CDN
P1-G-138-TU
New Avenue for Mid UV-Range Detection of Underivatized Carbohydrates and
Aminoacids in Capillary Electrophoresis
Cédric Sarazin1,2, Nathalie Delaunay2, Christine Costanza1, Véronique Eudes1,
Jean-Maurice Mallet3, Pierre Gareil2
1
Central Laboratory of the Prefecture de Police, Paris, F;
2
Chimie ParisTech, UPMC Univ, Paris, F; 3UPMC Univ, Paris, F
P1-G-139-MO
Pre-Separation of High Volume Biological Samples using Divergent Flow Isoelectric
Focusing
Filip Duša1,2, Jana Křenková1, Dana Moravcová1, Vladislav Kahle1, Karel Šlais1
1
2
Masaryk University, Brno, CZ
P1-G-140-TU
Protein-Ion Interactions Detected by Affinity Capillary Electrophoresis
Sabine Redweik, Yuanhong Xu, Hermann Wätzig
P1-G-141-MO
Quantification of Aspartate and Glutamate in Brain Microdialysates with CE-LIF
Zsolt Wagner, Tamás Tábi, Gergely Zachar, András Csillag, Éva Szökő
Semmelweis University, Budapest, H
P1-G-142-TU
Searching for Ampholytes Suitable for Oscillating Electrolytes in CZE
Martina Riesová, Lucie Maliňáková, Bohuslav Gaš
81
P1-G-143-MO
Simultaneous Determination of Aminothiols in Human Plasma by Layer-by-Layer
Assembly of Silica Nanoparticles with Amperometric Detection
Lin Zhou1, Corinna Zambardi2, Mila Pravda1, Erika Scavetta2, John H.T. Luong3,
Jeremy D. Glennon1
1
2
University of Bologna, Bologna, I;
3
NRC Institute for Biological Sciences, Montreal, Quebec, CDN
P1-G-144-TU
Speciation Analysis of Aluminium (III)-Dopamine using Capillary Electrophoresis with
Amperometric Detection
Una Barrett1, Fengjun Shang1, John, H. T. Loung2, Jeremy D. Glennon1
1
2
National Research Council Canada, Montreal, Quebec, CDN
P1-G-145-MO
Stability of Linear Polyacrylamide Coated Capillaries in Acidic Media in the Presence of
Organic Modifiers and Surfactants
Philippe Anres, Nathalie Delaunay, Pierre Gareil
P1-G-146-TU
The Effect of pH of the Background Electrolytes on CIEF Applying Sequential Injection
Protocol
Csilla Páger, Andrea Vargová, Ferenc Kilár
P1-G-147-MO
Transient Isotachophoresis of Trace Metals in a Zn Overloaded Saline Sample
Kihwan Choi, Asif Riaz, Ju Rung Park, Eun Jae Shim, Jihye Kim, Doo Soo Chung
Seoul National University, Seoul, ROK
P1-G-148-TU
Transient Trapping in Enantioseparation for High-Sensitive Detection. 2
Hiroshi Koino, Kota Hashiba, Kenji Sueyoshi, Fumihiko Kitagawa, Koji Otsuka
P1-G-149-MO
Use of Ligand Step Gradient Focusing in Combination with Isotachophoresis
(LSGF-ITP) for the Effective Pre-Concentration and Analysis of Heavy Metals
Eliška Glovinová, Jan Pospíchal
Mendel University, Brno, CZ
82
High-Temperature LC
P1-G-150-TU
Comonomer Distribution across Molar Mass Distribution in Polyolefins by GPC using a
Filter-Based IR Detector
Alberto Ortín1, Benjamín Monrabal1, María Celia García-Álvarez-Coque2,
José Ramón Torres-Lapasió2
1
Valencia Parc Tecnologic, Paterna, E; 2Universitat de Valencia, Burjassot, E
P1-G-151-MO
High Temperatures as a Tool to Increase Solvent Compatibility in Two-Dimensional
Liquid Chromatography
Jakob Haun1, Thorsten Teutenberg1, Torsten C. Schmidt2
1
Institut für Energie- und Umwelttechnik, Duisburg, D;
2
University of Duisburg-Essen, Essen, D
P1-G-152-TU
The Prospect of using Sintered Nanodiamond as Stationary Phase for
High-Performance Liquid Chromatography at Elevated Temperatures
Olga N. Fedyanina1, Pavel N. Nesterenko2
1
Moscow State University, Moscow, RUS; 2University of Tasmania, Hobart, AUS
P1-G-153-MO
Fast, UHPLC-like Separation of Basic Analytes at Elevated Column Temperature on
3 μm Particles under Elevated Temperature and Isocratic Conditions
Rainer W. Schmid, Goran Mitulović
Medical University of Vienna, Vienna, A
P1-G-154-TU
Use of Porous Graphitic Carbon in the Study of Thermal Gradient HPLC
Anthony Edge1, Luisa Pereira1, James Heaton2, Monica Dolci1, Harald Ritchie1,
Norman W. Smith2
1
Thermo Fisher Scientific, Runcorn, UK; 2Kings’s College, London, UK
Hyphenated Separations
P1-G-155-MO
1-D Liquid Chromatography – ESI – Tandem MS Coupling for Chemoselective and
Enantioselective Separations of Chiral Amino Acid Derivatives and its Application to
Biologically Relevant Samples
Roland J. Reischl, Wolfgang Lindner
83
P1-G-156-TU
Analysis of Decomposition Products of Hexafluorophosphate Salts in Aqueous Solution
Lydia Terborg1,2,3, Sascha Nowak2, Paul R. Haddad3, Pavel N. Nesterenko3,
Martin Winter2, Uwe Karst1
1,2
Westfälische Wilhelms-Universität Münster, Münster, D;
3
P1-G-157-MO
Analysis of Fentanyl and its Metabolite, Norfentanyl by Capillary Electrophoresis
Coupled to Mass Spectrometry with a Sheathless Porous Electrospray Interface
John C. Hudson
Beckman Coulter, Inc., Discovery Solutions Business Center, Brea, CA, USA
P1-G-159-MO
Analysis of Multi-Component Samples by LC×
×LC-MS/MS
S. Nakanishi, T. Noguchi, H. Miyamoto, T. Seki
Nissan Chemical Industries, Ltd., Chiba, J
P1-G-160-TU
Approaches to LC-MS Hyphenation for Simultaneous Quantification in Biological
Matrices of Xenobiotics and Metabolites with Wide pKa and Polarity Ranges
Zsuzsanna Kuklenyik, Antonia M. Calafat, John R. Barr, James L. Pirkle
Centers for Disease Control and Prevention, Atlanta, GA, USA
P1-G-161-MO
Challenges in the Structure Elucidation of New Bis-Indole Alkaloids: LC-FTICR-MS/MS
and NMR Analysis of Vinblastine and Vincristine Impurities
Viktor Háda, Zsófia Dubrovay, Zoltán Gulyás, Ágnes Lakó Futó
P1-G-162-TU
Comprehensive Investigation of the Influence of using Acidic and Basic Mobile Phases
on Bioanalysis Assay Sensitivity in Positive Ion ESI Mass Spectrometry
Paul D. Rainville1,2, Joanne Mather1, Norman W. Smith2, Robert S. Plumb1,2
1
Waters Corporation, Milford, MA, USA;
2
King’s College London, London,UK
P1-G-163-MO
Coupling of HT-HPLC with Enzymatic Assays – The Issue of Organic Solvent
Romy K. Scheerle1, Thorsten Teutenberg2, Johanna Grasmann1, Thomas Letzel1
1
TU München, Freising, D;
2
Institut für Energie- und Umwelttechnik e. V., Duisburg, D
84
P1-G-164-TU
Determination of Serotonin and its Precursors by Capillary LC-MS. Application to
Chocolate Samples
Vanesa Guillen-Casla, Noelia Rosales-Conrado, María Eugenia de León-González,
Luis Vicente Pérez-Arribas, Luis María Polo-Díez
Complutense University of Madrid, Madrid, E
P1-G-165-MO
Development of a Pre-Column Derivatization Strategy for the Measurement of the
Tricarboxylic Acid Cycle Intermediates by Means of Reversed Phase LC-MS with ESI+
Ionization
D. Kloos1, M. Giera1, M. Wijtmans2, R. J. E. Derks3, O. A. Mayboroda3, A. M. Deelder3,
W. M. A. Niessen1
1,2
VU Amsterdam, Amsterdam, NL;
3
LUMC Leiden, Leiden, NL
P1-G-166-TU
Development of a Raman Detector for Hyphenation with High-Temperature Liquid
Chromatography and Isotope Ratio Mass Spectrometry
Björn Fischer, Hans Bettermann
Heinrich-Heine-University, Düsseldorf, D
P1-G-167-MO
Development of a Simple, Fast and Quantitative UHPLC-MS/MS Method for the
Determination of Organic Acids in Fermentation Processes
Burhan Ozalp, Erwin Kaal, Lucien Duchateau
DSM Biotechnology Center, Delft, NL
P1-G-168-TU
Enabling Faster Separations and Smaller Sample Volumes with Micro-Flow Liquid
Chromatography
Steve Hobbs, Dave Neyer, Khaled Mriziq
Eksigent, division of AB Sciex, Dublin, CA, USA
P1-G-169-MO
Evaluation of SFC-MS Configurations for the Analysis of Lipids, Sterols and Polycyclic
Aromatic Hydrocarbons
Melissa Dunkle1, Alberto dos Santos Pereira1, Nobukazu Higashi2, Kazuhisa Mitsui2,
Hirooki Kanda3, Frank David1, Pat Sandra1
1
2
Japan Tobacco Inc., Yokohama, J;
3
Gerstel K.K., Tokyo, J
85
P1-G-170-TU
How to Select Orthogonal Conditions in Reverse Phase to Achieve LCxLC Separations
According to the Nature of Compounds
Ramia Al Bakain1, Isabelle Rivals2, Patrick Sassiat1, Didier Thiebaut1,
Marie-Claire Hennion1, Guillaume Euvrard2, Jérôme Vial1
1
UMR-CNRS-UPMC-PECSA, Paris, F;
2
ESPCI ParisTech, Paris, F
P1-G-171-MO
HPLC-MS-MS Analysis of Pteridines in Graphosoma Lineatum by Hydrophilic
Interaction Liquid Chromatography
P. Kozlík, J. Krajíček, E. Tesařová, R. Čabala, Z. Bosáková
P1-G-172-TU
Hydrophilic Interaction Liquid Chromatography (HILIC) Coupled to Mass Spectrometry
for the Characterization of Prebiotic Galactooligosaccharides
O. Hernández-Hernández1, I. Calvillo1, R. Lebrón-Aguilar2, F. J. Moreno3, M. L. Sanz1
1,2
CSIC, Madrid, E;
3
CSIC-UAM, Madrid, E
P1-G-173-MO
Improved Interface for Connecting SFC to MS and Moving toward Open Access
SFC/MS
Xu Zhang, Mark J. Hayward
Lundbeck Research USA, Paramus, NJ, USA
P1-G-174-TU
Improving Sensitivity in Bioanalytical LC/MS/MS through Efficient Management of
Mobile Phase pH
Paul D. Rainville, Robert S. Plumb, Thomas Wheat
P1-G-175-MO
In-Capillary Screening of Matrix Metalloproteinase Inhibitors by Capillary
Electrophoresis for Coupling with ESI Mass Spectrometry
Xu Wang, Erwin Adams, Ann Van Schepdael
K. U. Leuven, Leuven, B
P1-G-176-TU
LC-Ion Exchange SPE-NMR
Cristina Daolio, Markus Godejohann, Ulrich Braumann, Manfred Spraul
Bruker BioSpin GmbH, Rheinstetten, D
86
P1-G-177-MO
Measurement of Zwitterionic Osmolytes by LC-MS/MS
Chris McEntyre1, Crystal Lenky2, Michael Lever3
1,2
University of Canterbury, Christchurch, NZ;
3
Canterbury Health Laboratories, Christchurch, NZ
P1-G-179-MO
Optimization and Evaluation of a Sheathless Capillary Electrophoresis-Electrospray
Ionization-Mass Spectrometry (CE-ESI-MS) Platform for the Analysis of
Posttranslationally Modified Peptides: Comparison to LC-MS
Herbert Lindner, Klaus Faserl, Leopold Kremser, Bettina Sarg
Innsbruck Medical University, Innsbruck, A
P1-G-180-TU
Optimization of Lipidomic Analysis using Off-Line Two-Dimensional HILIC x RP
HPLC/MS
Eva Cífková, Miroslav Lísa, Michal Holčapek
P1-G-181-MO
Polyphenolic Fingerprint of Various Natural Matrices by RPLC Coupled to Quadrupole
and Hybrid Mass Analyzers
Francesco Cacciola1, Paola Donato2,1, Marina Russo3, Paola Dugo1,2, Luigi Mondello1,2
1
University of Messina, Messina, I; 2University Campus Bio-Medico, Rome, I;
3
Baller (s.r.l.), Messina, I
P1-G-182-TU
Rapid Method for the Detection of Metabolite of Lewisite – 2-Chlorovinylarsonous Acid
in Urine by Liquid Chromatography-Negative Electrospray-Tandem Mass Spectrometry
Arkady Braun1, Igor Rodin1, Oleg Shpigun1, Andrey Stavrianidi1, Igor Rybalchenko2
1
Lomonosov Moscow State University, Moscow, RUS; 2“Lumex ltd.”, Moscow, RUS
P1-G-183-MO
Robustness and Metal Release Testing of the New Agilent 1260 Infinity Bio-Inert LC
with Agilent 7700 ICP-MS
Nicole Fellner, Jochen Strassner, Katja Kornetzky
P1-G-184-TU
Separation and Structural Identification of Lipid A Molecules by Capillary
Electrophoresis – Electrospray Mass Spectrometry
Viktor Sándor, Ágnes Dörnyei, Anikó Kilár, Béla Kocsis, Ferenc Kilár
87
P1-G-185-MO
Separation of Polar Polycyclic-Aromatic Compounds by Online Comprehensive
Two-Dimensional Liquid Chromatography (LC×
×LC)
Rune Grasboll, Nikoline Juul Nielsen, Jan H. Christensen
University of Copenhagen, Frederiksberg C, DK
P1-G-186-TU
Sheathless Capillary Electrophoresis-Electrospray Ionization Mass Spectrometry for
the Analysis of Samples Available in Minute Amounts
Jean-Marc Busnel1,2, Jeff D. Chapman1, Jerald S. Feitelson1, Andre M. Deelder2,
Oleg A. Mayboroda2
1
Beckman Coulter, Inc., Brea, CA, USA;
2
Leiden University Medical Center, Leiden, NL
P1-G-187-MO
Towards Standard-Free Quantitative and Qualitative Analysis in Liquid
Chromatography
Markus M. Martin1, Frank Steiner1, Michael Heidorn1, Marc Plante2, Fraser McLeod1
1
Dionex-Softron GmbH, Germering, D;
2
Dionex Corporation, Chelmsford, MA, USA
P1-G-188-TU
Using a Sheathless MS Interface Leads to Higher Resolutions and Sensitivities in the
CE Analysis of Peptides
Rene Kuijpers, Peter Wierenga, Henk Schols, Harry Gruppen
Wageningen University, Wageningen, NL
P1-G-189-MO
Advantages of Multiple Time-Slice Injections in Sensitive, High-Throughput LC-MS
Analyses
David W. Neyer and Don W. Arnold, Remco van Soest
Eksigent Technologies, Dublin, CA, USA
Natural Product Analysis
P1-G-190-TU
A Comparison between Ultraviolet Detection and Pulsed Amperometric Detection for
the Simultaneous Analysis of Saikosaponins, Glycyrrhizinic Acid, Poncirin, and
Naringin in Caihu-Dayuan-Yin
Ha-Jeong Kwon, Hee-Jung Sim, Sa-Im Lee, Min-Jung Gu, Seon-Pyo Hong, Yong-Duk Park
Kyung Hee University, Seoul, ROK
88
P1-G-191-MO
Alcoholic Fraction Composition in Essential Fragrances: A Comparative Study between
CG-MS and HPLC-UV-MS with Pre-Column Derivatization
Miriam Beneito-Cambra, Tamara Cortell-Barberá, Guillermo Ramis-Ramos,
José Manuel Herrero-Martínez
P1-G-193-MO
Analysis of Native Carotenoid Composition in Sweet Bell Peppers using C30 Columns
in Tandem
Paola Dugo1,2, Daniele Giuffrida3, Germana Torre1, Francesco Cacciola1, Paola Donato2,1,
Luigi Mondello1,2
1,3
2
P1-G-194-TU
Analysis of Plant Hormones by HPLC-MS Based on New Pretreatment Methods
Lan Zhang, Qiaomei Lu
Fuzhou University, Fujian, PRC
P1-G-195-MO
Analysis of Polysaccharides from Chinese Herbs using Saccharide Mapping
Jing Zhao, Jing Xie, Yiwen Chen, Jia Guan, Shao-ping Li
University of Macau, Macau SAR, PRC
P1-G-196-TU
Analysis of Radix Angelicae Sinensis by Comprehensive Two-Dimensional
Chromatographic Separation Techniques
Roman Duck1, Alexandra von Trotha1, Margit Geisler2, Oliver J. Schmitz1
1
University of Wuppertal, Wuppertal, D;
2
Shimadzu Europa GmbH, Duisburg, D
P1-G-197-MO
Application of Acetylcholinesterase Enzyme Silica Capillary Tube Reactor for Online
Ligands and Extracts Screening
Joyce I. da Silva1 (PG), Marcela C. de Morais2 (PG), Cláudio Viegas Jr.3 (PQ),
Antônia Q. L Souza4 (PQ), Afonso D.L. de Souza4 (PQ), Quezia B. Cass2 (PQ),
Carmen Lúcia Cardoso1 (PQ)
1
USP Brazil, São Paulo, BR;
2
Universidade Federal de Sao Carlos, Sao Carlos, SP, BR;
3
Universidade Federal de Alfenas, Alfenas, BR;
4
Universidade Federal do Amazonas-ICB-DFCA/UFAM, Manaus, BR
89
P1-G-198-TU
Application of an HPLC Method on Analysis of Bioactive Compounds of Niuchangchih
(Antrodia Camphorata) on Hepatoprotection against Alcoholic Injury Analyses of
Bioactive Compounds in Niuchangchih (Antrodia Camphorata) via an HPLC and Its
Hepatoprotection Against Chronic Alcohol Injury
Yi-Chen Chen1, Min-Tze Wu2, Chia-Hsin Huang2, Yuan-Yen Chang3
1
National Taiwan University, Taipei, RC; 2Taiwan Agricultural Research Institute,
Taichung, RC; 3Chung Shan Medical University, Taichung, RC
P1-G-199-MO
Application of Chromatographic Methods in the Study and the Characterization of
Stem Bark Extracts from Phyllanthus muellerianus (Kuntze) Excell
Caterina Temporini, Gloria Brusotti, Ilaria Cesari, Giorgio Frassà, Gabriele Caccialanza
University of Pavia, Pavia, I
P1-G-201-MO
Application of Multidimensional Chromatographic Method using Combination of IMAC,
SEC and RP-HPLC for Characterization of Soil Humic Substances
Róbert Góra, Radoslav Halko, Milan Hutta, Pavol Rohárik, Imriščák Lukáš,
Veronika Počiatková
Comenius University, Bratislava, SK
P1-G-202-TU
Application of TLC-MS to Characterize Multifarious Plant Extracts
Árpád Könczöl1, Ágnes Alberti2, Ágnes Kéry2, Gyula Beke1, György Tibor Balogh1
1
Gedeon Richter Plc., Budapest, H; 2Semmelweis University, Budapest, H
P1-G-203-MO
Catalytic Hydrolysis of Cellulose in Ionic Liquid
Kati Helmja, Merike Vaher
Tallinn University of Technology, Tallinn, EST
P1-G-204-TU
Characterization of Biological Adhesives – Insects as an Inspiration for Biomimetic
Applications
Lisa Steinhauser, Julius Braun Manuela, Gradl, Tim Nicholson, Klaus Albert
University of Tübingen, Tübingen, D
P1-G-205-MO
Chromatographic Profiles of Betalain Degradation Products from Red Beet Root
Extracts
Aneta Sporna-Kucab, Sławomir Wybraniec, Paweł Stalica
Cracow University of Technology, Cracow, PL
90
P1-G-206-TU
Comparison of Different Techniques to Identify Similar Strains of Pseudomonas
Anna Kubesová1,3, Marie Horká1, Jaroslav Horký2, Hana Matoušková2, Karel Šlais1
1
2
State Phytosanitary Administration, Olomouc, CZ;
3
Masaryk University Brno, CZ
P1-G-208-TU
Comprehensive 2-Dimensional Liquid Chromatographic Analysis of Grape Tannins
Kathithileni M. Kalili, André de Villiers
P1-G-209-MO
Comprehensive 2-Dimensional Liquid Chromatographic Analysis of Rooibos Tea
(Aspalathus linearis) Phenolics
T. Beelders1, K.M. Kalili2, D. De Beer3, E. Joubert1,3, André de Villiers 2
1,2
Stellenbosch University, Matieland, ZA; 3ARC Infruitec-Nietvoorbij, Stellenbosch, ZA
P1-G-210-TU
Detection of Panax Ginseng Extracts using Comprehensive Two-Dimensional LC-MS
Coupled with PCA
Tatsunari Yoshida1, Ken-ichiro Tanaka1, Tairo Ogura1, Tsutomu Nishine1,
Hirohisa Mikami1, Luigi Mondello2, Paola Dugo2
1
Shimadzu Corporation, Hadano-city, Kanagawa, J; 2University of Messina, Messina, I
P1-G-211-MO
Determination of Astragalin and Astragalosides I–IV in Radix Astragali using HighPerformance Liquid Chromatography Method with Pulsed Amperometric Detection
Ha-Jeong Kwon, Yong-Duk Park
P1-G-212-TU
Determination of Carotenoids in Commonly Consumed Vegetables
Zora Kotíková, Alena Hejtmánková, Jaromír Lachman
Czech University of Life Sciences, Prague, CZ
P1-G-213-MO
Determination of Carotenoids, Flavonoids, Phenolic acids and Tocopherols in Ethanolic
Extracts of Pleurotus eryngii Fruit Bodies Harvested at Various Time by HPLC and
Antioxidant Capacities of the Extracts
Deng-Jye Yang1, Jau-Tien Lin2, Lao-Dar Juang3
1,2
Chung Shan Medical University, Taichung, RC;
3
National Chung Hsing University, Taichung, RC
91
P1-G-214-TU
Determination of Certain Flavonoids by Liquid Chromatograhy Employing Internal
Standard and its Application to Some Aromatic Plants
Ulku Dilek Uysal, Muzaffer Tuncel, Nilgun Ozturk, Elif Mine Oncu-Kaya, Sinem Türkkan,
Kubra Kurtulan
P1-G-216-TU
Determination of Phenolic Acids in Ginger by High Performance Liquid
Chromatography
Elif Mine Öncü Kaya, Nilgün Öztürk, Ülkü Dilek Uysal, Muzaffer Tunçel
P1-G-217-MO
Determination of Saponins in Paris formosana Hayata by High-Performance Liquid
Chromatography with Evaporative Light Scattering Detection
Jau-Tien Lin, Yan-Zin Chang, Shih-Chuan Liu, Mei-Peng Lu, Deng-Jye Yang
Chung Shan Medical University, Taichung, RC
P1-G-218-TU
Determination of the Composition of Natural Products by HPLC with Charged Aerosol
Detection
Ian N. Acworth, Bruce Bailey, Paul Gamache, John Waraska
P1-G-219-MO
Determination of Tocopherols in Pumpkin Seed Oils by HPLC-UV-Vis: Application to Oil
Classification According to Genetic Variety
Yanelis Saucedo-Hernández1, María Jesús Lerma-García2, José Manuel Herrero-Martínez2,
Guillermo Ramis Ramos2, Elisa Jorge Rodríguez1, Ernesto F. Simó-Alfonso2
1
Central University “Marta Abreu” of Las Villas, Santa Clara, C;
2
P1-G-220-TU
Development and Certification of Catechins and Alkaloids in Green Tea Containing
Reference Materials
L. C. Sander1, K. E. Sharpless1, S. A. Wise1, M. Bedner1, M. C. Tims1, R. Lieberman1,
J. H. Yen2, A. NguyenPho3, M. C. Roman4, M. Payne5, J. M. Betz6
1,2
National Institute of Standards and Technology (NIST), Gaithersburg, MD, USA;
3
Center for Drug Evaluation and Research (CDER), College Park, MD, USA;
4
Tampa Bay Analytical Research, Inc., Largo, FL, USA;
5
Hershey Foods Corporation, Hershey, PA, USA;
6
National Institutes of Health, Bethesda, MD, USA
92
P1-G-221-MO
Extraction and Analyses of Chiral Isomers (Eipgoitrin/Goitrin) from Isatis Indigotica
Fort Root Extract using SFE and SFC-MS
Jacquelyn Runco1, Jeff Wright1, Li Yang2, Kate Yu3, Rui Wang2, Yiming Li2,
Zhengtao Wang2, Alan Millar3, Harbaksh Sidhu4, Rui Chen1
1,3,4
Waters Corporation, New Castle, DE, USA;
2
Shanghai Traditional Chinese Medicine University, Shanghai, PRC
P1-G-222-TU
Gradient HPLC with Electrochemical Array Detection for the Measurement of
Polyphenols in Natural Products, Botanicals, Supplements, and Animal and Human
Tissues
Ian N. Acworth, John Waraska, Paul Gamache
P1-G-223-MO
High Throughput Methodology to Characterize Red Wine Polyphenols using Solid
Phase Extraction Combined with Ultra-Performance Liquid Chromatography
Jorge Pereira, Catarina Luis Silva, José S. Câmara
Universidade da Madeira, Funchal, P
P1-G-224-TU
High Throughput SPE/UPLC-PDA-based Methodology for the Simultaneous
Determination of Bioactive Phenolic Metabolites in Food Dietary Products
Carla Miguel, Jaime Camacho, Paulo Craveiro, Catarina L. Silva, Jorge Pereira,
José S. Câmara
P1-G-225-MO
High-Performance Liquid Chromatographic Determination of Bergenin and Arbutin in
Leaves of Different Bergenia Species
Borbála Boros1, Silvia Jakabová2,3, Réka Molnár4, Ágnes Farkas4, Attila Felinger2
1,2,4
3
Constantine the Philosopher University in Nitra, Nitra, SK
P1-G-226-TU
Identification of Morphological Similar Species of Genus Monilinia by Capillary and Gel
Format of the Electromigration Techniques and MALDI-TOF MS
Anna Kubesová1,3,, Marie Horká1, Jiří Šalplachta1, Eva Zapletalová2, Jaroslav Horký2
1
Institute of Analytical Chemistry of the ASČR, Brno, CZ;
2
State Phytosanitary Administration, Olomouc, CZ;
3
Masaryk University Brno, Brno, CZ
93
P1-G-227-MO
Improved Analysis of Isoquinoline Alkaloids in Goldenseal Root Extract using Charged
Surface Hybrid Technology
Mia Summers, Kenneth J. Fountain
P1-G-228-TU
Improving the Analysis of Complex Natural Products through Systematic Evaluation of
Different Liquid Chromatography Stationary Phase Chemistries and Modern Particle
Platforms
David S. Bell, Craig Aurand, Anders Fridstrom, Frank Michel
Sigma-Aldrich/Supelco, Bellefonte, Pennsylvania, USA
P1-G-229-MO
Isolation, Characterization and Qualitative Analysis of 5-Deoxyflavones in Mimosa
Displotricha
Lie-Chwen Lin, Chun-Tang Chiou
National Research Institute of Chinese Medicine, Taipei, RC
P1-G-230-TU
Isolation, Identification and Quantification of Cytokinin Nucleotides by High
Performance Liquid Chromatography and Capillary Electrophoresis
Tibor Béres1, Petr Tarkowski2, Miroslav Strnad1,2, Karel Doležal1,2
1
Institute of Experimental Botany ASCR, Olomouc, CZ;
2
Palacký University, Olomouc, CZ
P1-G-231-MO
LC/MS Separation of Natural Antioxidants in Herbs and Honey Extracts using PFP
Column
Petra Dinisova, Petr Česla, Lenka Česlova, Jan Fischer
P1-G-232-TU
LCxLC Separation of Polyphenols from the Stems of Rubus idaeus
M. Majdan-Skóra, D. Głód, M. Krauze-Baranowska
Medical University of Gdańsk, Gdańsk, PL
P1-G-233-MO
Molecularly Imprinted Polymers of Fructosazine for Extraction from Selected Plants
Nathaly Henry1,2, Raphaël Delepee1, Sylvie Coquerelle2, Jean-Marc Seigneuret2,
Luigi A. Agrofoglio1
1
Université d’Orléans, Orléans, F;
2
Alban Muller, Laboratoires PRAT, Montreuil, F
94
P1-G-234-TU
Monitoring of Opium Alkaloids from Papaver somniferum L. Collected in the Czech
Republic using LC-ESI-MS/MS Method
Alena Hejtmánková, Irena Stránská, Kateřina Hejtmánková, Vladimír Pivec, Kristina Jírů,
Jan Novák
Czech University of Life Sciences Prague, Prague, CZ
P1-G-235-MO
Monitoring of Vitamin E Stability in Milk and Cream using RSLC-ESI-MS Method
Kateřina Hejtmánková1, Alena Hejtmánková1, Vladimír Pivec1, Tereza Michlová1,
Ondřej Elich2
1
Czech University of Life Sciences Prague, Prague, CZ;
2
Dairy Research Institute, MILCOM a.s., Prague, CZ
P1-G-237-MO
Novel HPLC-Based Approach for the Global Measurement of Lipids
Fraser McLeod, Marc Plante, Ian N. Acworth, Frank Steiner
P1-G-238-TU
Phenolic Antioxidant Tyrosol in Czech Wines by HPLC
Matyáš Orsák, Kateřina Hejtmánková, Vladimír Pivec, Jaromír Lachman
Czech University of Life Sciences Prague, Prague, CZ
P1-G-239-MO
Polyphenol Composition and Antioxidant Potential of Certain Salvia Species
Nilgun Ozturk1, Hasibe Ozcan2, Muzaffer Tuncel3, Ismuhan Potoglu-Erkara2,
Onur Koyuncu2
1,3
Anadolu University, Eskişehir, TR;
2
Eskişehir Osmangazi University, Eskişehir, TR
P1-G-240-TU
Post-Column pH Buffered Electric Conductivity Detection of Organic Acids with Ultra
High Performance Liquid Chromatography
Kyoko Watanabe, Makoto Ogaito, Atsushi Ieuji, Hirohisa Mikami
Shimadzu Co., Kyoto, J
P1-G-241-MO
Rapid Analytical Approach for Quantification the Total L-Ascorbic Acid Content in
Fruits and Vegetables by Ultra-Performance Liquid Chromatography
Vitor Spinola, Berta Mendes, Jorge Pereira, José S. Câmara, Paula Castilho
95
P1-G-242-TU
Rapid Approach by Ultra Performance Liquid Chromatography Combined with
Microextraction by Packed Sorbent for Determination of Trans-Resveratrol in Wines
João Gonçalves, Jorge Pereira, José S. Câmara
P1-G-243-MO
Rapid Determination of Anthocyanins in Pomegranate Juice and Bilberries
Pranathi P. Perati, Brian M. De Borba, Jeffrey S. Rohrer
Dionex Corporation, Sunnyvale, CA, USA
P1-G-244-TU
Separation and Quantification of Different Flavonoids Found in Natural Therapeutics
and Functional Foods by RP-HPLC on a Stationary Phase Providing π-π
π Interactions
Robert Fredriksson, Joakim Högblom, Sylvia Winkel-Pettersson
Eka Chemicals AB, Bohus, S
P1-G-245-MO
Separation of Betalains from Red Beet (Beta vulgaris L.) by High-Performance
Countercurrent Chromatography (HPCCC) using High Salt-Solvent Systems
Aneta Spórna-Kucab1, Svetlana Ignatova2, Ian Garrard2, Sławomir Wybraniec1,
Paweł Stalica1
1
Cracow University of Technology, Cracow, PL;
2
Brunel University, Uxbridge, Middlesex, UK
P1-G-246-TU
Separation of Phenolic Acids in Marine Plants by Molecular Imprinting
Anion-Exchangeable Polymer Confined Ionic Liquids
Wentao Bi, Minglei Tian, Kyung Ho Row
Inha University, Incheon, ROK
P1-G-247-MO
Separation of Triacylglycerol Enantiomers and Regioisomers using Chiral HPLC/MS
Miroslav Lísa, Michal Holcapek
P1-G-248-TU
Simultaneous Analysis Method for Polar and Non-Polar Ginsenosides in White and
Red Ginseng by Reversed-Phase HPLC-PAD
Sa-Im Lee, Ha-Jeong Kwon, Seon-Pyo Hong
96
P1-G-249-MO
Simultaneous Determination of Eight Bioactive Compounds in Polygonum Multiflorum
using Pressurized Hot Water Extraction and High Performance Liquid Chromatography
Dong-qi Han, Jing Zhao, Shao-ping Li
University of Macau, Macao, PRC
P1-G-250-TU
Simultaneous Determination of Eleven Intact Glucosinolates in Fresh and Controlled
Atmospheres Stored Broccoli Plants by HPLC-MS/MS
M. F. Fernández-León1, M. Lozano1, M.C. Ayuso2, D. González-Gómez1
1
Instituto Agroalimentario de Extremadura (INTAEX), Badajoz, E;
2
University of Extremadura, Badajoz, E
P1-G-251-MO
Simultaneous Determination of Free Indole-3-acetic Acid and Related Esters in Plant
Tissues by LC-QTOF-MS
Yuan Liang, Xiaocui Zhu, Meiping Zhao, Huwei Liu
Peking University, Beijing, PRC
P1-G-252-TU
Simultaneous Identification of Dyes and Binding in Graphic Documents by Capillary
Electrophoresis
Ana Mª López-Montes, Cristina Prats Henares, Mª Esther Castillo Valdivia,
Teresa Espejo Arias, José Luis Vílchez Quero, Mª Rosario Blanc García
University of Granada, Granada, E
P1-G-253-MO
The Development and Validation of an LC-MS/MS Methods for the Determination of
Tetrodotoxin (TTX) in Trumpet Shell, Charonia lampas
Sharon Hutchinson1, Paul Barnes2, Joana Azevedo3,5, Vitor Vasconcelos3,4,
Cowan Higgins6, Judith Nzoughet7, Chris Elliott7, Ambrose Furey1
1
Cork Institute of Technology, Cork, IRL;
2
Agri-Food and Biosciences Institute – Stormont, Belfast, UK;
3
Centre of Marine and Environmental Research, Porto, P;
4
University of Porto, Porto, P;
5
School of Health Technology of Porto, Vila Nova de Gaia, P;
6
Agri-Food and Biosciences Institute, Belfast, UK;
7
University Belfast, Belfast, UK
P1-G-254-TU
UHPLC Determination of Glycoside Sweeteners: Steviol Glycosides and Mogroside V
Deanna C. Hurum, Brian M. De Borba, Deepali Mohindra, Jeffrey S. Rohrer
97
P1-G-255-MO
Ultrafast-High Performance Liquid Chromatography as a Suitable Methodology for the
Analysis of Carotenoids in Honey-Bee Pollen
D. González-Gómez, D. Bohoyo-Gil, S. Nogales-Delgado, M. Izquierdo Rey,
D. Domínguez-Valhondo
Instituto Tecnologico Agroalimentario, Badajoz, E
New Instrumentation for LC
P1-G-256-TU
Advantage of a New Generation of Evaporative Light-Scattering Detectors:
Universality, Higher Sensitivities and Cost-Effectiveness for Multi-Element Analyses in
Liquid Chromatography – An Application Review
Eric Verette
SEDERE SAS, Olivet, F
P1-G-257-MO
Assessment of a New Generation of Evaporative Light-Scattering Detectors for Liquid
Chromatography: Sensitivity, Linearity, Dynamic Range, Analyte Dispersion and
Response Variation with Eluent Composition
Eric Verette
SEDERE SAS, Olivet, F
P1-G-258-TU
Behavior of Glassy Carbon Paste Electrode in HPLC with Amperometric Detection
Hana Dejmkova, Jan Mika, Jiri Barek, Jiri Zima
P1-G-259-MO
A Complete Solution for Method Linearity in HPLC and UHPLC
Frank Steiner, Tobias Fehrenbach, Andreas Brunner, Fraser McLeod
Dionex Corporation, Germering, D
P1-G-260-TU
Complex Rapid Temperature Programming for Capillary and Microscale Liquid
Chromatography through the Application of Direct Contact Thermoelectric Module
Arrays
David Collins1, Ekaterina Nesterenko1, Damian Connolly1, Mirek Macka2,
Dermot Brabazon1, Brett Paull1,2
1
Dublin City University, Dublin, IRL;
2
98
P1-G-261-MO
Fast LC using a New Generation Micro-UHPLC System with Array Based UV Detection
Khaled S. Mriziq, David Neyer, Steve Hobbs, Remco van Soest, Phillip Paul, Don Arnold
P1-G-262-TU
Non-Discriminatory, Universal and Sensitive Detection Technologies for Fluid Based
Separation Techniques
Joseph P. Hutchinson1, Manish Khandagale1, Jianfeng Li1, William Farrell2,
Elizabeth Groeber3, Roman Szucs4, Greg Dicinoski1, Paul R. Haddad1
1
2
Pfizer Global R&D, La Jolla, CA, USA;
3
Pfizer Global R&D, Groton, CT, USA;
4
Pfizer Global R&D, Sandwich, Kent, UK
P1-G-264-TU
The Impact of Solvent Mixing on Liquid Chromatographic Performance
Christian Schmidt, Verena Jendreizik, Wulff Niedner, Fraser McLeod
P1-G-265-MO
Total Solutions for High-Throughput Analysis and Purifications
Steve Zulli, Ziqiang Wang, Dan Rolle, Jon Jones, Tim Martin, Harbaksh Sidhu
Waters Corporation, Newark, DE, USA
Oligonucleotide Separations
P1-G-266-TU
Improvement in the Sensitivity of RT-PCR Assays by using RP-HPLC Probe Purification
Alena G. Mosina1, Andrey N. Chuvilin2, Igor P. Smirnov2, Galina E. Pozmogova2,
Ekaterina F. Kislina2
1
Moscow State Academy of Fine Chemical Technology, Moscow, RUS;
2
Research Institute of Physical-Chemical Medicine, Moscow, RUS
P1-G-267-MO
UPLC System Optimization and Solid Phase Extraction Method Development
Strategies for the Analysis for Oligonucleotides
Xin Zhang, Pamela Iraneta, Frank Marszalkowski, Darryl Brousmiche, Kevin Wyndham,
Raymond P. Fisk, Tom Walter
99
Planar Chromatography
P1-G-268-TU
Comparing Reversed-Phase and Micellar Liquid Chromatography to Study Lipophylicity
of 1,2,4-Triazoles
Małgorzata Janicka1, Katarzyna Ste˛pnik1, Anna Pachuta-Stec2
1
Maria Curie-Skłodowska University, Lublin, PL; 2Medical University, Lublin, PL
P1-G-269-MO
Isolation and Characterization of Antimicrobial Compounds from Plant Extracts by
means of OPLC, GC-MS and BioArena
Ágnes M. Móricz1, Szabolcs Szarka2, Péter G. Ott1, Éva B. Héthelyi2, Éva Szőke2,
Ernő Tyihák1
1
Plant Protection Institute, HAS, Budapest, H; 2Semmelweis University, Budapest, H
P1-G-270-TU
Micellar HPLC, OPLC and TLC in Studying Lipophylicity of 1,2,4-Triazoles
Małgorzata Janicka1, Katarzyna Ste˛pnik1, Anna Pachuta-Stec2
1
Maria Curie-Skłodowska University, Lublin, PL; 2Medical University, Lublin, PL
P1-G-271-MO
Planar Chromatography with Different Detection Techniques: the Ultrafast
Quantitation of 5-Hydroxymethylfurfural in Honey
Elena S. Chernetsova1,2, Gertrud E. Morlock3
1
Russian Research Centre Kurchatov Institute, Moscow, RUS; 2People’s Friendship
University of Russia, Moscow, RUS; 3University of Hohenheim, Stuttgart, D
P1-G-272-TU
Potential of OPLC System with Multi-Inlet/Outlet
Emil Mincsovics1,2
1
OPLC-NIT Ltd., Budapest, H; 2Corvinus University, Budapest, H
P1-G-273-MO
The Investigations of the Chromatographic Properties of Selected d- and 4f-electron
Ion Element Complexes with Organic Ligands by TLC and Magneto-TLC methods
I. Malinowska, W. Ferenc, A. Wronka
Maria Curie-Skłodowska University, Lublin, PL
P1-G-274-TU
TLC of Some 1,3,4 – Thiadiazole Derivatives in Magnetic Field
M. Studziński1, I. Malinowska1, H. Malinowski2
1
Maria Curie-Skłodowska University, Lublin, PL;
2
Joint Institute For Nuclear Research, Dubna, RUS
100
Proteomics, Metabolomics, Glycomics
P1-G-275-MO
A Modified SVM Method for Analyzing Metabonomics Data from HPLC-MS
Xiaohui Lin1, Qiang Ruan1, Kang Yan1, Shili Chen2, Xinjie Zhao2, Yang Zhang1, Guowang Xu2
1
Dalian University of Technology, Dalian, PRC;
2
P1-G-276-TU
A New High Capacity MALDI Target Format for Improved LC-MALDI Analysis of
Complex Proteomics Samples
Zoltan Czentnar, Arndt Asperger, Martin Schuerenberg, Andrea Kiehne, Detlev Suckau,
Marcus Macht
P1-G-277-MO
An Improved NanoLC/MS/MS Ion Trap Setup for the Identification of 800 Proteins
from a Cell Line Lysate
Andrea Schneider, Andrea Kiehne, Markus Meyer, Arnd Ingendoh
P1-G-278-TU
Analysis of Single Amino Acid Mutations in Intact Proteins
H. J. Wirth1, D. Steer2, X. Yan3, T. Bannam3, J. Rood3, A. Gooley1
1
SGE Analytical Science, Ringwood, Vic., AUS; 2,3Monash University, Clayton, Vic., AUS
P1-G-279-MO
Characterization of the In Vitro and In Vivo Metabolites of the Novel
Thiosemicarbazone Anti-tumour Agents using HPLC-MS/MS
Jan Stariat1, Petra Kovarikova1, Milan Nobilis1, Vit Sestak1, Zuzana Kollarova1,
Jiri Klimes1, R. Des Richardson2
1
Charles University in Prague, Hradec Králové, CZ; 2University of Sydney, Sydney, AUS
P1-G-280-TU
Chromatographic Separation of Phosphorylated Neuropeptides by Applying
3D-ERLIC-HILIC-Reversed Phase Separation. Evaluation of Separation Conditions
Goran Mitulović, Verena Tretter
P1-G-281-MO
Comparison of Glycoprotein Enrichment Methods on Human Plasma Samples
Lilla Turiák, Oliver Ozohanics, Lászlo Drahos, Károly Vékey
101
P1-G-282-TU
Comparison of Microparticulate and Monolithic Reversed-Phase Columns for HPLC
Analysis of Tryptic Digests from Industrial Enzymes in Cleaning Products
Miriam Beneito-Cambra1, José Manuel Herrero-Martínez1, Guillermo Ramis-Ramos1,
Wolfgang Lindner2, Michael Lämmerhofer2
1
University of Valencia, Valencia, E; 2University of Vienna, Vienna, A
P1-G-283-MO
Data Mining of an Untargeted LCMS Metabolomics Study Performed using Aqueous
Compatible Reverse Phase Column
Syed Salman Lateef1, Sudha Rajagopalan1, Siji Joseph1, Nilanjan Guha1,
Yugandhar Reddy1, Michael Frank2
1
Agilent Technologies India Pvt. Ltd, Bangalore, IND;
2
Agilent Technologies Ltd, Waldbronn, D
P1-G-284-TU
Development of an Immunoaffinity Sorbent for the Analysis of Opioid Peptides by
IA-SPE-CE-MS
Fernando Benavente, Silvia Medina-Casanellas, José Barbosa, Victoria Sanz-Nebot
P1-G-285-MO
Efficient In-Line Digestion Methods to Support LC-MS Workflows
K. Flook1, E. J. Sneekes2, Y. Agroskin1, R. Swart2, C. Pohl1
1
Dionex Corporation, Sunnyvale, CA, USA; 2Dionex Corporation, Amsterdam, NL
P1-G-286-TU
Evaluation of Engineered AMPs Production in Transgenic Plants by MRM
Esther Izquierdo Alegre1, Sonia Hem1, Claude Nespoulous1, Maria Montero2,
Maria Pla2, Michel Rossignol1
1
Laboratoire de Proteomique Fonctionnelle, Montpellier, F; 2Universitat de Girona, Girona, E
P1-G-287-MO
Evaluation of Fully Porous and Superficially Porous Particles in Metabolomics
Applications
Ruben t’Kindt1, Gerd Vanhoenacker2, Frank David2, Pat Sandra2, Koen Sandra1
1
Metablys, Kortrijk, B; 2Research Institute for Chromatography, Kortrijk, B
P1-G-288-TU
Identification and Characterization of Wheat High-Molecular-Weight Glutenin Subunits
by Dynamic Capillary Isoelectric Focusing
Boleslaw P. Salmanowicz
Institute of Plant Genetics, Polish Academy of Sciences, Poznan, PL
102
P1-G-289-MO
Improving Quality to Improve Throughput in Quantitative Neurotransmitter Analysis
David P. Budac, Xu Zhang, Mark J. Hayward
Lundbeck Research USA, Paramus, NJ, USA
P1-G-290-TU
Integration of Protein Digestion Microreactors in a Comprehensive Two-Dimensional
Liquid Chromatography System
Filippo Bedani, Huiming Yuan, Lihua Zhang, Yukui Zhang
Dalian Institute of Chemical Physics, Chinese Academy of Science, Dalian, PRC
P1-G-292-TU
Metabolomic Approach with LC-QTOF-MS to Investigate Plasma Samples from
Patients with Abdominal Aortic Aneurysm
Joanna Teul1,2, Francisco Javier Rupérez2, Michal Ciborowski2,3,
Jose Luis Martin-Ventura4,5, Jesus Egido4,5, Coral Barbas2
1,3
Medical University in Bialystok, Bialystok, PL; 2San Pablo-CEU University, Madrid, E;
4
Fundacion Jimenez Diaz, Madrid, E; 5Autonoma University, Madrid, E
P1-G-294-TU
Monolithic Silica Based Columns for Fast Peptide Separations in Proteomics
Magnus Røgeberg1, Steven Ray Wilson1, Helle Malerød1, Elsa Lundanes1,
Nobuo Tanaka2, Tyge Greibrokk1
1
University of Oslo, Oslo, N; 2Kyoto Institute of Technology, Kyoto, J
P1-G-295-MO
N-Glycosylation of Antibodies Characterized by LC-MALDI in an Integrated Software
Approach
Zoltan Czentnar, Ulrike Schweiger-Hufnagel, Arndt Asperger, Anja Resemann,
Detlev Suckau
P1-G-296-TU
Non-Invasive Assessment of Embryo Viability in Assisted Reproduction using Capillary
Electrophoresis
Ales Madr1, Katerina Foltova1, Jana Zakova2, Eva Lousova2, Igor Crha2, Zdenek Glatz1
1
Masaryk University, Brno, CZ; 2Centre of Assisted Reproduction, Brno, CZ
P1-G-297-MO
Novel Aqueous Two-Phase Systems for Extraction of Biomolecules
Morteza G. Khaledi, Samuel I. Jenkins, Christopher Collins, Mahboubeh Nejati,
Nathaniel Weisner, Shuang Liang
North Carolina State University, Raleigh, NC, USA
103
P1-G-298-TU
On the Specificity of Selected Reaction Monitoring Coupled with Chromatographic
Separations for Proteomic Studies
Konstantinos Petritis, Ashoka Polpitiya, Jian Liu
The Translational Genomics Research Institute (TGen), Phoenix, Arizona, USA
P1-G-299-MO
Optimizing Particle Size and Column Length, what is the Best Way to Utilize Nano
UHPLC in Proteomics?
W. Decrop1, E. J. Sneekes1, Thomas Köcher2, K. Dekker1, B. de Haan1, Karl Mechtler2,
R. Swart1
1
Dionex Corporation, Amsterdam, NL;
2
Research Institute of Molecular Pathology (IMP), Vienna, A
P1-G-300-TU
Phosphoglycolipid Profiling of Bacterial Endotoxins
Ágnes Dörnyei, Anikó Kilár, Viktor Sándor, Béla Kocsis, Ferenc Kilár
P1-G-301-MO
Evaluating Accelerating Methods for Trypsin Digestion in LC-MS Based Proteomics
Helle Malerod, Hanne Kolsrud Hustoft, Steven Ray Wilson, Jan Leo Reubsaet,
Elsa Lundanes, Tyge Greibrokk
University of Oslo, Oslo, N
P1-G-302-TU
Selectivity of Mixed-Mode Chromatography for Structural Isomers of Phosphorylated
Carbohydrate Metabolites
H. Hinterwirth, A. Gargano, M. Lämmerhofer, W. Lindner
P1-G-303-MO
Study on a Rapid and Highly Selective Colorimetric Method for the Detection of
Tryptophan in a Mixture of Amino Acids using Liquid Chromatography-Mass
Spectrometry
Yanyan Huang, Guoquan Liu, Rui Zhao
Institute of Chemistry, Chinese Academy of Sciences, Beijing, PRC
P1-G-304-TU
The Hormonome of Developing Wheat and Bean Seeds as Revealed by LC/MS
Petre I. Dobrev1, Marie Trčková2, Miroslav Kamínek1
1
Institute of Experimental Botany AS CR v.v.i., Prague, CZ;
2
Crop Research Institute, Prague, CZ
104
P1-G-305-MO
The New Panacea in Metabolomics, Proteomics and Genomics –
Electrochemistry / MS
Jean-Pierre Chervet1, Agnieszka Kraj1, Martin Eysberg1; Herbert Oberacher2
1
Antec, Zoeterwoude, NL;
2
Innsbruck Medical University, Innsbruck, A
P1-G-306-TU
Top-Down LC-MALDI Identification of Protein in Mixtures of Moderate Complexity and
N- and C-terminal Assignments
Sven Meyer1, Andrea Kiehne1, Anja Resemann1, Shannon Cornett2, Eckhardt Belau1,
Detlev Suckau1
1
2
Bruker Daltonics Inc., Fairview, TN, USA
P1-G-307-MO
Two Dimensional SEC // RP Capillary LC for Top-Down Proteomics Analysis
Evert-Jan Sneekes, Macro Karsten, Wim Decrop, Remco Swart
Dionex Corporation, Amsterdam, NL
P1-G-308-TU
UHR-Q-TOF Analysis can Address Common Challenges in Targeted and Untargeted
Metabolomics
Zoltan Czentnar1, Aiko Barsch1, G. Zurek1, D. Krug2, R. Müller2
1
Bruker Daltonics, Bremen, D;
2
Universität des Saarlandes, Saarbrücken, D
P1-G-309-MO
Urinary Metabolic Profiling Analysis to Discover Potential Diagnostic Biomarkers
Based on LTQ-Orbitrap High Resolution Mass Spectrometry
Lina Zhou, Peiyuan Yin, Xin Lu, Guowang Xu
P1-G-310-TU
The Use of Dual cHiPLC Columns to Increase Throughput in Quantitative Peptide
MRM Analyses
J. Bryce Young, Nicole Hebert, Erika Lin, Remco van Soest
P1-G-311-MO
On-Line cHiPLC Based Digestion in NanoLC-MS for Increased Reproducibility
Remco van Soest, J. Bryce Young, Don Arnold and Nicole Hebert
105
P1-G-312-TU
High Performance at Highest Speeds for Protein Identification in Complex Matrices
Christie L. Hunter1, Sean L Seymour1, Doug Simmons2, Matthias Glueckmann3,
Thomas Knapman3, Henri Snijders3
1
AB SCIEX, USA; 2AB SCIEX, Canada; 3AB SCIEX, Europe
Ultra-High Pressure LC
P1-G-313-MO
Application of Modern Stationary Phases for Determination of Retinol and
α-tocopherol in Biological Material by UHPLC
Barbora Kučerová1,2, Lenka Krčmova1,2, Jiří Pliišek1,2, Markéta Kašparová1,2,
Dagmar Solichová2, Petr Solich1
1
Charles University, Hradec Králové, CZ; 2Teaching Hospital, Hradec Králové, CZ
P1-G-314-TU
Application of Whelk O-1 and DACH-DNB Selectors on Sub-2 Micron Particles for
Enantioselective UHPLC Separations in the Ultra-Fast Regime
Alessia Ciogli1, Ilaria D’Acquarica1, Francesco Gasparrini1, Carmela Molinaro1,
Marco Pierini1, Claudio Villani1, Jelena Kocergin2, Ted Szczerba2, Harald Ritchie3
1
Sapienza Università di Roma, Rome, I;
2
Regis Technologies, Inc., Morton Grove, IL, USA;
3
Thermo Fisher Scientific, Runcorn, UK
P1-G-315-MO
Characterization of System Dispersion and its Impact on Chromatographic
Separations
Aparna Chavali, Peyton Beals, Richard W. Andrews, Tanya Jenkins, Patricia McConville
P1-G-316-TU
Chromatographic Time Scale Transition from Minutes to Seconds in Chiral UHPLC
with the Sub-2 Micron Whelk O-1 Stationary Phase
Alessia Ciogli1, Ilaria D’Acquarica1, Francesco Gasparrini1, Carmela Molinaro1,
Claudio Villani1, Jelena Kocergin2, Ted Szczerba2, Harald Ritchie3
1
Sapienza Università di Roma, Rome, I; 2Regis Technologies, Inc., Morton Grove, IL, USA;
3
P1-G-317-MO
Comparative Study of Different UHPLC Systems by Kinetic Plot Method
Judit Orgoványi, Erzsébet Oláh, János Horváth, Mónika Babják
106
P1-G-318-TU
Development and Validation of a UHPLC-UV Method for the Detection and Quantification of
Erectile Dysfunction Drugs and Some of their Analogues Found in Counterfeit Medicines
Pierre-Yves Sacré1,2, Eric Deconinck1, Patrice Chiap3, Jacques Crommen2, Eric Rozet4,
Patricia Courselle1, Jacques O. De Beer1
1
Scientific Institute of Public Health, Brussels, B; 2,4University of Liège, Liège, B;
3
University Hospital of Liège, Liège, B
P1-G-319-MO
Enhanced Stationary Phase Selectivity for UHPLC Separations Based upon a
Core-Shell Technology
Jason A. Anspach, Lawrence Y. Loo, Thuylinh Tran, A. Carl Sanchez, Tivadar Farkas
Phenomenex, Torrance, CA, USA
P1-G-320-TU
Fast LC Method Optimisation using Kinetic Plots
L. Pereira, T. Edge, H. Ritchie, S. Luke, D. Milton
P1-G-321-MO
High Throughput Analysis of Model Drugs by Combining Ultra High Pressure and High
Temperature Chromatography using 1 mm ID Columns
Thorsten Teutenberg, Steffen Wiese, Paul Ermisch
Institut für Energie- und Umwelttechnik e. V., Duisburg, D
P1-G-322-TU
Intelligent System Emulation: Achieving Method Compatibility between HPLC and UHPLC
Monika M. Dittmann, Heike Otero-Martinez, Konstantin Choikhet, Klaus Witt,
Gerhart Metzler
Agilent Technologies GmbH, Waldbronn, D
P1-G-323-MO
Method Transfer from HPLC to Ultra Performance Liquid Chromatography (UPLCTM):
Biogenic Amines in Different Cheese Varieties
H. K. Mayer, G. Fiechter
BOKU – University of Natural Resources and Life Sciences Vienna, Vienna, A
P1-G-324-TU
New Technologies with UHPLC Improve Method Development and Chromatographic
Results
Anne Mack1, Maureen Joseph1, William Long1, Linda Lloyd2
1
Agilent Technologies, Wilmington, DE, USA;
2
Agilent Technologies UK Limited, Church Stretton, UK
107
P1-G-325-MO
The Effect of Frictional Heating under Practical UHPLC Conditions
Lucie Nováková1, Jean Luc Veuthey2, Davy Guillarme2
1
2
P1-G-326-TU
Quantitative Analysis of Catechins in Tea by UHPLC/UV
Guifeng Jiang, Terry Zhang
P1-G-327-MO
There are Problems Associated with Gradient and Method Transfer among HPLC, and
UHPLC, Systems and Columns – are there Explanations and Usable Workarounds?
Michael Woodman, Lori Sandford
Agilent Technologies, Wilmington, DE, USA
P1-G-328-TU
UHPLC Considerations – Demands for Ultra Pure Solvents, Additives and New Testing
Methods
Rudolf Köhling
Sigma-Aldrich Production GmbH, Buchs, CH
P1-G-329-MO
UHPLC – MS of Clinical Relevant Compounds using a New Type of 2 μm Silica
Particles
Michael Schulz, Anita Piper, Petra Lewits, Karin Cabrera
P1-G-330-TU
Ultra-Fast LC Analysis of Complex Samples at UHPLC Conditions
Matthias Pursch, Romina Hammes
Dow Deutschland Anlagengesellschaft mbH, Rheinmünster, D
P1-G-331-MO
Utilizing Extended Linear Velocity to Maximize Peak Capacity in Ultra-High Power
Chromatography
Dawn Stickle1, Goran Rasched2, Bob Giuffre2, Dat-Phan3
1
Agilent Technologies, Andover, MA, USA;
2
Agilent Technologies, Budd Lake, NJ, USA;
3
Agilent Technologies, Columbia, MD, USA
108
Biomarker Discovery
P1-S-332-TU
A Linkage Application of Multi-Dimensional Chromatography, Solid-Phase Peptide
Ligand Library, Two-Dimensional Difference Gel Electrophoresis and Mass
Spectrometry towards Plasma Biomarker Development
Tatsuo Hagiwara1,2, Yumi Saito1, Yasufumi Murakami2, Tadashi Kondo1
1
National Cancer Center Research Institute, Tokyo, J;
2
Tokyo University of Science, Tokyo, J
P1-S-333-MO
Analysis of the Altered Glycosylation of IgG1 in Rheumatoid Arthritis by Capillary
Electrophoresis
Csaba Váradi, Stefan Mittermayr, Márta Kerékgyártó, Bertalan Meskó
P1-S-334-TU
Ceramide Profiling in Skin using LC-QTOF-MS
Ruben t’Kindt1, Lucie Jorge1, Emmie Dumont2, Pauline Couturon3, Frank David2,
Pat Sandra2, Koen Sandra1
1
Metablys, Kortrijk, B;
2
3
Katholieke Universiteit Leuven, Heverlee, B
P1-S-336-TU
Determination of Acrylamide Metabolites in Urine by LC-MS/MS Technique
Krystyna Tyrpień, Magdalena Szumska
Silesian Medical University in Katowice, Zabrze, PL
P1-S-337-MO
Determination of Galanin Family Peptides in LC-MS Method using Fused-Core
Technology
François Mansion, Jacques Crommen, Anne-Catherine Servais, Marianne Fillet
P1-S-338-TU
Fractionation of the Human Plasma Proteome for Monoclonal Antibody Proteomics
Based Biomarker Discovery
András Kovács1, Edit Sperling1, Stefan Mittermayr 1, József Lázár2, Attila Balogh 2,
János Kádas2, Ákos Szekrényes1, László Takács2, István Kurucz2
1
University of Debrecen, Debrecen, H;
2
BioSystems International Ltd., Debrecen, H
109
P1-S-339-MO
Glycosylation Profile of Haptoglobin Phenotypes in Normal and Cancer Patients
Ákos Szekrényes, Csaba Váradi, Márta Kerékgyártó, Stefan Mittermayr
P1-S-340-TU
High Sensitivity Protein Quantitation using a Triple Quadrupole with a Dual Ion Funnel
Christine Miller1, Yanan Yang1, Christian Gotenfels2, Keith Waddell1
1
Agilent Technologies, Santa Clara, CA, USA; 2Agilent Technologies, Waldbronn, D
P1-S-341-MO
HPLC-MS Method for Monitoring Aldehydic Oxidative Stress Markers in Human
Clinical Samples
Kamila Syslová1, Petr Kačer1, Marek Kuzma2, Beata Vilhanová2, Štěpánka Vlčková3,
Jindřiška Lebedová3, Zdeňka Fenclová3, Daniela Pelclová3
1
Institute of Cheical Technology, Prague, CZ; 2Institute of Microbiology, Prague, CZ;
3
Charles University, Prague, CZ
P1-S-342-TU
Levels of MDA Determined by HPLC in Patients with Leukemia
Matheus Sampaio Goveia, Pamella Cristina Scheel, Carlos Eduardo Coral de Oliveira,
Julie Massayo Maeda Oda, Maria Angélica Ehara Watanabe, Suzana Lucy Nixdorf
Universidade Estadual de Londrina, Londrina, BR
P1-S-343-MO
Optimization and Application of Microwave-Assisted Acid Hydrolysis for Rapid
Quantification of Protein Oxidation Markers using LC-MS
Somaieh Afiuni-Zadeh1,2, Xinghua Guo1, Gholamhassan Azimi2, Ernst Lankmayr1
1
Graz University of Technology, Graz, A; 2University of Arak, Arak, IR
P1-S-344-TU
Quantification of Reduced Glutathione (GSH) as Biomarker of Toxicity in
Reconstructed Human Skin Models
Eric Arbey, Guillaume Léreaux, Jean-Roch Meunier, Joan Eilstein, Daniel Duche
L’Oreal Research & Innovation, Aulnay-Sous-Bois, F
P1-S-345-MO
Synthesis and Analysis of Neoglycoproteins to Generate Carbohydrate Specific
Antibodies for Glycomics Based Biomarker Discovery
Márta Kerékgyártó1, Csaba Váradi1, Stefan Mittermayr1, Ákos Szekrényes1, Ildikó Olajos2,
István Kurucz3
1,2
3
Biosystems International Ltd., Debrecen, H
110
P1-S-346-TU
Universal Fluorescent Multiplex PCR and Capillary Electrophoresis for Evaluation of
Gene Conversion between SMN1/SMN2 in Spinal Muscular Atrophy
Shou-Mei Wu, Chun-Chi Wang
Kaohsiung Medical University, Kaohsiung, RC
Biopharmaceutical and Biomedical Analysis
P1-S-347-MO
A New HPLC Method for the Determination of Neopterin, Kynurenine, Tryptophan and
Creatinine in Exudates and Amniotic Fluid
Lenka Krčmová1,2, Dagmar Solichová2, Bohuslav Melichar3, Petr Solich1
1
2
University Hospital, Hradec Králové, CZ;
3
Palacký University Medical School, Olomouc, CZ
P1-S-348-TU
A Rapid and Precise HPLC-Based Lipase Assay
Astrid Wirtz1, Kathrin Klein1, Laura Schneider1, Martina Pohl2, Karl-Erich Jaeger1,
Ulrich Krauss1
1
Heinrich-Heine-Universität Düsseldorf, Jülich, D;
2
Institut für Bio- und Geowissenschaften, Jülich, D
P1-S-349-MO
Advantages of UPLC in Biopharmaceutical Analysis
Yajun Jennifer Wang, Jennifer Rea, Tony G. Moreno, Tomasz Baginski, Dell Farnan
Protein Analytical Chemistry, Genentech Inc., South San Francisco, CA, USA
P1-S-350-TU
Analysis of Antibiotics in Biological Fluids using Surfactant Mediated Mobile Phases
Maria Rambla-Alegre1, Julián Paños-Pérez2, Juan Peris-Vicente1,
Inmaculada Casas-Breva3, Devasish Bose4, Nitasha Agrawal4, Josep Esteve-Romero1,
Samuel Carda-Broch1
1,2
Universitat Jaume I, Castello, E;
3
Hospital La Plana, Vila-real, E;
4
Dr. H. S. Gour University, Sagar, IND
P1-S-351-MO
Analysis of Biocides with the PerkinElmer Flexar FX-15 System Equipped with a PDA
Detector
April DeAtley, Njies Pedjie
PerkinElmer, Shelton, CT, USA
111
P1-S-352-TU
Analysis of Lidocaine and its Metabolite in Plasma Samples of Parturient Women with
Gestational Diabetes Mellitus by In-Tube Solid Phase Microextraction Coupled to
Liquid Chromatography (In-Tube SPME/LC)
Bruno José Gonçalves da Silva, Juciene Aparecida Caris, Vera Lúcia Lanchote,
Maria Eugênia Costa Queiroz
Universidade de São Paulo, Ribeirão Preto, BR
P1-S-353-MO
Analysis of Protein Primary Structure using Wide Pore Sub 2 μm Particles and
UHPLC
Phu T. Duong1, Brian A. Bidlingmeyer1, Linda L. Lloyd2
1
2
P1-S-355-MO
Boronate Functionalised Polymer Monoliths for Identification of New Biomarkers in
Type II Diabetes Mellitus
Anikó Takátsy
P1-S-356-TU
By-Products in Recombinant TAU Protein Production Characterized by LC-MALDI
Top-Down Sequencing (LC-MALDI-TDS)
Sven Meyer1, Arndt Asperger1, Marcus Macht1, Verena Tellsroem1, Branislav Kovacech2,
Andrej Kovac2
1
2
Inst. of Neuroimmunol., Slovak Academy of Sciences, Bratislava, SK
P1-S-357-MO
Carbon Nanotubes as a Gene Delivery Vehicle for Plant Cell Transfection
Maged F. Serag1, Noritada Kaji2, Yukihiro Okamoto1, Manabu Tokeshi1,
Yoshinobu Baba1,3
1,2
Nagoya University, Nagoya, J;
3
National Institute of Advanced Industrial Science and Technology (AIST), Takamatsu, J
P1-S-358-TU
Characterization of a Therapeutic Protein by Optimized Peptide Mapping, SEC and IEX
Srividya Kailasam1, Siji Joseph1, Angelika Gratzfeld-Huesgen2
1
Agilent Technologies India Pvt. Ltd., Bangalore, IND;
2
Agilent Technologies Waldbronn, Waldbronn, D
112
P1-S-359-MO
Characterization of Amino Acid Profiles of Culture Media using Ultra Performance
Liquid Chromatography, AQC Pre-Column Derivatization and UV Detection
Gregor Fiechter, Helmut K. Mayer
University of Natural Resources & Life Sciences Vienna, Vienna, A
P1-S-360-TU
Characterization of Praziquantel and its Metabolites by Ultra-Performance Liquid
Chromatography Coupled with Electrospray Tandem Mass Spectrometry
Veronika Jedličková1, Robert Jirásko1, Michal Holčapek1, Ivan Vokřál2, Lenka Skálová2
1
University of Pardubice, Pardubice, CZ; 2Charles University, Hradec Králové, CZ
P1-S-361-MO
Chromatographic Determination of the Antimalarial Alpha-Beta Arteether
Josep Esteve-Romero1, Samuel Carda-Broch1, Maria Rambla-Alegre1,
Adrián Martinavarro-Domínguez1, Juan Péris-Vicente1, Devasish Bose2,
Abhilasha Durgbanshi3, Nitasha Agrawal2
1
Universitat Jaume I, Castello, E; 2Dr. Harisingh Gour University, Sagar, IND;
3
Banaras Hindu University, Varanasi, IND
P1-S-362-TU
Comparative Glycomics: Rapid and Confident IgG Structural Elucidation using a
Multidimensional Liquid Phase Separation Approach
Stefan Mittermayr1,2, Jonathan Bones1, Margaret Doherty1, Pauline M. Rudd1
1
University College Dublin, Dublin, IRL; 2University of Debrecen, Debrecen, H
P1-S-363-MO
Comparison of Sialic Acid Determination in Glycoproteins: Two Liquid Chromatography
Methods
Deanna C. Hurum, Jeffrey S. Rohrer
P1-S-364-TU
C-terminal Processing Proteases from Pseudomonas Aeruginosa Cleave
Penicillin-Binding Proteins In Vitro
Astrid Wirtz1, Beatrix Santiago-Schübel2, Rien Hoge1,3, Frank Rosenau4, Diana Hofmann2
1
Heinrich-Heine-Universität Düsseldorf, Düsseldorf, D; 2Forschungszentrum Jülich GmbH,
Jülich, D; 3Deventer Hospital, Deventer, NL; 4Universität Ulm, Ulm, D
P1-S-365-MO
Defining the Optimum Parameters for Efficient Size Separations of Proteins
Linda Lloyd, Keeley Mapp
113
P1-S-366-TU
Determination of Benzophenones in Human Placental Tissue Samples by Liquid
Chromatography-Tandem Mass Spectrometry
Inmaculada Jiménez-Díaz, Fernando Vela-Soria, Rocío Rodríguez-Gómez,
Óscar Ballesteros, Alberto Zafra-Gómez, Alberto Navalón, Maria Fátima Fernández,
Nicolás Olea
P1-S-367-MO
Determination of Citrulline in Human Plasma Samples using a RP-HPLC Method
Agustín Acquaviva, Lílian Romero, Cecilia Castells
Universidad Nacional de La Plata, La Plata, Buenos Aires, RA
P1-S-369-MO
Determination of Parabens in Human Placental Tissue Samples by Liquid
Inmaculada Jiménez-Díaz, Fernando Vela-Soria, Óscar Ballesteros, Alberto Zafra-Gómez,
Alberto Navalón, Maria Fátima Fernández, Nicolás Olea
P1-S-370-TU
Determination of Phytochemical Compounds in Longan-Flower-Water-Extract
(Dimocarpus Longans Lour.) by HPLC and its Protection against Non-Alcoholic
Steatohepatitis
Jung-Kai Tseng1, Yi-Chen Chen2, Deng-Jye Yang3, Chin-Lin Hsu4
1,3,4
Chung-Shan Medical University, Taichung, RC;
2
National Taiwan University, Taipei, RC
P1-S-371-MO
Determination of Some Banned Aromatic Amines in Waste using Micellar Liquid
Chromatography
Sandeep Kumar Moury1, Swati Dubey1, Devasish Bose1, Abhilasha Durgbanshi2,
Josep Esteve-Romero3, Samuel Carda-Broch3, Maria Rambla Alegre3,
Monica-Ana Raviolo4
1
Dr. H.S.Gour University, Sagar, IND;
2
Banaras Hindu University, Vanarasi, IND;
3
4
Universidad de Córdoba, Córdoba, RA
P1-S-372-TU
Determination of Pteridines and Hidropteridines in Human Urine by HPLC-MS
Ana Jiménez Girón, Isabel Durán Martín-Merás, Anunciación Espinosa Mansilla
University of Extremadura, Badajoz, E
114
P1-S-373-MO
Development and Validation of a Novel HPLC Method for the Dose Formulation
Analysis of Parathyroid Hormone and an Analog in Saline
G. Wallace1, R. O’Rielly1, A. Bartlett1, G. Hattersley2
1
Charles River Laboratories, Preclinical Services, Seneville (Montreal), Quebec, CDN;
2
Radius Health, Inc., Cambridge, MA, USA
P1-S-374-TU
Development and Validation of Method for Retinol and α-Tocopherol Analysis in Breast
Milk by HPLC-DAD using Core-Shell Technology
Jiří Plíšek1,2, Markéta Kašparová1,2, Hana Vlčková1, Barbora Kučerová1,2,
Lenka Krčmová1,2, Dagmar Solichová2, Petr Solich1
1
2
Teaching Hospital, Hradec Králové, CZ
P1-S-375-MO
Development and Validation of Micellar Liquid Chromatographic Method for
Lamivudine and Derivatives
María S. Gualdesi1, Mónica A. Raviolo1, Josep Esteve-Romero2, Margarita C. Briñón1
1
Universidad Nacional Córdoba, Córdoba, RA;
2
Universidad Jaume I, Castello, E
P1-S-376-TU
Development of a Glycan Database For Waters Ultra Performance Liquid
Chromatography (UPLC)
Mark Hilliard, Weston Struwe, Barbara Adamczyk, Pauline M. Rudd
National Institute for Bioprocessing Research and Training (NIBRT), Dublin, IRL
P1-S-377-MO
Development of a Sphingomyelin Biomimetic Stationary Phase for Immobilized Artificial
Membrane (IAM) Chromatography
Dieter Verzele 1, Frédéric Lynen 1, Adrian G. Wright2, Melissa Hanna-Brown2,
Pat Sandra1
1
Pfizer Analytical Research Centre, Ghent University, Gent, Belgium;
2
Pfizer European R&D Headquarters, Sandwich, UK
P1-S-378-TU
Development of an HPLC Method to Quantify an Immunostimulant in an
Emulsion-Based Vaccine Adjuvant
J.-F. Cotte1, M. Raphat1, A. Debreyer1, F. Dalencon1, P Talaga1, J. Haensler1,
O. Adam1, K. Johnson2
1
Research Department, Sanofi Pasteur, Marcy l’Etoile, F;
2
3M Drug Delivery Systems Division, St. Paul, MN, USA
115
P1-S-380-TU
Direct UPLC-ESI-MS/MS Method of Brain Microdialysates: Rapid and Easy Method
for Neurotransmitters and their Metabolites Monitoring
Petr Kačer1, Kamila Syslova1,2, Věra Najmanová1, Lukáš Rambousek1,3,4, Marek Kuzma2,
Věra Bubeníková-Valešová3, Romana Šlamberová5
1
Institute of Chemical Technology, Prague, CZ;
2
Institute of Microbiology, Prague, CZ;
3
Prague Psychiatric Center, Prague, CZ;
4
Institute of Physiology, Prague, CZ;
5
P1-S-381-MO
Efficient Use of pH Gradients in the Ion Exchange Analysis of Proteins
Thomas E. Wheat, Daniel S. Root, Patricia R. McConville
P1-S-382-TU
A New UHPLC Column for Polar Analyte Retention
Fortis Technologies Ltd, Neston, UK
P1-S-383-MO
Evaluation of Size Exclusion Chromatography Packing Materials for the Analysis of
Proteins and Higher Order Aggregates
Paula Hong, Edouard S. P. Bouvier, Kenneth J. Fountain
P1-S-384-TU
Exploration of pH Gradient Ion-Exchange Chromatography for High Resolution Protein
Separations in Biotechnology and Proteomics
Wim Decrop, Marie-Jeanne Olivo, Evert-Jan Sneekes, Remco Swart
P1-S-385-MO
Forming Highly Accurate pH- and Salt-Gradients for Biomolecules Separation using
First Principle Calculations
Vlastimil Hruska1, Bohuslav Gas 1, Uwe Effelsberg2, Jochen Strassner2,
Tom van deGoor2
1
Charles University Prague, Prague, CZ;
2
116
P1-S-386-TU
Functionalised Polymeric Monolithic Sheets for Dried Blood and Plasma Spotting
Anna Nordborg1, Esme Candish1, Pavel N. Nesterenko1, Greg W. Dicinoski1,
Graeme Clark2, Paul R. Haddad1, Emily F. Hilder1
1
Pfizer Analytical Research Centre (PARC), Australian Centre for Research on Separation
Science (ACROSS), School of Chemistry University of Tasmania, Hobart, AUS;
2
Pfizer Global Research & Development, Sandwich, UK
P1-S-387-MO
Glycopeptide Analysis by Capillary Electrophoresis – QTOF – Mass Spectrometry
Suresh Babu CV1, Ravindra Gudihal1, Syed Salman Lateef1, Ning Tang2, Tobias Preckel3,
Martin Greiner3, Stephan Buckenmaier3
1
2
Agilent Technologies, Santa Clara, CA, USA;
3
Agilent Technologies R&D and Mktg. GmbH & Co.KG, Waldbronn, D
P1-S-388-TU
High Throughput Determination of Levonorgestrel in Human Plasma using a Sensitive
LC-MS/MS Method
Cédric Hubert1, Bruno Streel2, Renilde Sibenaler3, Joëlle Widart4, Attilio Ceccato5,
Philippe Hubert1
1,4
University of Liège, Liège, B;
2
Galephar, Marche-en-Famenne, B;
3
SMB Laboratories, Bruxelles, B;
5
Odyssea Pharma, Grâce-Hollogne, B
P1-S-390-TU
Hydrophilic Interaction Liquid Chromatography Coupled to Mass Spectrometry for the
Separation of Dalargin and Structurally Related Enkephalins
Ayat Abbood1, Christine Herrenknecht2, Rana Alsalim1, Myriam Taverna1, Claire Smadja1
1
Université Paris-Sud, Chatenay-Malabry, F; 2Université de Nantes, Nantes, F
P1-S-391-MO
Identification and Characterization of Tetracosactide Impurities by CE and RP-HPLC
Coupled to TOF MS
Angelina Taichrib1, Gerhard K. E. Scriba2, Christian Neusüß1
1
Aalen University, Aalen, D; 2Friedrich Schiller University of Jena, Jena, D
P1-S-392-TU
Internal Standard Addition for Dried Blood Spot Analysis based on Flow Through
Desorption Solid-Phase Extraction and Mass Spectrometry
Lena Knegt, Bert Ooms, Emile Koster
Spark Holland, Emmen, NL
117
P1-S-394-TU
Laboratory Diagnostics of Adenosindeaminase (ADA) Deficiency by HPLC
J. Bártl, P. Hornik, J. Krijt, S. Šťastná, I. Šebesta
P1-S-395-MO
Liquid Chromatographic Method for Simultaneous Determination of Fungicides in
Seeds, Fungicide Formulations, Plant Material, Soil and Water Samples
Sandeep Kumar Moury1, Devasish Bose1, Abhilasha Durgbanshi2, Josep Esteve-Romero3,
Samuel Carda-Broch3, Maria Rambla-Alegre3, Sergio Marco-Peiró3, Monica-Ana Raviolo4
1
Dr. H. S. Gour University, Sagar, IND; 2Banaras Hindu University, Vanarasi, IND;
3
Universitat Jaume I, Castello, E; 4Universidad de Córdoba, RA
P1-S-396-TU
Micellar Liquid Cromatography in Bioanalytical Chemistry
Josep Esteve-Romero1, Samuel Carda-Broch1, Maria Rambla-Alegre1, Mei-Liang Chin-Chen1,
Mónica-Ana Raviolo2, Devasish Bose3, Abhilasha Durgbanshi4, Inmaculada Casas-Breva5
1
Universitat Jaume I, Castello, E; 2Universidad Nacional Córdoba, Córdoba, RA;
3
Dr. H. S. Gour University, Sagar, IND; 4Banaras Hindu University, Vanarasi, IND;
5
Hospital la Plana, Vila-real, E
P1-S-397-MO
Mobile Phase Considerations for Improved LC-MS Amenable Peptide Separations
Anders Fridstrom1, Hillel K. Brandes2, David S. Bell2, Craig R. Aurand2
1
Sigma-Aldrich Chemie GmbH, Buchs, CH; 2Sigma-Aldrich/Supelco, Bellefonte, PA, USA
P1-S-398-TU
Newly Developed Two Types of Packing Materials Based on Organic/Inorganic Hybrid
Silica and High-Strength Silica for Preparative HPLC of Peptides and Proteins
Takashi Sato, Noriko Shoji, Chie Yamashita, Takatomo Takai, Masakatsu Omote,
Naohiro Kuriyama
YMC Co., Ltd., Ishikawa, J
P1-S-399-MO
Novel Derivatives of Lamivudine. Stability Studies in Different Matrices
María S. Gualdesi1, Mónica A. Raviolo1, Josep Esteve-Romero2, Margarita C. Briñón1
1
Universidad Nacional Córdoba, Córdoba, RA; 2Universidad Jaume I, Castello, E
P1-S-400-TU
On-line Simultaneous Analysis of Negative Charged and Positive Charged Analytes by
Capillary Electrophoresis with FASI-Sweeping and its Applications
Shao-Yun Wei, Su-Hwei Chen
118
P1-S-401-MO
Optimization of Analytical Conditions for Amino Acids in Urine by CE-LIF
Mª Paz Lorenzo, Carmen Fernández, Coral Barbas, Antonia García
San Pablo-CEU University, Madrid, E
P1-S-402-TU
Optimization of Monoclonal Antibody Separation Conditions on Size Exclusion
Chromatography
Hiroyuki Moriyama, Hiroyuki Yamasaki, Michiko Sakata
TOSOH Corporation, Yamaguchi, J
P1-S-403-MO
Optimization of Protein Separations on Weak Cation Exchange Columns – a Study of
Particle Size, Buffer Salts and Gradients
Faizy Ahmed1,2, Christina Song2, Jennifer Palladino2, Taegen Clary1
1
Agilent Technologies, Santa Clara, CA, USA; 2University California Irvine, Irvine, CA, USA
P1-S-404-TU
Performance Characteristics of Commercially Available Gels for Protein Analysis by
Capillary Gel Electrophoresis with UV Detection
Christian Wenz, Rainer Nitsche, Hans Brunnert, Martin Greiner
Agilent Technologies R&D and Marketing GmbH & Co.KG, Waldbronn, D
P1-S-405-MO
Proline-Hydroxyproline Dipeptide Analysis using Barium Hydroxide and Barium Acetate
by High-Performance Anion-Exchange Chromatography Coupled with Pulsed
Amperometric Detection
Ha-Jeong Kwon, Hee-Jung Sim, Seon-Pyo Hong
P1-S-406-TU
Proteins and Peptides Separation with 2 μm Non-Porous High-Resolution ODS Column
Itaru Yazawa
Imtakt Corporation, Kyoto, J
P1-S-407-MO
Qualitative and Quantitative Determination of Brain Phospholipids by Reversed Phase
LC/MS(MS) Method
Róbert Berkecz1, Zoltán Kele1, Zoltán Szabó1, Heikki Tanila2, Daniel Michaelson3,
Tamás Janáky1
1
2
University of Eastern Finland, Kuopio, FIN;
3
Tel-Aviv University, Tel-Aviv, IL
119
P1-S-408-TU
Quality Control of Intact Biotherapeutics by High-Resolution LC/MS
Arnd Ingendoh, Dirk Wunderlich, Christian Albers
P1-S-410-TU
Reversed-Phase Performance Liquid Chromatographic Determination of Lipophilicity of
Potential Antitrypanosomal Compounds
Mónica A. Raviolo1, Margarita C. Briñón1, Maria Rambla-Alegrec, Samuel Carda-Broch2,
Adrián Martinavarro-Domínguez2, Josep Esteve-Romero2, Devasish Bose2
1
Universidad Nacional Córdoba, Córdoba, RA;
2
Universidad Jaume I, Castello, E
P1-S-411-MO
Separation of Peptides and RNA/DNA Fragments in 100% Aqueous Solution on
RPLC-Phases with Tuned Hydrophobicity
Joakim Högblom, Anders Törncrona, Maria Forsberg, Sylvia Winkel-Pettersson
Eka Chemicals AB, Bohus, S
P1-S-412-TU
Simultaneous Determination of Catecholamines from Rat Cerebrospinal Fluid by
High-Performance Liquid Chromatography with UV Detection
Min-Jung Gu, Hee-Jung Sim, Seon-Pyo Hong
P1-S-413-MO
Simultaneous Determination of Clarithromycin and Tobramycin in Different Plasma by
Sensitive LC-MS/MS
B. Cahay, B. Mertens, R. Klinkenberg, B. Streel
Galephar M/F, Marche-en-Famenne, B
P1-S-414-TU
Simultaneous Determination of Doxorubicin and Epirubicin in Plasma by Capillary
Electrophoresis with Field Amplified Sample Injection and its Application
Su-Hwei Chen, Ping-Chih Lin
P1-S-415-MO
Simultaneous Determination of Drugs in Human Autopsy Material
R. Oertel, J. Pietsch, N. Arenz, S. G. Zeitz, L. Goltz, W. Kirch
Technical University Dresden, Dresden, D
120
P1-S-416-TU
Strategies for Coupling of IEC and SEC to MS Detection for the Separation and
Characterization of Related Substances in Biopharmaceuticals
W. Decrop, E. J. Sneekes, R. Swart
P1-S-417-MO
Two-Dimensional Chromatography for Quantitation and MS Analysis of Monoclonal
Antibodies in Complex Samples
Sean M. McCarthy, Thomas E. Wheat, Ying Qing Yu, Jeff R. Mazzeo
Waters Corporation, Biopharmaceuticals, Milford, MA, USA
P1-S-418-TU
UHPLC/MS/MS Metabolites Characterization of Flubendazole
Robert Jirásko1, Michal Holčapek1, Veronika Jedličková1, Milan Nobilis2, Lenka Skálová2,
Jiří Lamka2
1
University of Pardubice, Pardubice, CZ; 2Charles University, Hradec Králové, CZ
Polymer Analysis
P1-S-419-MO
Analytical Study of a Resin used as Sealing Material in Ancient Pottery from
Archaeological Site by Light Microscopy, Vibrational Spectroscopy and Pyrolysis-Gas
Chromatography-Mass Spectrometry
J. Peris-Vicente1, L. Osete-Cortina2, F. M. Valle-Algarra3, M. A. Ferrer-Eres4,
J. V. Gimeno-Adelantado3, M. T. Doménech-Carbó2, R. Mateo-Castro3,
M. D. Soriano-Piñol3, M. Rambla-Alegre1, S. Carda-Broch1, J. Esteve-Romero1
1
Universitat Jaume I, Castello, E; 2Polytechnical University of Valencia, Valencia, E;
3,4
P1-S-420-TU
Chromatographic and Mass-Spectrometric Techniques for Characterizing
Carbene-Type Polymers
Petra Aarnoutse, Eva Reingruber, Erica Jellema, Markus Finger, Bas de Bruin,
Peter Schoenmakers
P1-S-421-MO
Deformation and Degradation of Polymers in Ultra-High-Pressure Liquid
Chromatography
Elena Uliyanchenko1, Sjoerd van der Wal1,2, Peter Schoenmakers1
1
University of Amsterdam, Amsterdam, NL; 2DSM Resolve, Geleen, NL
121
P1-S-422-TU
HPLC and SFC Analyses of Trimer Fatty Acids
John Kimmel, Lisa Zang, Sue D’Antonio
Column Technology and Stationary Phases
P2-G-423-WE
A Critical Comparison of Different Reversed-Phase/Cation-Exchange/Anion-Exchange
Trimodal Stationary Phases
Xiaodong Liu, Christopher A. Pohl
P2-G-424-TH
A New Phenyl-Type Stationary Phase and its Uses
Xiaodong Liu, Mark Tracy, Christopher Pohl
P2-G-425-WE
A New UHPLC Column for Polar Analyte Retention
P2-G-426-TH
A Novel Bonding Technique using a Polyfunctional Silyl-Reagent for Reversed-Phase
Liquid Chromatography – A new Approch II
Norikazu Nagae1, Anders Grahn2, Vinay D. Gaitonde2, Ralf Jutvik2
1
ChromaNik Technologies Inc., Osaka, J;
2
Biotech AB, Onsala, S
P2-G-427-WE
About the Separation of Sugars on Monolithic HPLC Columns
K. Cabrera, P. Knoell, G. Jung, A. Piper, K. Kreher, E. Machtejevas
P2-G-428-TH
Achieving Better and Faster Separations in UHPLC by Selecting Optimum Column
Technologies
Xiaoli Wang, Jason Link, Bill Barber
Agilent Technologies, Inc., Wilmington, DE, USA
122
P2-G-429-WE
Amino Acid Grafted Poly(glycidyl Methacrylate-co-ethylene Glycol Dimethacrylate)
Capillary Monoliths for Plasmid DNA Isoform Separation
A. Gargano, W. Lindner, M. Lämmerhofer
P2-G-430-TH
Amino-Coated Silica Gel Modified with Gold Nanoparticles as a Novel Stationary Phase
for HPLC
Yana Elfimova, Irina Ananieva, Artem Kuznetsov, Aleksandr Majouga, Oleg Shpigun
Lomonosov Moscow State University, Moscow, RUS
P2-G-431-WE
Amplification of Molecular Shape Selectivity with Self-assembled Molecular
Gel-immobilized Silica in Reversed-Phase HPLC
Makoto Takafuji, Thiraporn Charoenraks, Jin Izumi, Hiroataka Ihara
Kumamoto University, Kumamoto, J
P2-G-434-TH
Applications of New Monolithic Silica Capillaries with Various Dimensions and Surface
Modifications
Simon Forster, Sven Andrecht, Stephan Altmaier
P2-G-435-WE
Capillary Chelation Ion Chromatography and Extraction of Transition and Heavy Metals
using Iminodiacetic Acid (IDA) Modified Polymer Monoliths
Aine Moyna, Ekaterina Nesterenko, Damian Connolly, Brett Paull
Dublin City University, Dublin, IRL
P2-G-436-TH
Carbon and Polymer Monolith Focussed Ion Beam Serial Sectioning and Imaging for
3D Surface Reconstruction and Morphological Parameter Evaluation
Aymen BenAzouz, Xiaoyun He, Mercedes Vazquez, Ekaterina Nesterenko, David Collins,
Pavel N. Nesterenko, Brett Paull, Dermot Brabazon
P2-G-437-WE
Characterization and Evaluation of a Novel C18 Column Based on Organic/Inorganic
Hybrid Silica for HPLC and UHPLC
Takashi Sato, Noriko Shoji, Akiko Matsui, Mai Yamashita, Takatomo Takai,
Naohiro Kuriyama
123
P2-G-438-TH
Characterization of New Stationary Phases for HPLC Based on
Poly(methyoctadecylsiloxane) Thermally Immobilized onto Zirconized Silica
Carla Grazieli Azevedo da Silva, Carol H. Collins
University of Campinas (UNICAMP), Campinas, SP, BR
P2-G-439-WE
Cholesterol Bonded Phases for Liquid Chromatography
Szymon Bocian1, Maria Matyska2, Joseph Pesek2, Bogusław Buszewski1
1
Nicolaus Copernicus University, Torun, PL; 2San Jose State University, San Jose, CA, USA
P2-G-440-TH
Chromatographic Approaches for the Analysis of Polar Compounds
M. Dolci, B. Faulkner, L. Pereira, T. Edge
P2-G-441-WE
Chromatographic Performance of a Column Packed with Sub-1 μm Partially Porous
C18 Silica Particles
Elaine Stack, Jesse O. Omamogho, Jeremy D. Glennon
University College Cork, IRL
P2-G-442-TH
Chromatographic Properties of Novel Polymer Monolithic Column
Norio Ishizuka, Koji Furukawa
Emaus Kyoto Inc., Kyoto, J
P2-G-443-WE
Column Selectivity in Reversed-Phase LC using LC/MS Compatible Mobile Phases
William Long1, Anne Mack1, Maureen Joseph1, Linda Lloyd2
1
2
P2-G-444-TH
Comparison of the Kinetic Performance of Packed and Monolithic Columns in Gradient LC
Axel Vaast, Ken Broeckhoven, Gert Desmet, Sebastiaan Eeltink
P2-G-445-WE
Description of HILIC Properties of Hydrophobic Carbon-Coated Zirconia
Reversed-Phase Stationary Phase
Peter Kalafut, Radim Kučera, Jiří Klimeš
124
P2-G-446-TH
Design and Evaluation of a New Tweezers-Like Stable Stationary Phase for Hydrophilic
Interaction Chromatography-Mass Spectrometry (HILIC-MS)
Alessia Ciogli, Ilaria D’Acquarica, Francesco Gasparrini, Dorina Kotoni, Claudio Villani
Sapienza Università di Roma, Rome, I
P2-G-447-WE
Development of Novel Temperature-Responsive Chromatographic Stationary Phase
with Tunable the Aromatic Selectivity
Akari Nojima1, Ryosuke Kanazashi1, Tadashi Nishio1, Hideko Kanazawa1,
Kenichi Nagase2, Teruo Okano2
1
Keio University, Tokyo, J;
2
Tokyo Women’s Medical University, Tokyo, J
P2-G-448-TH
Development of Superficially Porous Silica with Polyfunctional C18 Bonding Technique
for Reversed Phase HPLC
Anders Grahn1, Norikazu Nagae2
1
Biotech AB, Onsala, S; 2ChromaNik Technologies Inc., Osaka, J
P2-G-449-WE
Evaluation of Incorporation of Silver Nanoparticles in Laurylmethacrylate Monoliths in
the Separation of Neutral Compounds by Capillary Electrochromatography
María Navarro Pascual-Ahuir, Alejandro Prieto Arnal, María Jesús Lerma-García,
Ernesto F. Simó-Alfonso, Guillermo Ramis-Ramos, José Manuel Herrero-Martínez
P2-G-450-TH
Evaluation of Some New Immobilized Stationary Phases. Part II: Effect of pH,
Temperature, Buffer Type and Buffer Concentration on Stability
Endler Marcel Borges, Carla Grazieli Azevedo da Silva, Carol H. Collins
University of Campinas (UNICAMP), Campinas, SP, BR
P2-G-451-WE
Evaluation of Sub-2 μm Silica and Hybrid Particles for SFC Applications
Christopher J. Hudalla, S. Collier, J. Fairchild, K.J. Fountain, J. Hill, P. Iraneta,
J. Jablonski
P2-G-452-TH
Expanding Selectivity in RP Separations using NUCLEODUR® PFP
Florian Taft, Markus John, Stephan Frech, Thomas Schuseler
MACHEREY-NAGEL GmbH & Co. KG, Düren, D
125
P2-G-453-WE
Experimental Investigation of the Difference in B-Term Dominated Band Broadening
between Fully Porous and Porous-shell Particles for Liquid Chromatography using the
Effective Medium Theory
Anuschka Liekens, G. Desmet
Vrije Universiteit Brussel, Brussel, B
P2-G-454-TH
Fabrication and Characterisation of Advanced Capillary-Scale Columns Incorporating
Immobilised Silica Nanoparticles for Potential HILIC or WAX Applications
Ali Alwy, Damian Connolly, Marcello Iacono, Andreas Heise, Brett Paull
P2-G-455-WE
Fabrication and Characterisation of Porous Graphitic Carbon Monoliths Using
C60-Fullerene Modified Silica Gel Templates
Xiaoyun He1, Ekaterina P. Nesterenko1, Lin Zhou2, Jeremy D. Glennon2,
Pavel N. Nesterenko3, Brett Paull1
1
Dublin City University, Dublin, IRL;
2
3
P2-G-456-TH
Fast Separation of Small Inorganic Anions using Methacrylate-Ester-based
Anion-Exchange Monolithic Column Prepared by Low Temperature UV
Photo-Polymerization
Mutsumi Takahashi, Tomohiko Hirano, Shinya Kitagawa, Hajime Ohtani
Nagoya Institute of Technology, Nagoya, J
P2-G-457-WE
Functionalization of Porous Graphitic Carbon with Improved Chromatographic
Characteristics
David Scott Jensen1, Vipul Gupta 1, Andrew Dadson2, Michael Vail 2,
Matthew R. Linford 1
1
2
US Synthetic Corporation, Orem, UT, USA
P2-G-458-TH
Geometric Isomer Selectivity of Emerging Stationary Phases
Catherine A. Rimmer, Jacolin A. Murray, Lane C. Sander
National Institute of Standards and Technology, Gaithersburg, MD, USA
126
P2-G-459-WE
High Performance Polymer-Based Monolithic Capillary Columns Prepared by γ-Ray
Triggered Polymerization: Influence of the Monomers and Cross-Linkers on the
Selective Separation of Small Molecules, Peptides and Proteins
Patrizia Simone1, Francesco Gasparrini1, Giuseppe Pierri1, Claudio Villani1,
Giancarlo Angelini2, Ornella Ursini2
1
Sapienza Università di Roma, Rome, I;
2
Istituto di Metodologie Chimiche, Monterotondo, I
P2-G-460-TH
High-Density Grafting of Polymer Brushes on Silica Particles under Supercritical CO2
and their Application in RP-HPLC
Hullathy Subban Ganapathy, Miyuki Doi, Makoto Takafuji, Hirotaka Ihara
P2-G-461-WE
High-Temperature Stability of Commercially Available HPLC Columns
Jakob Haun1, Thorsten Teutenberg1, Torsten C. Schmidt2
1
2
University of Duisburg-Essen, Essen, D
P2-G-462-TH
HILIC separation of Nucleoside Triphosphates with Temperature as a Separation
Parameter
Elin Johnsen1, Steven Ray Wilson1, Andreas Krapp1, Ingvild Odsbu2, Helle Malerod1,
Kirsten Skarstad2, Elsa Lundanes1
1
University of Oslo, N; 2Oslo University Hospital, Oslo, N
P2-G-463-WE
How Many HILIC Columns do we Need? A Systematic Column Characterization Study
Georg Schuster, Wolfgang Lindner
P2-G-464-TH
Impact of Polymeric Ion-Exchange Columns’ Designs on the Separation of Proteins
K. Flook, C. Saini, Y. Hou, S.Rao, A. Woodruff, M. Rey, Hongmin Zhang, C. Pohl, Y. Agroskin
P2-G-465-WE
Influence of Base Particles and Coverage on Selectivity and Peak Shape of a Diverse
Range of Achiral Analytes in SFC
P. Iraneta, D. W. Brousmiche, J. Fairchild, J. Hill, X-J. Song
Waters Corporation Chemistry Operations, Milford, MA, USA
127
P2-G-466-TH
Introduction of Phospho-Alkyl Bonded Phases for Liquid Chromatography
Szymon Bocian, Bogusław Buszewski
Nicolaus Copernicus University, Torun, PL
P2-G-467-WE
Iron Oxide Nanoparticle Coating: New Modification of Organic Polymer Monolithic
Column for Phosphopeptide Enrichment
Jana Krenkova, Frantisek Foret
Institute of Analytical Chemistry of the ASCR, v. v. i., Brno, CZ
P2-G-468-TH
Kinetic Optimisation of Open-Tubular Liquid-Chromatography Capillaries Coated with
Thick Porous Layers for Increased Loadability
Tim J. Causon1,2, Emily F. Hilder1, Robert A. Shellie1, Sebastiaan Eeltink2, Gert Desmet2
1
2
P2-G-469-WE
Maximizing your Lab’s Throughput with Optimized Column Lengths and Particle
Diameters
Ken Broeckhoven, Gert Desmet
VUB, Brussels, B
P2-G-470-TH
Microbore Columns: a Contribution to Green Chemistry
Adrian Ueberwasser, Ruth Katinka Meike, Thomas Hartmann, Andrea Wille
Metrohm International Headquarters, Herisau, CH
P2-G-471-WE
Modification of Silica-Based Monolithic Capillary Columns for Boronate Affinity
Chromatography
Dana Moravcova, Josef Planeta, Vladislav Kahle, Michal Roth
Institute of Analytical Chemistry of the ASCR, v. v. i., Brno, CZ
P2-G-472-TH
Monolithic Columns Based on Copolymers of Divinylbenzene with Ethylvinylbenzene and
Hydroxyalkyl Methacrylates for Reversed-Phase Chromatography of Small Molecules
Konstantin N. Smirnov, Ivan A. Dyatchkov, Andrey V. Pirogov, Oleg A. Shpigun
Moscow State University, Moscow, RUS
128
P2-G-473-WE
Monolithic Micro-Reactors with Covalently Attached Palladium/Platinum Nanoflowers
for Selected Redox Reactions
Patrick Floris, Damian Connolly, Brett Paull
P2-G-474-TH
Monolithic Silica Based Lectin Affinity Stationary Phase for Bioanalysis
Ugis Danilevics, Ekaterina P. Nesterenko, Roisin Thompson, Paul Clarke,
Brendan O’Connor, Brett Paull
P2-G-475-WE
MonoPLOT Columns Functionalised with Lectin Modified Gold Nano-Particles for
Affinity Extraction of Selected Glycoproteins
Ekaterina Nesterenko, Alexander Yavorskyy, Roisin Thompson, Paul Clarke,
Brendan O’Connor, Brett Paull
P2-G-476-TH
Morphological Analysis of Physically Reconstructed Capillary Hybrid Silica Monoliths
and Correlation with Separation Efficiency
Stefan Bruns1, Takeshi Hara2, Bernd Smarsly2, Ulrich Tallarek1
1
Philipps-Universität Marburg, Marburg, D; 2Justus-Liebig-Universität Giessen, Giessen, D
P2-G-477-WE
N-[Tris(hydroxymethyl)methyl] Acrylamide Functionalized Porous Silica and its
Application in Hydrophilic Interaction Chromatography
Nhat Thi Hong Bui1, Wen Jiang2, Knut Irgum1
1
Umeå University, Umeå, S; 2Merck SeQuant AB, Umeå, S
P2-G-478-TH
New Approach for High Integration of Weak Interaction Sites for Selectivity
Enhancement in HPLC: Synthesis of New Monomers and their Alternating
Copolymerization on Silica
Abul K. Mallik, Hondeng Qiu, Tsuyoshi Sawada, Makoto Takafuji, Hirotaka Ihara
P2-G-479-WE
New Diamond and Carbon-Based Materials for Liquid Chromatography
Matthew R. Linford1, Landon A. Wiest1, David S. Jensen1, Robert C. Davis2,
Andrew Dadson3, Michael A. Vail3
1,2
Brigham Young University, Provo, UT, USA; 3US Synthetic Corporation, Orem, UT, USA
129
P2-G-480-TH
New Evaluations of a PMOS-SiO2 Stationary Phase. Part I: Effect of pH, Type and
Concentration of Buffer on Chromatographic Performance
Endler M. Borges, Karen Goraieb, Carol H. Collins
State University of Campinas, Campinas, SP, BR
P2-G-481-WE
New Polar Embedded Group Stationary Phase with Unique Selectivity
Markus John, Stephan Frech, Florian Taft, Thomas Schuesseler
P2-G-482-TH
New Proposal of Hydrophilic but Nonionic Polymer Phase for High-Selective Normal
Phase Liquid Chromatography
Abul K. Mallik, Kaori Shingo, Aika Ezaki, Tsuyoshi Sawada, Makoto Takafuji,
Hirotaka Ihara
P2-G-483-WE
Novel Approach to Porous Monoliths with Large Surface Area based on
Organic-Inorganic Hybrid Silsesquioxanes and their Surface Functionalization
Ivo Nischang, Ian Teasdale, Oliver Bruggemann
Johannes Kepler University Linz, Leonding, A
P2-G-484-TH
Novel Chromatographic System Utilizing Temperature-Responsive Polymer Containing
Aromatic Amino Acids
Tadashi Nishio1, Ryosuke Kanazashi1, Hideko Kanazawa1, Kenichi Nagase2, Teruo Okano2
1
Keio University, Tokyo, J; 2Tokyo Women’s Medical University, Tokyo, J
P2-G-485-WE
Novel Polymeric Anion Exchangers with Heightened Hydrophilicity for Ion
Chromatography
Alexandra V. Zatirakha, Alexandr D. Smolenkov, Oleg A. Shpigun
P2-G-486-TH
Octadecylsilica Stationary Phase Synthesis via Catalytic Coupling of Unsaturated
Organic Compounds onto a Silica Hydride Surface in Supercritical Carbon Dioxide
Amy P. Nagle1, Norma M. Scully1, Jesse O. Omamogho1, Helen Yeman2, Klaus Albert2,
Jeremy D. Glennon1
1
2
Universität Tübingen, Tübingen, D
130
P2-G-487-WE
Optimized Filling and Protein Separation with a New High Resolution Glass Column
M. Fuchs
Wissenschaftliche Gerätebau Dr. Ing. Herbert Knauer GmbH, Berlin, D
P2-G-488-TH
Ordered Mesoporous (Organo)Silica Particles as Packing Material in RPLC: Increasing
Retention and Improving Particle Stability
Matthias Ide, Frédéric Lynen, Pat Sandra, Pascal Van Der Voort
Ghent University, Gent, B
P2-G-489-WE
Orthogonally Unique Polar Selective Phases for HPLC and UHPLC
David Crowshaw, Melissa Wilcox, Laura Kaepplinger, Michael Early, Chitra Sundararajan
Grace Davison Discovery Sciences, Deerfield, IL, USA
P2-G-490-TH
Pellicular Stationary Phases Created using Glass Carbon Cores with Porous
Nanodiamond Shells for use in Extreme pH Reversed-Phase LC
Landon A. Wiest1, David S. Jensen1, Chuan-Hsi Hung1, Rebecca E. Olsen1,
Robert C. Davis2, Michael A. Vail3, Andrew Dadson3, Pavel Nesterenko4,
Matthew R. Linford1
1,2
3
US Synthetic Corporation, Orem, UT, USA; 4University of Tasmania, Hobart, AUS
P2-G-491-WE
Polystyrene-Based Monolithic Separation Media for Separation of Small Organic
Compounds
Adéla Svobodová1, Jiří Vojta1, Jakub Širc2, Petr Šálek2, Eva Tesařová3, Pavel Coufal1
1,3
Charles University in Prague, Prague, CZ; 2Institute of Macromolecular Chemistry,
Academy of Sciences of the Czech Republic, Prague, CZ
P2-G-492-TH
Preparation and Characterization of Lauryl Methacrylate-Based Reversed Phase
Monolith Chemically Anchored to Microbore PEEK Tubing
Shin Shu, Hiroharu Kobayashi, Akhmad Sabarudin, Michio Butsugan, Tomonari Umemura
Nagoya University, Nagoya, J
P2-G-493-WE
Preparation of a Hybrid Monolithic Silica Capillary Column with Inner Diameter
of 530 μm
Takeshi Hara, Christoph Weidmann, Thomas Traut, Bernd Smarsly
Justus-Liebig-University of Giessen, Giessen, D
131
P2-G-494-TH
Preparation of a Stationary Phase for HPLC by Immobilization of Mixtures of PDMS
and PMODS
Elias Severo da Silva Júnior, Carol H. Collins
Labcrom, Instituto de Química, Campinas, SP, BR
P2-G-495-WE
Preparation of Surface-Coated Macroporous Silica (Fused-Core Silica Monolith) for
HPLC Separations
Risako Ito1, Kazuki Nakanishi1, Kei Morisato1,2, Kazuyoshi Kanamori1
1
Kyoto University, Kyoto, J; 2GL Sciences Inc., Saitama, J
P2-G-496-TH
Preparation, Characterization and Application of Benzyl Methacrylate Capillary
Monolithic Columns
A. Yacine Badjah-Hadj-Ahmed, Zeid A. Al-Othman, Ahmad Aqel,
Abdulrahman A. Al-Warthan
King Saud University, Riyadh, SA
P2-G-497-WE
Reconstruction and Characterization of Polymeric Monolithic Stationary Phases using
Serial Block Face Scanning Electron Microscopy
Tibor Müllner1, Herbert Reingruber2, Armin Zankel2, Ulrich Tallarek1
1
Philipps-University of Marburg, Marburg, D;
2
Graz University of Technology, and Center for Electron Microscopy Graz, Graz, A
P2-G-498-TH
Research in Hybrid Organic/Inorganic Packing Materials
Kevin Wyndham, Pamela Iraneta, Daniel Walsh, Bonnie Alden, Thomas Walter,
Beatrice Muriithi, Jonathan Turner, James Cook, Cheryl Boissel, Scott McCall,
Uwe Neue
P2-G-499-WE
Analyte – Column Interactions in a Phosphatidylcholine HILIC Column
Clara-Eugenia Banos, Susanne K. Wiedmer, Marja-Liisa Riekkola
P2-G-500-TH
Selectivity of Pentafluorophenyl (PFP) and Fluoro-hexyl HPLC Columns Operated under
Hydrophilic Interaction (HILIC) Conditions
Rajesh Desai, Michael Schwartz, Cynthia Miller-Stein, Eric Woolf
Merck Research Laboratories, West Point, PA, USA
132
P2-G-501-WE
Selectivity Testing in Reversed-Phase LC
L. Pereira, T. Edge, M. Dolci, D. Milton, S. Luke
P2-G-502-TH
Separation of Inorganic Anions using Polar Stationary Phases in Capillary Liquid
Chromatography
Lee Wah Lim, Tatsuya Kawasaki, Tetsuya Kida, Toyohide Takeuchi
Gifu University, Gifu, J
P2-G-503-WE
Separation of Silybin and Acetylsilybin Diastereoisomers by Narrow-Bore C18
Silica-Based Monolithic and Core-Shell Columns
Petr Marhol, Radek Gažák, Vladimír Křen
Institute of Microbiology, Academy of Sciences of the Czech Republic, Prague, CZ
P2-G-504-TH
Stability and Performance of Slurry Packed Capillary Columns
Martin Franc, Jiří Vojta, Zuzana Bosáková, Pavel Coufal
P2-G-505-WE
Stationary Phase Characterization of Totally Porous and Superficially Porous sub
3-μ
μm Particle Packed Columns
Silvia Jakabová1,2, Péter Vajda1, Borbála Boros3, Attila Felinger1
1,3
2
Constantine the Philosopher University in Nitra, Nitra, SK
P2-G-506-TH
Stationary Phase Made by Solid Phase Synthesis
Éva Jámbor, Ágnes Bóna, László Márk, Róbert Ohmacht
P2-G-507-WE
Stationary Phases for Reversed-Phase High-Performance Liquid Chromatography
using Thermal Immobilization of Poly(phenylpropyl)methylsiloxane onto Silica
Marcelo V. F. Delmonde, Isabel C. S. F. Jardim, Carol H. Collins
Labcrom, Instituto de Química, Campinas, SP, BR
133
P2-G-508-TH
Styrene-Based Monolithic Columns for Simultaneous Separation of Biomolecules and
Small Molecules
Rainer Koeck1, Rania Bakry1, Lukas Trojer1, Kelly J. Flook2, Yury Agroskin2,
Guenther K. Bonn1
1
Leopold-Franzens University, Innsbruck, A; 2Dionex Corporation, Sunnyvale, CA, USA
P2-G-509-WE
Sub-1-micron Silica Particles Functionalized with C18 for Drugs Separation using
Capillary Liquid Chromatography
Carlos Eduardo Domingues Nazario, Fernando Mauro Lanças
University of Sao Paulo, Sao Carlos, SP, BR
P2-G-510-TH
Superficially Porous NUCLEOSHELL Sorbents for High Efficiency and Fast LC
Applications
Florian Taft, Markus John, Stephan Frech, Maria Thelen, Thomas Schüßeler
P2-G-511-WE
Synthesis and Evaluation of Hybrid Organic/Inorganic Particles for Biomolecular
Separations
N. Lawrence, K. Wyndham, K. Glose, J. Sargent, E. Bouvier, N. Brady, S. Serpa,
Tom Walter
P2-G-512-TH
Synthesis of Lectin Affinity Macroporous Silica-Based Stationary Phase for Selective
Extraction of Glycoproteins
Nicola McGilicuddy1, Jesse Omamogho2, Ekaterina P. Nesterenko1, Roisin Thompson1,
Paul Clarke1, Brendan O’Connor1, Jeremy D. Glennon1, Brett Paull1
1
Dublin City University, Dublin, IRL; 2University College Cork, Cork, IRL
P2-G-513-WE
The Application of Silica Gel Supported Gold Nanoparticles in HPLC
Irina Ananieva, Yana Elfimova, Aleksandr Majouga, Daria Pichugina, Igor Rodin, Oleg Shpigun
P2-G-514-TH
The Impact of Extra-Column Band Broadening on the Chromatographic Efficiency of
5 cm Long Narrow-Bore Very Efficient Columns
Szabolcs Fekete, Jenő Fekete
134
P2-G-515-WE
The Influence of Changing Stationary Phases and pH to Avoid Matrix Effects in
Different Biological Matrices by using LC-MS/MS
Patrick Johansson, Jennie de Verdier
AstraZeneca R&D Mölndal, Mölndal, S
P2-G-516-TH
The Synthesis and Design of Temperature-Responsive Polymer for Aqueous and Green
Chromatography
Mirai Shimamura1, Tadashi Nishio1, Hideko Kanazawa1, Kenichi Nagase2, Teruo Okano2
1
Keio University, Tokyo, J;
2
Tokyo Women’s Medical University, Tokyo, J
P2-G-517-WE
Towards Wide-Bore Monolithic Columns for Size/Topology Separations of Branched
Polysaccharides
Francisco Vilaplana1,2, Mitchell A. Sullivan2, Robert G. Gilbert2, Peter Schoenmakers1
1
University of Amsterdam, Amsterdam, NL;
2
The University of Queensland, Brisbane, AUS
P2-G-518-TH
Transferring Compendial Methods to Superficially Porous Columns
William Long1, Anne Mack1, Maureen Joseph1, Linda Lloyd2
1
2
P2-G-519-WE
Ultra-High-Selective HPLC Packing Materials from Ionic Self-Assembly of Azobenzene
Dye and Poly(Ionic Liquid)-Modified Silica
Hongdeng Qiu1,2, Abul K. Mallik1, Makoto Takafuji1, Shengxiang Jiang2, Hirotaka Ihara1
1
Kumamoto University, Kumamoto, J;
2
Lanzhou Institute of Chemical Physics, Chinese Academy of Science, Lanzhou, PRC
P2-G-520-TH
Unexpected Properties of an Unusual HPLC Stationary Phase
Zsanett Gulyás1, Mariann Makuta1, Gerda Varga2, János Harangi3
1,2
3
P2-G-521-WE
Use C30 as a General-Purpose Stationary Phase for a Broad Range of Applications
Xiaodong Liu, Mark Tracy, Christopher Pohl
135
Enviromental Analysis, Food Safety, Agricultural Analysis
P2-G-523-WE
A New Ultra Performance Liquid Chromatography Method for the Determination of
Total Isoflavone Aglycones in Different Soybean Cultivars after Enzymatic Hydrolysis
Gregor Fiechter, Ivana Opacak, Bernd Raba, Helmut K. Mayer
BOKU – University of Natural Resources & Life Sciences Vienna, Vienna, A
P2-G-524-TH
A Revisited Strategy for Analysis of Polar Compounds by Reversed Phase Liquid
Chromatography using Serially Coupled Columns
Thorsten Teutenberg1, Steffen Wiese1, Jochen Tuerk1, Cristoph Portner1, Vera Slomka2,
Annika Reeh3, Harald Weber3
1
2
University Duisburg-Essen, Essen, D;
3
Niederrhein University of Applied Science, Krefeld, D
P2-G-525-WE
A Separation Technique for Chlorophyll Metabolites in Oriental Tobacco Leaf
Naoyuki Ishida
Japan Tobacco Inc., Yokohama, J
P2-G-526-TH
Adsorption of Pharmaceuticals on Beta Zeolites
Alberto Cavazzini, Luisa Pasti, Nicola Marchetti, Annalisa Martucci, Francesco Dondi
P2-G-527-WE
An Alternative Method for Microcystins Analysis in Aerosol Samples
Roberta Zangrando1, Elena Barbaro2, Elisa Scalabrin2, Valentina Felin2, Carlo Barbante1,2,
Andrea Gambaro1,2
1
Institute for the Dynamics of Environmental Processes CNR, Venice, I;
2
DAIS, University of Venice, Venice, I
P2-G-528-TH
Analysis of 1-Hydroxypyrene in Urine Samples using Traditional C18-type Column and
C18 Column Packed with the New Core-Shell Technology (C-18 Kinetex)
Magdalena Szumska, Krystyna Tyrpień, Cezary Dobosz, Tomasz Wielkoszyński
Medical University of Silesia, Zabrze, PL
136
P2-G-529-WE
Analysis of 3-chloropropane-1,2-diol (3-MCPD) Esters in Edible Oils by Liquid
Chromatography-Tandem Mass Spectrometry (LC-MS/MS)
Lubomir Karasek, Thomas Wenzl, Franz Ulberth
Institute for Reference Materials and Measurements, Geel, B
P2-G-530-TH
Analysis of Polycyclic Aromatic Hydrocarbons by LC Utilizing Multiple Detection
Methods
Ty W. Kahler, Michelle Misselwitz, Sharon Lupo, Julie Kowalski, Rick Lake,
Chris Denicola, Steve Kozel
Restek Corporation, Bellefonte, PA, USA
P2-G-531-WE
Analysis of Pristine Fullerenes in Water by Liquid Chromatography-Atmospheric
Pressure Photoionization-Mass Spectrometry (LC-APPI-MS)
Oscar Núñez1, Héctor Gallar-Ayala1, Claudia P.B. Martins2, Encarnación Moyano1,
Maria Teresa Galceran1
1
University of Barcelona, Barcelona, E;
2
Thermo Fisher Scientific, Barcelona, E
P2-G-533-WE
Application of LC-MS/MS and One-Point Calibration to Pesticide Residue Control in
Fruits and Vegetables
Anna Stachniuk, Agnieszka Szmagara, Emilia Fornal
The John Paul II Catholic University of Lublin, Lublin, PL
P2-G-534-TH
Application of Multi-Dimensional Chromatography to the Separation and Identification
of the Components of Dissolved Organic Matter (DOM)
Sara Sandron, Brian Kelleher, Ekaterina Nesterenko, Margaret McCaul, Brett Paull
P2-G-535-WE
Application of Phenomenex Products in Food Analysis in Food Toxicology National
Reference Laboratory Hungary
Ádám Tölgyesi1,3, Katalin Békési1, Virender K. Sharma2, Jenő Fekete3
1
Central Agricultural Office Food and Feed Safety Directorate Food Toxicology National
Reference Laboratory, Budapest, H;
2
Chemistry Department Florida Institute of Technology, Melbourne, FL, USA;
3
137
P2-G-536-TH
Application of UHPLC-MS/MS to the Determination of Eight Quinolones of Veterinary
use in Honey
Manuel Lombardo-Agüí, Ana M. García-Campaña, Carmen Cruces-Blanco,
Laura Gámiz-Gracia
P2-G-537-WE
Association of Anthocyanins from Grapes to Ripening and Varietal Differentiation by
LC-DAD-MS and Principal Component Analysis
Karina Fraige, Felipe A. T. Serafim, Emanuel Carrilho
Universidade de São Paulo, Sao Carlos, SP, BR
P2-G-538-TH
Bridging the Gap: Ultrahigh Resolution Analysis of Dissolved Organic Matter and
Inorganic Trace Elements in the Ocean
Oliver J. Lechtenfeld1, Boris P. Koch1,2, Gerhard Kattner1, Arnd Ingendoh3,
Matthias Witt3
1
Alfred Wegener Institute for Polar and Marine Research, Bremerhaven, D;
2
University of Applied Sciences, Bremerhaven, D;
3
P2-G-539-WE
Characterization and Determination of Mixtures of Fatty Alcohol Ethoxylates and Alkyl
Ether Sulfates in Industrial and Environmental Samples
Miriam Beneito-Cambra, Laura Ripoll-Seguer, José Manuel Herrero-Martínez,
Ernesto Francisco Simó-Alfonso, Guillermo Ramis-Ramos
P2-G-540-TH
Characterization of Alkylpolyphosphonates by HILIC using a Polymeric Zwitterionic
Stationary Phase
Enrique Javier Carrasco-Correa, Miriam Beneito-Cambra, José Manuel Herrero-Martínez,
P2-G-541-WE
Characterization of Hydroxycinnamic Acids from Brewer’s Spent Grain by
HPLC-UV-ESI-MS
Manuela M. Moreira, Joana A. Vieira, Aquiles A. Barros, Luís F. Guido
Universidade do Porto, Porto, P
138
P2-G-542-TH
Chromium, Cobalt and Nickel in Eye Shadows: Particle Size Distributions and
Elements Concentration by SdFFF and AAS
Catia Contado, Antonella Pagnoni
P2-G-543-WE
Classification of Vegetable Oils According to their Botanical Origin using Fatty Acid
Profiles Established by Capillary Electrophoresis with Indirect UV Detection
María Vergara-Barberan, Aarón Escrig-Domenech, María Jesús Lerma-García,
Ernesto Francisco Simó-Alfonso, José Manuel Herrero-Martínez
P2-G-544-TH
Classification of Vegetable Oils According to their Botanical Origin using Hydrocarbon
Profiles Established by GC-MS
Sandra Martínez-Estévez, María Jesús Lerma-Garcia, Alejandro Prieto-Arnal,
Ernesto Francisco Simó-Alfonso, José Manuel Herrero-Martínez
P2-G-545-WE
Classification of Vegetable Oils According to their Botanical Origin using
Triacylglycerol Profiles Established by Capillary Electrochromatography
María Jesús Lerma-García, María Vergara-Barberán, José Manuel Herrero-Martínez,
Ernesto Francisco Simó-Alfonso
P2-G-546-TH
Comparison of Solid-Phase Microextraction Coupled with Gas Chromatography-Mass
Spectrometry and Ultrafast Liquid Chromatography Method for Analysis of Volatile
Organic Compounds in Selected Polish Fruit Juices
Monika Kula, Jerzy Oszczudlowski, Zygfryd Witkiewicz
P2-G-547-WE
Comparison of Solid-Phase Microextraction Coupled with Gas Chromatography-Mass
Spectrometry and Ultrafast Liquid Chromatography Method for Analysis of Volatile
Organic Compounds in Selected Polish Honeys
Milena Lisowska, Jerzy Oszczudlowski, Zygfryd Witkiewicz
139
P2-G-548-TH
Comparison of Different Sample Treatments for the Analysis of Ochratoxin A in Wine
by Capillary HPLC with Laser Induced Fluorescence Detection
Natalia Arroyo-Manzanares, Ana M. García-Campaña, Laura Gámiz-Gracia
P2-G-550-TH
Comprehensive Confirmation Workflow for Full Scan Accurate Mass Multi-Target
Screening of Pesticides in Food Giving Results with Maximum Confidence
Sven Meyer1, Ellen Scherbaum2, Rebekka Loetterle2, Petra Decker1, Oliver Raether1,
Ilmari Krebs1, Verena Tellstrom1
1
2
Chemisches und Veterinäruntersuchungsamt Stuttgart, Stuttgart, D
P2-G-551-WE
Control of Antibiotics by Micellar Liquid Chromatography in Food Samples
Maria Rambla-Alegre1, Julián Paños-Pérez2, Beatriz Beltrán-Martinavarro1,
Abhilasha Durgabanshi3, Devasish Bose4, Nitasha Agrawal4, Josep Esteve-Romero1,
Samuel Carda Broch1
1,2
3
Banaras Hindu University, Vanarasi, IND;
4
Dr. H.S. Gour University, Sagar, IND
P2-G-552-TH
Core-Shell versus Ultra Performance Liquid Chromatography Columns for the Analysis
of Environmental Samples
C. Hug, N. Ulrich, W. Brack
UFZ-Helmholtz Centre for Environmental Research, Leipzig, D
P2-G-553-WE
Derivatization with Glyoxylic Acid as New Approach for Unsymmetrical
Dimethylhydrazine HPLC-UV Determination
Timofey Bolotnik, Oleg Shpigun, Roman Smirnov, Alexander Smolenkov
P2-G-554-TH
Determination of 29 Personal Care Products in Water using High-Flow Solid-Phase
Extraction and Ultra-High Performance Liquid Chromatography/Tandem Mass
Spectrometry
M.-T. Lu, P.-K. Hsiao, S.-C. C. Lung, G.-S. Wang, C.-Y. Chen
140
P2-G-555-WE
Determination of B-Vitamins, Choline, and Carnitine in NIST Food-Matrix SRMs
Melissa M. Phillips, Lane C. Sander, Katherine E. Sharpless, Stephen A. Wise
P2-G-556-TH
Determination of Carbamazepine, Sulfamethoxazole and Cocaine in Surface Water in
Berlin by LC-MS/MS and ELISA
Andreas Lehmann, Arnold Bahlmann, Michael G. Weller, Ulrich Panne,
Rudolf J. Schneider
BAM Federal Institute for Materials Research and Testing, Berlin, D
P2-G-557-WE
Determination of Coccidiostats in Fermented Milk Products
Szilárd Nász1, Zsuzsanna Eke1,2
1
Eötvös Loránd University, Budapest, H;
2
Wessling International Research and Educational Centre, Budapest, H
P2-G-558-TH
Determination of Endocrine Disrupting Phenols in Seawaters and Industrial Effluents
by in-situ Ionic Liquid-Dispersive Liquid-Liquid Microextraction and High-Performance
Jessica López-Darias, Verónica Pino, Juan H. Ayala, Ana M. Afonso
Universidad de La Laguna (ULL), La Laguna, Tenerife, E
P2-G-559-WE
Determination of Endogenous and Syntetic Glucocorticoids in Sewage Sludge, Sewage
and River Water by PLE/SPE-UHPLC-MS/MS
Pol Herrero, Francesc Borrull, Rosa Mª Marce, Eva Pocurull
Rovira i Virgili University, Tarragona, Catalonia, E
P2-G-560-TH
Determination of Glucosamine by Ultra-High Pressure LC in Shrimp By-Products
A. Sanches-Silva1, T. Ribeiro1, T. G. Albuquerque1, P. Paseiro2, R. Sendón2,
J. López-Cervantes3, D. I. Sánchez-Machado3, H. Soto Valdez4, I. Angulo5,
G. P. Aurrekoetxea5, H. S. Costa1
1
National Health Institute Dr Ricardo Jorge, I.P., Lisboa, P;
2
University of Santiago de Compostela, Santiago de Compostela, E;
3
Instituto Tecnologico de Sonora, Sonora, MEX;
4
A.C., CTAOV, Sonora, MEX;
5
Gaiker, Technological Center, Zamudio, E
141
P2-G-562-TH
Determination of Isocyanates in the Air of Working Environment by HPLC Method
Alžbeta Hegedűsová1, Jarmila Dubajová2, Ondrej Hegedűs2, Zuzana Šmotláková2,
Silvia Jakabová1,3, Tímea Pernyeszi3
1
Constantine the Philosopher University, Nitra, SK; 2Regional Public Health Authority in
Nitra, Nitra, SK; 3University of Pécs, Pécs, H
P2-G-564-TH
Determination of Non-Steroidal, Analgesic, Anti-Inflammatory Drugs (NSAIDs) in
Environmental Water Samples Using Liquid-Phase Microextraction Method (LPME)
Prior to UV-Vis Spectrophotometer
Farideh Mofazzeli1, Narges Ashraf2
1
Islamic Azad University, Quchan, IR; 2Ferdowsi University of Mashhad, Mashhad, IR
P2-G-565-WE
Determination of Ochratoxin A in Coffee Drinks with High-Flow Liquid
C.-W. Chang, C.-Y. Chen
P2-G-566-TH
Determination of Perfluorinated Chemicals in Food and Drinking Water Using
High-Flow Solid-Phase Extraction and Ultra-High Performance Liquid Chromatography
/ Tandem Mass Spectrometry
Y.-J Chang, P.-C. Chen, G.-S. Wang, C.-Y. Chen
P2-G-568-TH
Determination of Priority Substances in Wastewater using SPE, LCMS and GCMS
L. Jones, F. Regan
P2-G-569-WE
Determination of Some Textile Dyes in Waste Waters by Solid Phase Extraction
Followed by Liquid Chromatography-Electrospray Ionization Mass Spectrometry
Florina Copaciu1, Virginia Coman2, Dorina Simedru3, Simion Beldean-Galea1,
Ocsana Opriş1, Dumitru Ristoiu1
1,2
Babeş-Bolyai University, Cluj-Napoca, RO; 3INCDO-INOE 2000, Cluj-Napoca, RO
P2-G-570-TH
Determination of Soy Isoflavones in Foods and Dietary Supplements
Mary Bedner, Manuela K. Gradl, Mariana Arce-Osuna, Melissa M. Phillips,
Catherine A. Rimmer, Lane C. Sander, Katherine E. Sharpless, Klaus Albert
142
P2-G-571-WE
Determination of Total Selenium Ant its Species in Selenium Enriched Garden Peas
(Pisum sativum L.)
Silvia Jakabová1,2, Borbála Boros3, Alžbeta Hegedűsová2, Ondrej Hegedűs4,
Attila Felinger1
1,3
2
Constantine the Philosopher University in Nitra, Nitra, SK;
4
Regional Public Health Authority in Nitra, Nitra, SK
P2-G-572-TH
Developing a Novel Monitoring Programme for Priority Substances in Water
Fiona Regan, Lisa Jones, Antoin Lawlor
P2-G-573-WE
Development and Validation of a Reversed Phase Liquid Chromatography Method for
the Determination of Indole-3-Acetic Acid, Indole-3-Pyruvic Acid and Abscisic Acid
in Barley
Ilva Nakurte, Anete Keisa, Nils Rostoks
University of Latvia, Riga, LV
P2-G-574-TH
Development of a Chromatographic Method for the Simultaneous Analysis of Seven
Carotenoids and Two Vitamins in Food Samples
A. Sanches-Silva1, H. S. Costa1, T. Albuquerque1, P. Finglas2
1
Instituto Nacional de Saude Doutor Ricardo Jorge, I.P. (INSA), Lisboa, P;
2
Institute of Food Research, Norwich, UK
P2-G-575-WE
Development of a Reference Material for L-Ascorbic Acid in Fruits and Vegetables
Ana Valente, Ana Sanches-Silva, Tania G. Albuquerque, Helena S. Costa
Instituto Nacional de Saude Doutor Ricardo Jorge, I.P. (INSA), Lisboa, P
P2-G-576-TH
Different Preconcentation Techniques for Enhancing Sensitivity in the Determination
of Parabens by Capillary Electrophoresis
Irene Maijó, Francesc Borrull, Marta Calull, Carme Aguilar
University Rovira i Virgili, Tarragona, E
P2-G-577-WE
Direct IC-MS Determination of Endothall in EPA Method 548.1
Richard F. Jack, Leo (Jinyuan) Wang, Marcus Miller, William C. Schnute
143
P2-G-578-TH
Elucidation of the Antioxidant Activity in Complex Mixtures: DPPH and ABTS Radical
Scavenging Coupled to RPLC and HILIC
Bram Miserez1, Seppe De Smet1, Maria Rambla-Alegre2, Frédéric Lynen1, Pat Sandra1
1
Pfizer Analytical Research Centre, Ghent University, Ghent, B;
2
Universitat Jaume I, Castello, E
P2-G-579-WE
Elucidation of the Antioxidant Activity in Complex Mixtures: Optimization of the On-Line
ABTS-Based Radical Scavenging Assay and Application in Food Analysis
Bram Miserez 1, Seppe De Smet 1, Maria Rambla-Alegre 2, Frédéric Lynen 1,
Pat Sandra 1
1
Pfizer Analytical Research Centre, Ghent University, Ghent, B;
2
P2-G-580-TH
Environmental Loading Studies: How to Estimate the Real Impact of Growing
Pharmaceutical Consumption on Aquatic Fauna and Flora?
Renáta Varga, Iván Somogyvári, Zsuzsanna Eke, Kornél Torkos
Eötvös Loránd University, Budapest, H
P2-G-581-WE
Evaluation of the Performance Improvements Needed in an ESI-QTOF-MS System for
Qualitative and Quantitative Multi-Target Pesticide Screening in Food
Carsten Baessmann1, Sven Meyer1, Ellen Scherbaum2, Rebekka Loetterle2,
Petra Decker1, Oliver Raether1, Ilmari Krebs1
1
2
Chemisches und Veterinaruntersuchungsamt Stuttgart, Stuttgart, D
P2-G-582-TH
Fast Online SPE Purification of Plant Extracts for Improved Determination of Steviol
Glycosides
René Borstel1, Udo Kienle2
1
Dr. Ing. Herbert Knauer GmbH, Berlin, D;
2
Institute of Agricultural Engineering University Hohenheim, Stuttgart, D
P2-G-583-WE
Full-Scan Accurate Mass Selectivity of Liquid Chromatography Combined with Orbitrap
Mass Spectrometry in the Analysis of Anti-Bacterial Substances in Feed Matrices
George Kaklamanos, Vincent Ursula
European Commission, Joint Research Centre (EC-JRC-IRMM), Geel, B
144
P2-G-584-TH
Hollow Fiber Liquid Phase Microextraction Combined with High Performance Liquid
Chromatography for the Determination of Antimicrobial Agents in Water and Sewage
Sludge
Ester Sagristà, Marta Casademont, Victòria Salvadó, Manuela Hidalgo
University of Girona, Girona, E
P2-G-586-TH
HPLC Determination of Pesticides using a Doubly Zirconized Silica Support with a
Chemically Bonded and End-Capped C18 Stationary Phase
Karen Goraieb, Carol Hollingworth Collins
State University of Campinas (UNICAMP), Campinas, BR
P2-G-587-WE
HPLC Fluorescence Determination of Ochratoxin A Utilizing a Double Internal
Standard and its Application to Poultry Feed
Muzaffer Tuncel1, Elif Mine Oncu-Kaya2, Ulku Dilek Uysal2, Tufan Guray3
1,2
Anadolu University, Eskişehir, TR; 3Eskişehir Osmangazi University, Eskişehir, TR
P2-G-588-TH
HPLC Monitoring of All Steps of L-Lactide Manufacture from Renewable Biomass
S. Beksaev1, S. Mulyashov1, I. Ilushka2, O. Grechishkina1, F. Sirovski1
1
D.I. Mendeleev University of Chemical Technology of Russia, Moscow, RUS; 2Krasnodar
Branch of The Federal State Enterprise ‘Bio Plant Protection Agents’, Krasnodar, RUS
P2-G-589-WE
HPLC-DAD-MS Evaluation of Phenolic Profiles of Olive Mill Wastewaters Treated by
Membrane Filtration Systems
Patrizia Comandini1, María Jesús Lerma-García2, Pietro Massanova1,
José Manuel Herrero-Martínez2, Ernesto Francisco Simó-Alfonso2, Tullia Gallina Toschi1
1
University of Bologna, Cesena, FC, I; 2University of Valencia, Burjassot, E
P2-G-590-TH
HPLC-FD Method Validation for Determination of Several Fluoroquinolones in
Biodegradation Assays
Alexandra Maia1,4, Ana Rita Lado Ribeiro1,2, Paula Maria Lima Castro2,
Maria Elizabeth Tiritan1,3
1
Centro de Investigacao em Ciencias da Saude (CICS), Gandra, PRD, P; 2Universidade
Catolica Portuguesa, Porto, P; 3,4Universidade do Porto (CEQUIMED-UP), Porto, P
P2-G-591-WE
Identification of Impurities in Melatonin Tablets by LC-ToF
Sharanya Reddy1, Shida Shen1, Sean Daughtery2, Eugene Davidov1, Adam Patkin1
1
PerkinElmer, Inc., Shelton, CT, USA; 2PerkinElmer Inc., Seer Green, Beaconsfield, UK
145
P2-G-592-TH
Influence of Ultra-Violet Radiation on the Ascorbic Acid Content of Pineapple
By-Products Determined by HPLC
Ana Freitas1, Ana Valente2, Tania G. Albuquerque2, Margarida Moldão-Martins1,
Helena S. Costa2, Ana Sanches-Silva2
1
Technical University of Lisbon, Lisboa, P;
2
National Health Institute Dr Ricardo Jorge, I.P. Lisboa, P
P2-G-593-WE
Ion- and Liquid Chromatographic Profiling of Photocatalytic Degradation Pathways of
Environmental Pollutants
Erzsébet Szabó-Bárdos1, Ottó Horváth1, Norbert Törő2, Gyula Kiss3, Krisztián Horváth4,
Péter Hajós4
1,2,4
University of Pannonia, Veszprém, H;
3
HAS Chemistry Group at University of Pannonia, Veszprém, H
P2-G-594-TH
Isoflavone Analysis with Ultra Performance Liquid Chromatography: Application to
Soy-Based Nutritional Supplements
Gregor Fiechter, Ivana Opacak, Bernd Raba, Helmut K. Mayer
University of Natural Resources & Life Sciences Vienna, Vienna, A
P2-G-595-WE
Large Volume Sample Injection into 2D-HPLC System for High Sample Preconcentration
and Highly Sensitive Determination of Insecticides in Surface Water Analysis
Dalibor Šatínský1, Ivana Brabcová1, Maria Albertovna Khalikova2, Petr Solich1
1
2
Belgorod State University, Belgorod, RUS
P2-G-596-TH
LC/MS/MS Analysis of Cyanotoxins in the Drinking Water Chain Following an
Extraordinary Bloom of Cyanobacterium Planktothrix Rubescens in an Italian Basin
Luca Lucentini1, Federica Nigro Di Gregorio1,6, Emanuele Ferretti1, Ilaria Di Giacomo1,
Sara Bogialli4, Massimo Ottaviani1, Matteo Cannarozzi De Grazia2, Nicola Ungaro3,
Pierpaolo Abis5
1
Italian National Health Institute, Rome, I; 2Dept. of Health, Apulia Region, Bari, I;
3
Regional Agency for the Prevention and Environmental Protection, Bari, I;
4
University of Padova, Padova, I; 5Aqueduct of Puglia, Bari, I;
6
University “Sapienza”, Rome, I
P2-G-597-WE
LC-MS/MS Separation of Emerging Contaminants on Fluorous Stationary Phases
Nicola Marchetti1, Alberto Cavazzini1, Luisa Pasti1, Aldo Laganà2, Francesco Dondi1
1
University of Ferrara, Ferrara, I; 2University “Sapienza”, Rome, I
146
P2-G-598-TH
Liquid Chromatography Tandem Mass Spectrometry Confirmatory Method of
Nitroimidazole Residues in Food and Feed Samples
L. Giannetti1, A. Giorgi1, F. Necci1, F. Marini1, E. Gennuso1, D. Colangelo1,
R. Baccelliere1, M.V. Russo2, B. Neri1
1
Istituto Zooprofilattico Sperimentale del Lazio e Toscana, Rome, I;
2
Universita del Molise, Campobasso, I
P2-G-599-WE
Liquid Chromatography-Tandem Mass Spectrometry for the Determination of
Aminoglycosides in Honey
Élida Alechaga, Encarnación Moyano, M. Teresa Galceran
University of Barcelona, Barcelona, E
P2-G-600-TH
Maximizing Separation Efficiency for Wine Analysis and Developing Ultra Fast
Qualitative Analysis Method of Catechins using Ultra High Pressure Reverse Phase
Lisa Zang1, Adeline Delcambre2, Yann André2, Dawn Visintainer2, Cedric Saucier2
1
Agilent Technologies, Santa Clara, CA, USA; 2University of British Columbia, Kelowna BC, CDN
P2-G-601-WE
Method for the Analysis of 4-Methylimidazole by LC/MS and LC/MS/MS
Ty W. Kahler, Julie Kowalski, Rick Lake, Steve Kozel, Chris Denicola
P2-G-603-WE
Monitoring of Iodine- and Gadolinium-Containing Contrast Media in Drinking Water
Treatment Plants
Moritz Thomas1, Pfundstein Peter2, Martin Christian2, Schulz Wolfgang3, Seitz Wolfram3,
Flottmann Dirk1
1
Metrohm International Headquarters, Herisau, CH; 2Hochschule Aalen, Aalen, D;
3
Zweckverband Landeswasserversorgung, Langenau, D
P2-G-604-TH
Multiresidue UHPLC-MS/MS Analysis of Antiparasitic Veterinary Drugs in Vegetable
Edible Matrices
Anna Martínez-Villalba, Encarnación Moyano, Maria Teresa Galceran
University of Barcelona, Barcelona, E
P2-G-605-WE
New Certified Reference Materials for Reliable Measurements of Oxytetracycline in Milk
Reinhard Zeleny, Heinz Schimmel
Institute for Reference Materials and Measurements (IRMM), Geel, B
147
P2-G-606-TH
Novel Polychloromethylstyrene Coated Superparamagnetic Surface Molecularly
Imprinted Core-Shell Nanoparticles for Selective Separation of Bisphenol A
Jizhong Liu, Weizhi Wang, Yanyan Huang, Yongliang Liu, Guoquan Liu, Rui Zhao
Institute of Chemistry, Chinese Academy of Sciences, Beijing, PRC
P2-G-607-WE
Online Enrichment Method for the Quantification of Chlorinated Herbicides in Water
by LC-UV
Srividya Kailasam1, Syed Salman Lateef1, Angelika Gratzfeld-Huesgen2
1
2
Agilent Technologies Waldbronn, Waldbronn, D
P2-G-608-TH
Online High Volume SPE-LC-APCI-MS/MS for the Determination of Steroid Hormones
with Enhanced Separation and Elution using a Ternary Mobile Phase Composition
Paul B. Fayad1, Michèle Prévost2, Sébastien Sauvé1
1
Université de Montréal, Montréal, Qc, CDN;
2
École Polytechnique de Montréal, Montréal, Qc, CDN
P2-G-609-WE
On-Line Hyphenation of Immuno-Preconcentration and Capillary Zone Electrophoresis:
Application to the Analysis of Ochratoxin A
J. Chamieh1, C. Faye2, O. Vandenabeele-Trambouze2, T. Moreau2, V. Dugas1, C. Demesmay1
1
Université de Lyon, Villeurbanne, F; 2Université Montpellier II, Montpellier, F
P2-G-610-TH
On-Line Micro Solid-Phase Extraction Combined with Capillary Liquid
Chromatography-Tandem Mass Spectrometry for High Throughput Analysis of
Microcystins and Nodularin-R in Tap Water and Lake Water
Yuanhong Shan, Xianzhe Shi, Guowang Xu
P2-G-611-WE
On-Line SPE-UPLC-MS/MS Methodology for the Selective Determination of Several
Endocrine Disrupting Compounds in Sewage Samples
T. Vega-Morales, Z. Sosa-Ferrera, J. J. Santana-Rodríguez
Universidad de Las Palmas de Gran Canaria, Las Palmas de Gran Canaria, E
P2-G-612-TH
Optimization of a SPE-UPLC-MS/MS Method for the Determination of Benzotriazole
Compounds used in Personal Care Products
Sarah Montesdeoca-Esponda, Zoraida Sosa-Ferrera, José Juan Santana-Rodríguez
Universidad de Las Palmas de Gran Canaria, Las Palmas de Gran Canaria, E
148
P2-G-613-WE
Pesticides in Water, Sediments and Biota of Óbidos Lagoon, Portugal
Maria Isabel Pinto1, Ana Ferreira2, Carlos Vale2, Gerhard Sontag3, João Paulo Noronha1
1
Universidade Nova de Lisboa, Caparica, P;
2
National Institute of Biological Resources, Lisboa, P; 3University of Vienna, Vienna, A
P2-G-614-TH
Phenolic Characterisation of Grapevine Cultivars Native to Hungary by LC-MS
Borbála Boros1, Silvia Jakabová2,3, Lajos Vincze4, Attila Felinger2, Marianna Kocsis5
1,2,5
3
Constantine the Philosopher University in Nitra, Nitra, SK; 4Simkon Kft., Budapest, H
P2-G-615-WE
PPCPs Detected in Laboratory Water
Maricar Tarun1, Chuan Wang2, Stephane Mabic3, Yinfa Ma2
1
EMD Millipore, Billerica, MA, USA;
2
Missouri University of Science & Technology, Rolla, MO, USA;
3
Merck Millipore, St Quentin, F
P2-G-616-TH
Qualitative and Quantitative Analysis of COPs in Cypriot Meat Samples using
HPLC-Determination of the Most Effective Sample-Preparation Procedures
Christiana A. Georgiou, Constantina P. Kapnissi-Christodoulou
P2-G-617-WE
Quantitation of Fluoroacetic Acid and Fluoroacetamide with Mass Spectrometric Detection
Richard Jack, Marcus Miller, Leo (Jinyuan) Wang, William C. Schnute
P2-G-618-TH
Quantitative Analysis of Carbonyl-DNPH Derivatives by UHPLC/UV
Terry Zhang, Guifeng Jiang
P2-G-619-WE
Quantitative Analysis of Pyrrolizidine Alkaloids in Commercially Available Honey using
High Performance Liquid Chromatography coupled to an Ion Trap Mass Spectrometer
Caroline T. Griffin1, Martin Danaher2, Christopher Elliott3, D. Glenn Kennedy4,
Ambrose Furey1,5
1,5
Cork Institute of Technology (CIT), Cork, IRL;
2
Ashtown Food Research Centre (AFRC), Dublin, IRL;
3
Queens University Belfast (QUB), Belfast, UK;
4
Agri-Food and Biosciences Institute (AFBI), Belfast, UK
149
P2-G-620-TH
Rapid UHPLC Determination of Nine Common Herbicides in Drinking Water with the
PerkinElmer Flexar FX-15 System Equipped with a PDA Detector
April DeAtley, Njies Pedjie
PerkinElmer, Shelton, CT, USA
P2-G-621-WE
Separation and Determination of Alkyl Sulfates in Wastewater Treatment Plants by
Liquid Chromatography-Mass Spectrometry
Carolina Fernández-Ramos, Inmaculada Jiménez-Díaz, Rosario Blanc, Óscar Ballesteros,
Alberto Navalón, Alberto Zafra-Gómez, Jose Luís Vílchez
P2-G-622-TH
Separation of Alkylpolyphosphonates by Derivatization with Benzyl Alcohol Followed by
Enrique Javier Carrasco-Correa, Miriam Beneito-Cambra, José Manuel Herrero-Martínez,
P2-G-623-WE
Simultaneous Analysis of Water Soluble Vitamins in Vitamin Enriched Beverage and
Multi-Vitamin Dietary Supplements by Ultra-High Performance Liquid Chromatography
Tandem Mass Spectrometry
Jinyuan Wang, Xiaodong Liu, William C. Schnute
P2-G-624-TH
Simultaneous Determination of Endocrine Disrupters in Surface Water and in Water
for Human Consumption by LC/MS/MS
Laura Achene1, Sara Bogialli2, Federica Nigro Di Gregorio1,5, Luca Lucentini1,
Emanuele Ferretti1, Franca Palumbo3, Enrico Raffo3, Stefano Polesello4, Sara Valsecchi4,
Massimo Ottaviani1
1
Italian National Health Institute, Rome, I; 2University of Padova, Padova, I;
3
AMGA Foundation, Genova, I; 4CNR-IRSA, Brugherio, MB, I;
5
University “Sapienza”, Rome, I
P2-G-626-TH
Speciation Analysis of Gd-Based MRI Contrast Agents in Wastewater Treatment
Plants
Lena Telgmann, Christoph Wehe, Jens Künnemeyer, Uwe Karst
University of Münster, Münster, D
150
P2-G-627-WE
Study of the Spoilage of Fish Sauce by the Evaluation of Biogenic Amines Amount
using a Micellar Liquid Chromatography-Based Method after Derivatization with
3,5-Dinitrobenzoyl Chloride
Mei-Liang Chin-Chen1, Samuel Carda-Broch1, Juan Peris-Vicente1, Maria Rambla-Alegre1,
Josep Esteve-Romero1, Beatriz Beltrán-Martinavarro1, Sergio Marco-Peiró1,
Inmaculada Casas-Breva2
1
Universitat Jaume I, Castello, E; 2Hospital La Plana, Vila-real, E
P2-G-628-TH
Tannin Analysis by HPLC-DAD-MS of Chestnut Bark Extracts (Castanea sativa Mill.)
Patrizia Comandini1, María Jesús Lerma-García2, Jose Manuel Herrero-Martínez2,
Ernesto Francisco Simó-Alfonso2, Tullia Gallina Toschi1
1
University of Bologna, Cesena, FC, I;
2
University of Valencia, Burjassot, Valencia, E
P2-G-629-WE
The Dog Ate my Homework. The Instrument Ate my Peak. Contamination and
———————————————
Quenching During HPLC Analysis of Petroleum Hydrocarbons
Lori Sanford, Michael Woodman
Agilent Technologies, Schaumburg, IL, USA
P2-G-630-TH
The Use of Chromatographic Techniques for Substance Characteristic on the Needs
of the REACH System Registration
Grzegorz Boczkaj1, Mariusz Jaszczołt1, Anita Skrzypczak1,2, Sebastian Zalewski1,
Marian Kamiński1
1
Gdansk University of Technology, Gdansk, PL;
2
BLIRT Biolab Innovative Research Technologies, Gdansk, PL
P2-G-631-WE
The Use of HPLC/MS/MS for Identification and Determination of Explosives and
Related Degradation Products in Soil Samples
Zdeněk Šimek1, Ivana Ungrádová1, Jitka Bečanová1, Svatopluk Zeman2, Zdeněk Friedl3
1
Masaryk University, Brno, CZ; 2University of Pardubice, Pardubice, CZ;
3
Brno University of Technology, Brno, CZ
P2-G-632-TH
Transport Evaluation of the Herbicide Diuron and its Metabolites Simultaneously
Detected by HPLC-DAD
Ana Lúcia de Souza Madureira Felício1, Maria Josefa Santos Yabe1, Felipe Augusto Gorla1,
Elisa Yoko Hirooka2, Suzana Lucy Nixdorf1
1
151
P2-G-633-WE
UHPLC-MS/MS and UHPLC-HRMS for the Analysis of UV-Ink Photoinitiators in
Packaged Food
Hector Gallart-Ayala1, Oscar Núñez1, Claudia P. B. Martins2, Encarnación Moyano1,
Maria Teresa Galceran1
1
University of Barcelona, Barcelona, E;
2
Thermo Fisher Scientific, Barcelona, E
P2-G-634-TH
Ultra Low Level Determination of Bisphenol A and Poly Aromatic Hydrocarbons in
River Water Using Column-Stitching HPLC with Fluorescence Detection
Yoshiyuki Watabe1, Takashi Hine1, Tetsuya Tanigawa2, Takuya Kubo2, Ken Hosoya2
1
Shimadzu Corporation, Kyoto, J;
2
Tohoku University, Sendai, J
P2-G-635-WE
Ultra-High Pressure LC Method to Determine Astaxanthin in Shrimp By-Products and
Migration Evaluation from an Active Plastic Film Produced with Shrimp Waste to
Fatty Food Simulants
A. Sanches-Silva1, T. Ribeiro1, P. Paseiro2, R. Sendón2, A. Rodriguéz-Bernaldo de Quirós2,
J. López-Cervantes3, D. I. Sánchez-Machado3, H. Soto-Valdez4, I. Angulo5, G. Aurrekoetxea5,
H. S. Costa1
1
National Health Institute Dr Ricardo Jorge, Lisboa, P;
2
University of Santiago de Compostela, Santiago de Compostela, E;
3
Instituto Tecnologico de Sonora, Sonora, MEX;
4
Centro de Investigacion en Alimentacion y Desarrollo, Sonora, MEX;
5
Gaiker, Technological Center, Zamudio, E
P2-G-636-TH
Ultra-High Pressure LC to Determine α-Tocopherol and BHT in Active Plastic Films
and to Evaluate their Migration into a Fatty Food Simulant
Ana Sanches-Silva1, Helena S. Costa1, Tânia G. Albuquerque1, Giovanna Buonocore2
1
National Health Institute Dr Ricardo Jorge, Lisbon, P;
2
Institute for Composite and Biomedical Materials, Napoli, I
P2-G-637-WE
UPLC-MS/MS Method for the Determination of Triclabendazole Residues in Liver,
Muscle and Milk
Michelle Whelan1,2, John O’Mahony1, Mary Moloney1, Martin McCormack1,
Ambrose Furey2, Martin Danaher1
1
Teagasc, Ashtown Food Research Centre, Dublin, IRL;
2
Cork Institute of Technology, Cork, IRL
152
P2-G-638-TH
Validation Method of Syntetic Food Dyes in Fish by Reversed-Phase High-Performance
Liquid Chromatography with Diode-Array Detector
Francesca Longo, Rocco Baccelliere, Daniela Barchi, Laura Spinaci, Erica Romualdi,
Andrea Giorgi, Bruno Neri
Istituto Zooprofilattico Sperimentale delle Regioni Lazio e Toscana, Rome, I
P2-G-639-WE
WO3 Colloids Characterized through SdFFF and FlFFF
Catia Contado, Roberto Argazzi, Laura Ravani
Industrial Aspects of Separations
P2-G-640-TH
Development of Novel Stationary Phases for Supercritical Fluid Chromatography (SFC)
William Farrell1, Toshi Ono2, Tsunehisa Hirose3, Kazuhiro Kimata3
1
Pfizer Inc., Global Research & Development, San Diego, CA, USA;
2
Nacalai USA, Inc., San Diego, CA, USA;
3
Nacalai Tesque, Inc., Kyoto, J
P2-G-641-WE
Enhancement on SFC Chromatographic Performances by Fluidic Profile Optimization
Ziqiang Wang, Chuping Luo
SFC Division, Waters Corp. Newark, DE, USA
P2-G-642-TH
High Performance Carbon Dioxide Recycling for Supercritical Fluid Chromatography
John Whelan, Ziqiang Wang, Harbaksh Sidhu
SFC Division, Waters Corp., Newark, DE, USA
P2-G-643-WE
Improvement of Lab Scale SMB Operation by Pump Flow Control
Matthias Lübbert
Wissenschaftliche Gerätebau Knauer, Berlin, D
P2-G-644-TH
Isolation and Purification of Carbohydrates from Biological Sources by Recycling Liquid
Chromatography
William R. Alley, Jr., Benjamin F. Mann, Vlastimil Hruska, Milos V. Novotny
153
P2-G-645-WE
Method Development using an Advanced QbD Approach and Validation of the Design
Space Produced
Mia Summers, Peter Alden, Dominic Moore, Doug McCabe, Kenneth J. Fountain
P2-G-646-TH
Optimizing Chromatographic Media and Separation Conditions using Supercritical Fluid
Chromatography for Preparative Applications
Jo-Ann M. Jablonski, Kenneth J. Fountain, Steven M. Collier, Christopher J. Hudalla,
Damian Morrison
P2-G-647-WE
Pseudo-Intelligent Automated Mass-Directed HPLC Purification at AstraZeneca Charnwood
Phil Abbott, Alex Brien, Andrew Wright
AstraZeneca Charnwood, Leicestershire, UK
P2-G-648-TH
Quality by Design: Multidimensional Exploration of the Design Space in HPLC Method
Development for Better Robustness before Validation
I. Molnár1, H. J. Rieger1, Kate Monks1, B. Bogáti2, E. Szabó2
1
Molnár-Institute for Applied Chromatography, Berlin, D;
2
TEVA Hungary, Gödöllő, H
P2-G-649-WE
Special Injection Technique for External Recycle of Fractions with Insufficient Purity in
Preparative Reversed Phase Liquid Chromatography
Anita Prechl, György Balogh, Attila Rill
P2-G-650-TH
In Preparative Scale Gradient Reversed Phase Liquid Chromatography, Peak Shape as
a Function of pH, Buffer Concentration, and Mass Load for Basic Compounds are
Readily Rationalized Based on Secondary Chemical Equilibria in the Eluent
Xu Zhang, Chi Zhang, David P. Budac, Mark J. Hayward
Lundbeck Research USA, Inc., Paramus, NJ, USA
P2-G-651-WE
The Life CYCLE of an HPLC System – an Environmental Perspective
Laura Schneider1, Matthias Finkbeiner1, Alexandra Knauer2, Alexander P. Bünz2
1
Technische Universitat Berlin, Berlin, D;
2
Wissenschaftliche Gerätebau Dr. Ing. Herbert Knauer GmbH, Berlin, D
154
Pharmaceutical Analysis
P2-G-652-TH
A First of its Kind Walk-up LC/SFC-MS System
Muhammad Alimuddin, Wei Wang, William Farrell, Christine Aurigemma, Jennifer Lafontaine
Pfizer Global R&D, La Jolla, CA, USA
P2-G-653-WE
A New Pre-Column Derivatization Method for Determination of Roxarsone in Animal
Products by High-Performance Liquid Chromatography-UV Detection
Han Young Eom, Joon Hyuk Suh, Unyong Kim, Jeong-Rok Youm, Sang Beom Han
Chung-Ang University, Seoul, ROK
P2-G-655-WE
Analysis of Metabolically Produced Trifluoroacetaldehyde by Isotopedilution Mass
Spectrometry Coupled with Chromatography
Laszlo Prokai, Xiaoli Wang, Katalin Prokai-Tatrai
University of North Texas Health Science Center, Fort Worth, TX, USA
P2-G-656-TH
Analysis of Mianserin Hydrochloride by Capillary Electrophoresis Method using an
Experimental Design for Robustness
Letícia Lenz Sfair, Caren Gobetti, Alini Dall Cortivo Lange, Clésio Soldateli Paim,
Martin Steppe, Elfrides Eva Scherman Schapoval
Federal University of Rio Grande, Porto Alegre, RS, BR
P2-G-657-WE
Analytical SFC System Performance Qualification and Method Validation in Early
Development
Paul Carrick1, Adrian Davis1, Yun Huang2, Paul Rodwell1
1
Pfizer Global Research & Development, Kent, UK;
2
Groton Laboratories, Groton, CT, USA
P2-G-658-TH
Application of Automatic HPLC Method Development and Robustness Tests for
Separation of Terbinafine and its Impurities
Francois Vogel1, Iryna Shyshkina2, Sergey Galushko2
1
Novartis, Basel, CH; 2ChromSword, Muehltal, D
P2-G-659-WE
Application of HPLC and UHPLC Methods for Testing Dissolution Samples
Péter Tonka-Nagy, Dániel Kocsis, Jusztina Barta, Réka Szoleczky, Magda Leventiszné Huszár
EGIS Plc., Budapest, H
155
P2-G-660-TH
Application of HPLC-UV Method for the Determination of Faropenem Sodium in
Stability Studies
Judyta Cielecka-Piontek1, Aran Lunzer2
1
Poznan University of Medical Sciences, Poznań, PL; 2Hokkaido University, Sapporo, J
P2-G-661-WE
Application of HPLC-UV Method for the Stability Studies of
[(Nmorpholine)methylene]daunorubicin
Anna Krause1, Anna Jelińska2, Judyta Cielecka-Piontek2, Przemysław Zalewski2,
Irena Oszczapowicz3, Małgorzata Wa˛sowska3
1
GlaxoSmithKline Pharmaceuticals S.A., Poznań, PL; 2Poznan University of Medical
Sciences, Poznań, PL; 3Institute of Biotechnology and Antibiotics, Warsaw, PL
P2-G-662-TH
Automated Multidimensional UHPLC with UV-CAD-MSn Detection: Instrumentation,
Orthogonality and Applications in Pharmaceutical Analysis
Kelly Zhang, Yi Li, Midco Tsang, Nik P. Chetwyn
Small Molecule Analytical Chemistry and Quality Control, South San Francisco, CA, USA
P2-G-663-WE
Bioreactors Based on Human Purine Nucleoside Phosphorylase: Development,
Characterization and Validation
Marcela Cristina de Moraes1, Rodrigo G. Ducati2, Diógenes Santiago Santos2,
Carmen Lucia Cardoso3, Quezia Bezerra Cass1
1
Federal University of São Carlos, São Carlos, BR;
2
Pontifical Catholic University, Rio Grande do Sul, BR;
3
Faculty of Philosophy, Science and Letters of Ribeirão Preto, Ribeirão Preto, BR
P2-G-664-TH
Characterization of Gemifloxacin Mesylate Degradation Product by NMR and MS
Clésio Soldateli Paim, Fernanda Führ, Martin Steppe, Elfrides Eva Scherman Schapoval
Federal University of Rio Grande, Porto Alegre, RS, BR
P2-G-665-WE
Chemical Analytical Assistance of Generic Pharmaceutical Development
Ildikó Hanákné Székely, Péter Tonka-Nagy, Magda Leventiszné Huszár
P2-G-666-TH
Composite Samples – A Strategic Tool for HPLC Method Development
Mike McBrien, Andrey Vazhentsev, Alexey Galin
Advanced Chemistry Development, Toronto, CDN
156
P2-G-667-WE
Delapril and Manidipine Measurements by Liquid Chromatography-Tandem Mass
Spectrometry in Pharmaceutical Formulation
Vítor Todeschini, Diogo Miron, Maximiliano S. Sangoi, Nadia Maria Volpato
Federal University of Rio Grande do Sul, Porto Alegre, RS, BR
P2-G-668-TH
Determination and Separation of Sildenafil and its Impurities by Micellar Liquid
Chromatography
M. Rambla-Alegre1, J. Paños-Pérez2, D. Bose3, A. Durgbanshi3, N. Agrawal3,
M. A. Raviolo4, J. Esteve-Romero1, S. Carda-Broch1
1,2
Universitat Jaume I, Castello, E; 3Dr. H.S. Gour University, Sagar, IND;
4
Universidad de Córdoba, Córdoba, RA
P2-G-670-TH
Determination of Four Immunosuppressive Drugs in whole Blood using MEPS and
LC-MS/MS Allowing Automated Sample Work-up and Analysis
Rana Said
Karolinska Institute, Stockholm, S
P2-G-672-TH
Determination of Some Frequently Used Antibiotics from Waste Waters using High
Performance Liquid Chromatography
Ocsana Opriş1, Maria-Loredana Soran2, Costel Sârbu3, Florina Copaciu1, Virginia Coman4,
Dumitru Ristoiu1
1,3,4
“Babeş-Bolyai” University, Cluj-Napoca, RO; 2National Institute for Research and
Development of Isotopic and Molecular Technology, Cluj-Napoca, RO
P2-G-673-WE
Determination of the Gentiopicroside in Rat Blood and Bile for the Pharmacokinetics
and Biliary Excretion Studies by HPLC-UV and LCMS/MS
Wan-Ling Chang-Liao1, Lie-Chwen Lin1,2, Chao-Feng Chien1, Hsin-Ling Hsieh3,
Tung-Hu Tsai1,3
1
National Yang-Ming University, Taipei, RC;
2
National Research Institute of Chinese Medicine, Taipei, RC;
3
Taipei City Hospital, Taipei, RC
P2-G-675-WE
Development a Sensitive HPLC Method for Determination of Memantine in Human
Plasma using OPA Derivatization and Fluorescence Detection
Afshin Zarghi1, Farshid Abolfathi Araghi2
1
Shahid Beheshti University of Medical Sciences, Tehran, IR;
2
Noor Research and Educational Institute, Tehran, IR
157
P2-G-677-WE
Development and Validation of a HPLC Methods for the Determination of
Paracetamol, Rutin, Ascorbic and Succinic Acids in Paediatric Oral Suspension
Liubov Oliferova, Yuri Khomyakov, Andrei Mihalev, Rimma Abramovich
Peoples’ Friendship University of Russia, Moscow, RUS
P2-G-678-TH
Development and Validation of a Rapid HPLC Method for the Determination of
Ascorbic Acid, Phenylephrine, Paracetamol, Salicylic Acid (Internal Standard) and
Caffeine using a Monolithic Column
Petra Koblová, Hana Sklenářová, Ivana Brabcová, Petr Solich
P2-G-679-WE
Development and Validation of a Simple and Efficient HPLC Method for the
Determination of Zonisamide in Pharmaceuticals and Human Plasma
Duygu Yeniceli, Dilek Dogrukol-Ak
P2-G-680-TH
Development and Validation of a Thin-Layer Chromatographic/Densitometric Method
for the Quantitative Determination of 6-Amino-Benzoxazolone in Active Pharmaceutical
Ingredient
Katalin Varga, Mónika Babják, Mária Gazdag
P2-G-683-WE
Development of a Highly Sensitive UPLC-MS/MS Technique for the Simultaneous
Determination L-Ascorbic Acid and Acetylsalicylic Acid in Aspirin C Effervescent Tablet
Zeid Abdullah Alothman, Mohammad Rizwan Khan, Saikh Mohammad Wabaidur
King Saud University, Riyadh, SA
P2-G-684-TH
Development of a New HPLC Method for Determination of Related Substances of
Aprotinin
Gabriella Szabovik, Mónika Babják, Mária Gazdag
158
P2-G-685-WE
Development of an Analytical Methodology to Quantify Melamine in Dietetic
Supplements using Micellar Liquid Chromatography Coupled to Absorbance Detection
Juan Peris-Vicente1, Samuel Carda-Broch1, Josep Esteve-Romero1,
Maria Rambla-Alegre1, Sergio Marco-Peiró1, Beatriz Beltrán-Martinavarro1,
Adrian Martinavarro-Dominguez2, Enrique Ochoa-Aranda2
1
2
Hospital Provincial, Castellon de la Plana, E
P2-G-686-TH
Dried Blood Spots UHPLC-MS/MS Assay for the Analysis of Oseltamivir and
Oseltamivircarboxylaten (TamifluR) in Clinical Samples
Gero P. Hooff, Roland JW Meesters, Jeroen JA van Kampen, Nick A. van Huizen,
Birgit Koch, Asmar FY Al Hadithy, Teun van Gelder, Albert DME Osterhaus,
Rob A. Gruters, Theo M Luider
University Medical Center Rotterdam, Rotterdam, NL
P2-G-687-WE
Faster Method Development using Enhanced Selectivity for Various Fused-Core
Bonded Phases
Barry E. Boyes1, Timothy J. Langlois1, William L. Johnson1, Thomas J. Waeghe2,
Stephanie A. Schuster1
1
Advanced Materials Technology, Inc., Wilmington, DE, USA;
2
Mac-Mod Analytical, Inc., Chadds Ford, PA, USA
P2-G-688-TH
Fesoterodine Stress Degradation Behavior by LC-UV and LC-ESI-MS
Maximiliano S. Sangoi, Diogo Miron, Vítor Todeschini, Martin Steppe
Federal University of Rio Grande do Sul, Porto Alegre, RS, BR
P2-G-689-WE
Generic Method for Cytochrome P450 Metabolism Studies Employing Short End
Injection Capillary Electrophoresis Mode
Roman Řemínek, Jana Sedláčková, Eva Pakostová, Aleš Mádr, Zdeněk Glatz
Masaryk University, Brno, CZ
P2-G-690-TH
Green Bioanalysis: Investigations into the Use of Ethanol instead of Acetonitrile in
Routine, Generic Bioanalysis in Drug Discovery by Reversed-Phase LC-MS/MS
David N. Mallett
GlaxoSmithKline R&D, Herts, UK
159
P2-G-691-WE
High Performance Liquid Chromatography-Electrochemistry-Electrospray Ionization
Mass Spectrometry (HPLC-EC/ESI-MS) for Detection and Characterization of
Roscovitine Oxidation Products
Michal Karady1, Ondřej Novák1, Aleš Horna4,5, Miroslav Strnad2, Karel Doležal2,3
1,2
Palacky University and Institute of Experimental Botany ASCR, Olomouc, CZ;
3
Institute of Experimental Botany ASCR, Olomouc, CZ; 4RADANAL Ltd., Pardubice, CZ;
5
Tomas Bata University in Zlín, Zlín, CZ
P2-G-692-TH
High Resolution Accurate Mass MS and MS/MS for Pharmacokinetics Analysis of
Clozapine and Quantitation and Characterization of its Metabolite in Rat Plasma
Angelika Gratzfeld1, Na Pi2, Shane Tichy2, Adam Amaral3, Jakal Amin3, Panos Hatsis3,
Yuqin Dai2
1
Agilent Technologies, Inc., Waldbronn, D; 2Agilent Technologies, Inc., Santa Clara, CA, USA;
3
Novartis Institute for Biomedical Research, Inc., Cambridge, MA, USA
P2-G-693-WE
High Speed Separation of Clindamycin Phosphate and Process Impurities on Different
Columns Types
Silvia Marten
Mareike Naguschewski Knauer GmbH, Berlin, D
P2-G-694-TH
High-Performance Liquid Chromatographic Study of the Oscillatory Condensation with
L-Lactic Acid
Mieczysław Sajewicz, Dorota Kronenbach, Monika Gontarska, Teresa Kowalska
P2-G-695-WE
HILIC Applied to the Quantitation of Various Complex Oral Formulations; a Feasibility Study
Lee Kelepouris
McNeil AB, Helsingborg, S
P2-G-696-TH
HPLC Determination of Lutein, Zeaxanthin and Beta-Carotene in Dietary Supplements
Ivana Brabcová, Petra Koblová, Petra Dvořáková, Dalibor Šatínský, Petr Solich
P2-G-697-WE
HPLC Determination of Sibutramine in Pharmaceutical Tablets: Value of Different
Type of Stationary Phases
Goksel Arli, Nafiz Oncu Can
160
P2-G-698-TH
HPLC-ESI-MS Method for the Monitoring ABL Tyrosine Kinase
Hui Chen, Erwin Adams, Ann Van Schepdael
Katholieke Universiteit Leuven, Leuven, B
P2-G-699-WE
Identification of Antimicrobial Molecules from Fermentation Broth Produced by
Saccharomonospora sp. using RP-HPLC/ESI-SQMS
Ágota Pénzes1,2, Károly Hűvös1, Tibor Bartók3,4, Ákos Juhász5, József Péter Pallos1
1
PannonPharma Ltd, Pécsvárad, H; 2University of Pécs, Pécs, H;
3
University of Szeged, Szeged, H; 4Fumizol Ltd., Szeged, H;
5
PannonPharma cPlc, Pécs, H
P2-G-700-TH
Implementation of a Walk-Up, High Pressure, Capillary Ion Chromatograph for the
Fast Separation of Pharmaceutical Relevant Inorganic Anions and Cations
Terri Christison, Fei Pang, Khalil Divan
P2-G-701-WE
Impurity Fingerprints for the Identification of Counterfeit Medicines – A Feasibility
Study
Pierre-Yves Sacré1,4, Eric Deconinck1, Michal Daszykowski2, Patricia Courselle1,
Roy Vancauwenberghe5, Patrice Chiap3, Jacques Crommen4, Jacques O. De Beer1
1
Scientific Institute of Public Health, Brussels, B; 2The University of Silesia, Katowice, PL;
3
University Hospital of Liège, Liège, B; 4University of Liège, Liège, B;
5
Federal Agency for Medicines and Health Products, Brussels, B
P2-G-702-TH
Impurity Profiling of Carbamazepine by HPLC/UV
Terry Zhang, Guifeng Jiang, Sergio Guazzotti
P2-G-703-WE
In vitro HPLC-DAD/MS Study on Fluoroquinolones-Calcium Interaction
Katalin Pápai, Petra Füredi, Christopher Schlieper, Krisztina Ludányi, István Antal,
Imre Klebovich
Semmelweis University, Budapest, H
P2-G-704-TH
Investigation into the Stability of HILIC Based Cetirizine Assay
Richard Ludwig, Luisa Pereira, Tony Edge
Thermo Fisher Scientific, Runcorn, Cheshire, UK
161
P2-G-705-WE
Is it Really Necessary to Validate an Analytical Method or not? That is the Question
Maria Rambla-Alegre, Josep Esteve-Romero, Samuel Carda-Broch
Universitat Jaume, Castello, E
P2-G-706-TH
LC Method for Analysis of Aspirin and Clopidogrel and their Related Substances in
Combined Dosage Forms
Getu Kahsay, Ann Van Schepdael, Erwin Adams
Catholic University of Leuven, Leuven, B
P2-G-708-TH
LC/MS Analysis of Putative Hydrazone Metabolites in Plasma, Urine and Tissues in
Isoniazid Intoxication
Ivana Pasáková, Petra Kovaříková, Martin Štěrba, Olga Popelová, Eduard Jirkovský,
Jiří Klimeš
P2-G-709-WE
LC/MS Evaluation of Drug-Protein Interactions
Tomas Leek, Maria Lindskog
AstraZeneca R&D Molndal, Molndal, S
P2-G-710-TH
LC-MS Analysis of Cardioprotectant Dexrazoxane and its Active Metabolite
Petra Kovaříková, Ján Stariat, Jiří Klimeš
P2-G-711-WE
Measurement of Oseltamivir and its Metabolite, Oseltamivir Carboxylic Acid, in
Plasma, Placenta, Amniotic Fluid and Fetus for a Pregnant Rat by Liquid
Chia-Chun Lin1, Jiin-Cherng Yen1, Yu-Tse Wu2, Lie-Chwen Lin2,3, Tung-Hu Tsai2,4
1,2
National Yang-Ming University, Taipei, RC;
3
National Research Institute of Chinese Medicine, Taipei, RC;
4
Taipei City Hospital, Taipei, RC
P2-G-713-WE
Method Development in Pharmaceutical Industry
Channer Barbara, Goldschmidt Frédéric
Actelion Pharmaceuticals Ltd., Allschwil, CH
162
P2-G-714-TH
Micellar Liquid Chromatography in the Determination of Antibiotics: An Overview
M. Rambla-Alegre1, J. Paños-Pérez2, J. Péris-Vicente1, D. Bose3, A. Durgbanshi3,
N. Agrawal3, S. Carda-Broch1, J. Esteve-Romero1
1,2
3
Dr. H.S. Gour University, Sagar, IND
P2-G-715-WE
Micellar Liquid Chromatography: a Worthy Technique for the Analysis of Penicillin
Antibiotics in Urine and Pharmaceutical Samples
Maria Rambla-Alegre, Rosa Martí-Centelles, Josep Esteve-Salvador, Samuel Carda-Broch
P2-G-716-TH
Molecularly Imprinted Polymer of AMP – a Biomimetic Sensor of Nucleoside
Phosphorylation Mediated by Adenylate Kinase
K. Puzio, R. Delépée, F. Breton, A. Montagu, V. Roy, L. A. Agrofoglio
Universite d’Orléans, Orleans, F
P2-G-717-WE
On Simple Experimental Evidence on Supramolecular Aggregation and Aggregate
Mobility with S(+)-Naproxen in Aqueous Ethanol Solution
Mieczysław Sajewicz, Monika Gontarska, Teresa Kowalska
P2-G-718-TH
On-Line Electrochemistry/MS – A Powerful Technique for Rapid Prediction of Phase I
and II Drug Metabolism
Jean-Pierre Chervet, Agnieszka Kraj, Martin Eysberg
1 Antec, Zoeterwoude, NL
P2-G-719-WE
Partition Behavior of Pramipexole and its Five Impurities in Microemulsion Liquid
Chromatography
And– elija Malenović, Ana Vemić, Tijana Rakić, Nad– a Kostić, Biljana Jančić-Stojanović
University of Belgrade, Belgrade, SRB
P2-G-720-TH
Purity Analysis of Combined Drug Products by HPLC – New Challenges in the
Analytical Method Developement
Lívia Sipos-Szabó, Ilona Vígh
163
P2-G-721-WE
Rational Approach to Early Clinical Stage Pharmaceutical Stability Indicating Methods
Paul Ferguson, Paul Carrick, Justin van Duine, Fiona Harvey-Doyle, Ronan Huet, Paul Rodwell
Pfizer Global Research & Development, Sandwich, Kent, UK
P2-G-722-TH
Reversed Phase HPLC Analysis of Escitalopram in Pharmaceutical Tablets using C18
Bonded Monolithic Silica, Conventional C18 and Phenyl Columns
Nafiz Oncu Can, Goksel Arli
P2-G-723-WE
Robustness Test for Identification of Relevant Factors in HPLC Analysis for
Determination of Antifungal Isomers and Establishment of System Suitability Limits
Diogo Miron, Fernanda Batisti, Paulo Maiorga, Elfrides Eva Scherman Schapoval
Federal University of Rio Grande do Sul, Porto Alegre-RS, BR
P2-G-724-TH
RP-LC Method and Mass Spectrometry Detection for a Main Degradation Product of
Vildagliptin in Tablets
Amanda Thomas Barden, Bárbara Salamon, Diogo Miron, Elfrides Eva Scherman Schapoval,
Martin Steppe
Federal University of Rio Grande do Sul, Porto Alegre-RS, BR
P2-G-725-WE
Semi-Quantitative Analysis for High Throughput Screening of Compound Libraries
Frank Steiner, Ian N. Acworth, Christopher Crafts, Fraser McLeod
P2-G-726-TH
Separation Methods for Analysis of Cyclodextrin Derivatives
Katalin Csabai1, Erzsébet Varga1, Róbert Iványi1,2, Krisztina Ludányi3, László Tölgyesi4,
Gábor Varga5, Lajos Szente1, Julianna Szemán1
1
CycloLab R&D Ltd., Budapest, H; 2Bio-Sol-Dex Ltd., Kecskemét, H; 3Semmelweis
University, Budapest, H; 4Kromat Ltd., Budapest, H; 5ChiroQuest Ltd, Budapest, H
P2-G-727-WE
Separation of NiII(3-OMe-salophene) Complex from Related Compounds by LC:
Comparing the Application of 3 mm RP-18 Monolithic Silica and
Pentafluorophenylpropyl Fused Core Columns
Sami El Deeb1,2, Gerhard Wolber1, Ronald Gust3
1
Freie Universität Berlin, Berlin, D; 2Al-Azhar University-Gaza, Gaza, PS;
3
University of Innsbruck, Innsbruck, A
164
P2-G-728-TH
Simple Sensitive and Semi-Quantitative Analytical Approaches for Cleaning
Validation Studies
Philip DeLand, Ian N. Acworth, Christopher Crafts, Fraser McLeod, Frank Steiner
P2-G-729-WE
Simultaneous Determination of Protein Unbound Aspirin and Salicylic Acid in Rat
Blood and Brain by Microdialysis: An Application to Herbal-Drug Interaction
Lee-Hsin Shaw1, Tung-Hu Tsai1,2
1
National Yang-Ming University, Taipei, RC; 2Taipei City Hospital, Taipei, RC
P2-G-732-TH
Stability and Quality Evaluation of Pharmaceuticals using Ultra High-Speed Liquid
Chromatography
Hideko Kanazawa, Yoshiko Nagata
Keio University, Tokyo, J
P2-G-733-WE
Stability-Indicating HPLC Method for the Determination of Cefoselis Sulphate
Przemysław Zalewski, Judyta Cielecka-Piontek, Anna Jelińska
Poznań University of Medical Sciences, Poznań, PL
P2-G-734-TH
Stability-indicating LC Method for Determination of Sitagliptin and Cytotoxicity Assay
to the Degradation Products
Alini Dall Cortivo Lange, Franciele Tams Gasperin, Clésio Soldateli Paim,
Nadia Maria Volpato, Elfrides Eva Scherman Schapoval
Federal University of Rio Grande do Sul-UFRGS, Porto Alegre-RS, BR
P2-G-735-WE
Stability-Indicating LC Method for the Determination of Biapenem in the Presence of
Degradation Products
Judyta Cielecka-Piontek1, Anna Krause2, Marek Milewski2, Aran Lunzer3, Anna Jelińska1,
Przemysław Zalewski1
1
Poznań University of Medical Sciences, Poznań, PL; 2PozLab Contract Research
Organization Poznań, PL; 3Hokkaido University, Sapporo, J
P2-G-736-TH
Streamlined QbD HPLC Method Development with Automated Data Processing
Gang Xue1, Jeff Harwood1, Charles Cheng1, David Fortin1, Jian Wang1, George Reid1,
Mike McBrien2, Andrey Vazhentsev2
1
Pfizer Global R&D, Groton, CT, USA; 2Advanced Chemistry Development Inc., Toronto, CDN
165
P2-G-737-WE
Supercritical Fluid Chromatography for Analysis of Basic Drugs
Alexandre Grand-Guillaume-Perrenoud1, Joëlle Verne2, Bertrand Duléry2, Hélène Boiteux3,
Jean-Luc Veuthey1, Davy Guillarme1
1
University of Geneva, University of Lausanne, Geneva, CH;
2
Sanofi Aventis Research & Development, Strasbourg, F;
3
TharSFC, Waters Corporation, Guyancourt, F
P2-G-738-TH
The Analysis of Opiate Alkaloids using Two-Dimensional Reverse Phase-Reverse Phase
High Performance Liquid Chromatography with UV-Absorbance, Chemiluminescence
and Mass Spectrometry Detection
Tiffany A. Goodie1, Xavier A. Conlan2, R. Andrew Shalliker3,4, Neil W. Barnett1
1
Deakin University, Waurn Ponds, VIC, AUS; 2Deakin University, Geelong, VIC, AUS;
3
University of Western Sydney, Parramatta, AUS;
4
University of Western Sydney, Penrith South, AUS
P2-G-739-WE
The Benefits of 2D-LC in Pharmaceutical R&D
Rudy Sneyers, Jeroen Peeters, Luc van Grieken, Gaby Török
Janssen Pharmaceutical Companies of Johnson & Johnson, Beerse, B
P2-G-740-TH
The use of HILIC as an Alternative Strategy to RPLC for Pharmaceutical Applications
Josephine Ruta, Serge Rudaz, Jean-Luc Veuthey, Davy Guillarme
P2-G-741-WE
Ultra Performance Liquid Chromatography coupled to Mass Spectrometry
Determination of Cholecalciferol and its Derivatives in a Pharmaceutical Oily Matrix
R. Klinkenberg1, B. Mertens1, B. Cahay1, J. Harzimont1, F. Vanderbist2, B. Streel1
1
Galephar M/F, Marche en Famenne, B; 2Laboratoires SMB, Brussels, B
P2-G-742-TH
UPLC Method for Simultaneous Determination of Cefalexin and its Impurities in
Capsules
Vesna Mijatović, Vesna Zabelaj
Medicines and Medical Devices Agency of Serbia, Belgrade, SRB
P2-G-743-WE
UPLC-MS/MS of Cephalosporin Antibiotics in Support of Cleaning Validation
Alexander H. Schmidt
Steiner & Co., Deutsche Arzneimittelgesellschaft mbH & Co. KG, Berlin, D
166
P2-G-744-TH
Use of Charged Aerosol Detection as an Orthogonal Quantification Technique for Drug
Metabolites in Safety Testing (MIST)
Frank Steiner, Christopher Crafts, Ian N. Acworth, Fraser McLeod
P2-G-745-WE
Use of Electrochemical Flow Cells to Facilitate Early Stage Characterization of Drug
Metabolites and Reactive Species
Ian N. Acworth, Paul Gamache, Frank Steiner, Fraser McLeod
P2-G-746-TH
USP Website on HPLC Column Equivalency
Margareth R. Marques
US Pharmacopeia, Rockville, MD, USA
P2-G-747-WE
Utilizing of a Novel Organic/inorganic Hybrid C18 Column for Efficient Method
Development over a Wide pH Range
Noriko Shoji, Takashi Sato, Chie Yokoyama, Takatomo Takai, Naohiro Kuriyama
P2-G-748-TH
Validating Analytical Methods with Charged Aerosol Detection
Fraser McLeod, Christopher Crafts, Ian N. Acworth, Frank Steiner
Data Analysis and Chemometrics
P2-S-749-WE
A Complete Solution for Method Linearity in HPLC and UHPLC
Frank Steiner, Tobias Fehrenbach, Susanne Fabel, Andreas Brunner, Fraser McLeod
P2-S-750-TH
A Strategy for Assessing Information Content in Dual Mode UPLC-MS Fingerprinting
Data: Platform Selection for Analysis of Complex Uncharacterized Samples
Nikoline Juul Nielsen1, Giorgio Tomasi2, Jan H. Christensen1
1
University of Copenhagen, Frederiksberg C, D;
2
European Commission Joint Research Centre, Ispra (Varese), I
167
P2-S-751-WE
Adequate Criteria for the Development of Robust Comprehensive Two-Dimensional
Chromatography Liquid Methods
P. F. Vanbel, P. J. Schoenmakers
P2-S-752-TH
An Approach Based on the Peak Count Concept Oriented to the Full Resolution of
Complex Mixtures
José Ramón Torres-Lapasió1, Alberto Ortín2, María Celia García-Álvarez-Coque1
1
Universitat de València, Burjassot, E;
2
Polymer Characterization, S. A., Paterna, E
P2-S-753-WE
Characterization of the Carbohydrate Content in Different Grains using HPLC-HPAE-PAD
and Chemometrics to Evaluate Adulteration in Roasted and Ground Coffee
Elis Daiane Pauli, Julia Estéfane Martins de Abreu, Diego Soares Domingues,
Suzana Lucy Nixdorf
P2-S-754-TH
Comparison of the Quantitative Performances and Measurement Uncertainty
Estimates Obtained during Method Validation versus Routine Applications of a Novel
Hydrophilic Interaction Chromatography Method for the Determination of Cidofovir in
Human Plasma
F. Lecomte1, B. Streel2, C. Hubert1, S. Demarche1, C. De Bleye1, A. Dispas1, M. Jost4,
F. Frankenne4, A. Ceccato3, E. Rozet1, Ph. Hubert1
1
2
Galephar MF, Marche-en-Famenne, B;
3
Odyssea Pharma, Grace-Hollogne, B;
4
Mithra Pharmaceuticals, Liège, B
P2-S-755-WE
Computer-Assisted Optimization in the Development of a Robust RPLC Method for the
Analysis of Some Phenolics Pollutants
L. Didaoui, A. Touabet
Université des Sciences et de la Technologie Houari Boumediene (USTHB), Alger, DZ
P2-S-756-TH
Evaluation of Regression Models during Validation of Bioanalytical Assays measured
by HPLC/MS
A. Jakab, F. Picard, O. Kretz
Novartis Institutes for Biomedical Research, Basel, CH
168
P2-S-757-WE
HPLC Peak Area Precision Improves with Increasing Signal to Noise Ratios
Christoph Meyer1, Patricia Seiler1, Veronika R. Meyer2
1
Novartis Pharma AG, Basel, CH; 2EMPA, St. Gallen, CH
P2-S-758-TH
Implementation of a Design Space Approach for Enantiomeric Separations in Polar
Organic Solvent Chromatography
Iolanda Nistor1,2, Pierre Lebrun1, Attilio Ceccato3, Fred Lecomte1, Ines Slama4,
Eric Rozet1, Radu Oprean2, Eduard Badarau5, Fabien Dufour5, Jean-François Liégeois5,
Philippe Hubert1
1,5
2
University of Medicine and Pharmacy ‘Iuliu Hatieganu’, Cluj-Napoca, RO;
3
Galephar MF, Marche-en-Famenne, B;
4
Advanced Institute of Environmental Science and Technology, Hammam-Lif, TN
P2-S-759-WE
Improved Outlier Detection using the Combination of R-NN Curves with other
Conventional Algorithms
Xi Deng, Sebastian Rohrer, Simone Schröder, Thomas Hahne, Hermann Wätzig
Technical University Braunschweig, Braunschweig, D
P2-S-760-TH
Noise Filtering: the Ultimate Solution
Yuri Kalambet1, Yuri Kozmin2, Sergey Maltsev1
1
Ampersand Ltd., Moscow, RUS; 2Institute of Bioorganic Chemistry RAS, Moscow, RUS
P2-S-761-WE
Precision of Peak Area and Height Determination
Veronika R. Meyer
EMPA, Swiss Federal Laboratories for Materials Science and Technology, St. Gallen, CH
P2-S-762-TH
Software Application for Active Sharing of One HPLC Autosampler Unit with Several
(Indepently running) HPLC Lines Under Dionex Chromeleon Control
Wolf Freinbichler, Rainer W. Schmid
P2-S-763-WE
Time-Alignment in HPLC-MC Based on Blank Measurement
Jan Urban1, Pavel Hrouzek2, Jan Vaněk1, Jiří Kopecký2, Dalibor Štys1
1
University of South Bohemia, Nove Hrady, CZ;
2
Institute of Microbiology, Academy of Sciences of the Czech Republic, Třeboň, CZ
169
P2-S-764-TH
Variable Solvent Content and pH Optimal Experimental Designs Based on Prediction
Error Surfaces
José Ramón Torres-Lapasió, Juan José Baeza-Baeza, María Celia García-Álvarez-Coque
P2-S-765-WE
Verification of Coffee Quality by Chemometrics and Chromatographic Profiles of
Arabica and Canephora Coffea, Husks and Sticks
Elis Daiane Pauli, Francieli Barbieri, Ieda Spacino Scarminio,
Carlos Alberto Paulinetti da Camara, Suzana Lucy Nixdorf
P2-S-766-TH
Brij-35, an Organic Modifier for Green Reversed-Phase Liquid Chromatography
María José Ruiz-Ángel, Juan José Fernández-Navarro, María Celia García-Álvarez-Coque
Reteniton Mechanisms and Retention Models
P2-S-767-WE
Determination of the Interparticle Void Volume in Packed Beds via Donnan Exclusion
Daniela Stoeckel1,2, Stefanie Jung2, Ulrich Tallarek2
1
Justus-Liebig-University of Giessen, Giessen, D;
2
Philipps-University of Marburg, Marburg, D
P2-S-768-TH
Development of a LSER Model for Identification of Unknowns in Environmental
Samples
Nadin Ulrich, Werner Brack
Helmholtz Centre for Environmental Research, Leipzig, D
P2-S-769-WE
Effective Teaching Techniques using a Virtual Chromatography Laboratory
Michael McBrien
Advanced Chemistry Development Inc. (ACD/labs), Toronto, CDN
P2-S-770-TH
Mechanistic Investigations of Alternative Retention and Selectivity using
Pentafluorophenyl Stationary Phases in Reversed-Phase Liquid Chromatography
David S. Bell, Craig Aurand, Anders Fridstrom, Frank Michel
Sigma-Aldrich/Supelco, Bellefonte, PA, USA
170
P2-S-771-WE
Prediction of the Retention of Ionizable Analytes under RP-HPLC Gradient Elution by
Means of a Chromatographic Model
Axel Andrés, Adolfo Téllez, Elisabeth Bosch, Martí Roses
P2-S-772-TH
Retention Studies in Liquid Chromatography at Different Mobile Phase Compositions
and at Moderately Elevated Temperatures by using the Solvation Parameter Model
Agustin Acquaviva, Javier Gotta, Cecilia Castells, Mario Reta
Universidad Nacional de La Plata (UNLP), La Plata, RA
P2-S-774-TH
Study of Retention Mechanism in HILIC in Terms of Deuterium Isotope Effect
Tomoyuki Okada, Tohru Ikegami, Masatoshi Miyamoto, Nobuo Tanaka
Kyoto Institute of Technology, Kyoto, J
P2-S-775-WE
Study of Retention of Several Pesticides in Gradient Elution
Grazielle de Campos Anaia, João Pedro Simon Farah, Marina Franco Maggi Tavares
University of Sao Paulo, Sao Paulo, BR
P2-S-776-TH
The Hydrophobic-Subtraction Model and Reversed-Phase Selectivity – A Simplified
Look at Column Phase Selection
Ty Kahler, Rick Lake, Steve Kozel, Mike Wittrig, Bruce Albright, Chris Denicola
P2-S-777-WE
Toward a Better Understanding of Retention Behavior in Chromatography by
Comparison of HPLC and Suspended-State HR/MAS-NMR-Spectroscopy
Helen Yeman1, Maria T. Matyska2, Joseph J. Pesek2, Paul Schuler1, Klaus Albert1
1
University of Tübingen, Tübingen, D;
2
San Jose State University, San Jose, CA, USA
P2-S-778-TH
Using “F Factor” for Prediction of the Retention of Anthraquinone Derivatives on C18
Stationary Phases
Witold Nowik1,2, Alain Tchapla1, Benoît Chauvin3, Myriam Bonose1, Sylvie Heron1,
Pierre Chaminade3
1
Université Paris-Sud, Orsay, F;
2
Laboratoire de Recherche des Monuments Historiques, Champssur-Marne, F;
3
Université Paris-Sud, Chatenay-Malabry, F
171
Sample Preparation
P2-S-779-WE
A Problem of the Sample Preparation with Orthogonal Separation System
GPC/NP-HPLC for Quantitative Analysis of Polycyclic Aromatic Hydrocarbons in
High-Boiling Petroleum Products by GCMS and RP-HPLC-FLD
Grzegorz Boczkaj, Ewelina Gilgenast, Mariusz Jaszczołt, Marian Kamiński
P2-S-780-TH
An On-Line Approach towards Unbreakable Sol-Gel-Based In-Tube Solid Phase
Microextraction
Habib Bagheri, Hamed Piri-Moghadam, Ali Es’haghi
Sharif University of Technology, Tehran, IR
P2-S-781-WE
Application of Novel Sorbent Phases in Adsorptive Micro-Extraction Techniques for
the Analysis of Persistent Organic Pollutants in Environmental Matrices
Carlos V. P. Almeida, Andreia Alegre, José M. F. Nogueira
University of Lisbon, Lisbon, P
P2-S-782-TH
Automated Ion Chromatographic Determinations over Six Orders of Magnitude
Adrian Ueberwasser, Thomas Hartmann, Andrea Wille
Metrohm International Headquarters, Herisau, CH
P2-S-783-WE
Bar Adsorptive Micro-Extraction (BA μE): A Novel Analytical Approach for the
Determination of Phenolic Compounds in Water Matrices
Nuno R. Neng, Paulo J. A. Madeira, Maria H. Florêncio, José M. F. Nogueira
University of Lisbon, Lisbon, P
P2-S-784-TH
Comparison between Sol-Gel Hybrid and Polymer Coatings for Stir Bar Sorptive
Extraction of Non-Steroidal Anti-Inflammatory Drugs in Human Urine
Wan Aini Wan Ibrahim1,2, Aemi Syazwani Abdul Keyon2, Niki Prastomo3, Atsunori Matsuda3,4
1,2
Universiti Teknologi Malaysia, Johor Bahru, MAL;
3,4
Toyohashi University of Technology, Tempaku, J
P2-S-785-WE
Comparison of the Measurement Accuracy of Automated and Manual Analytical Pipettes
L. Pereira, J. Gartland, K. Meadows, S. Aspey, M. Oliver
172
P2-S-786-TH
Coupling RP SPE Sample Preparation and HILIC Chromatography for Increased
Sample Throughput, Applied for Serotonin Determination
Petrus Hemstrom
Merck Sequant AB, Umeå, S
P2-S-787-WE
Determination of Additives in Diesel Fuels by Coupling LC/GC with a Various Methods
of Detection
Grzegorz Boczkaj, Mariusz Jaszczołt, Marian Kamiński
P2-S-788-TH
Determination of Ciprofloxacin Preconcentration Efficiency of Fourteen Different SPE
Sorbents
Judith Elumeze, Okechukwu Clinton Ifegwu, Peter Farotade, Olutoun Sanusi, Bayo Olajide,
Chimezie Anyakora
University of Lagos, Lagos, NGR
P2-S-789-WE
Determination of Feminizing Chemicals in Sediment and Biota using One- and
Two-Dimensional Ultra-High Performance Liquid Chromatography/Tandem Mass
Spectrometry
W.-L. Chen, G.-S. Wang, C.-Y. Chen
P2-S-790-TH
Determination of Ibuprofen Preconcentration Efficiency of Fourteen Different SPE
Sorbents
Morenike Akinyemi, Okechukwu Clinton Ifegwu, Kenneth Nwaeze, Tomi Majekodunmi,
Sixtus Amadi, Chimezie Anyakora
University of Lagos, Lagos, NGR
P2-S-791-WE
Determination of Pesticide Residues in Seaweeds by Pressurized Liquid Extraction
(PLE) and Liquid Chromatography – Mass Spectrometry in Tamdem Detection
Antonia M. Carro, Sandra Pais, Inés Racamonde, Rafael Cela, Diego García-Rodríguez,
Rosa A. Lorenzo
University of Santiago de Compostela, Santiago de Compostela, E
173
P2-S-793-WE
Development of In-Tube Molecularly Imprinted Polymer Solid-Phase Microextraction
for Selective Interferon Determination in Plasma Sample
Andréa Rodrigues Chaves, Lidervan de Paula Melo, Fernando Mauro Lanças,
Maria Eugênia Costa Queiroz
Universidade de São Paulo, Ribeirão Preto, São Carlos, SP, BR
P2-S-794-TH
Development of MEPS as the Sample Preparation Technique for UHPLC-MS/MS
Determination of Atorvastatin, Rosuvastatin and their Metabolites in Biological Samples
Hana Vlčková, Lucie Nováková, Jiří Plíšek, Milan Bláha, Petr Solich
P2-S-795-WE
Evaluation of Carbon Nanotube as Adsorbent for Solid Phase Extraction of Benzoic
Acid Compounds by High Performance Liquid Chromatography
M. Amirzehni, S. Baikzade
Islamic Azad University-Tabriz Branch, Tabriz, IR
P2-S-796-TH
Expanding the Performance of Analytical Extractions of Solid Samples Based on Ionic
Liquid-Surfactants: In Situ Ionic Liquid Preconcentration
Mónica Germán-Hernández1, Verónica Pino1, Jared L. Anderson2, Ana M. Afonso1
1
Universidad de La Laguna, La Laguna, Tenerife, E;
2
The University of Toledo, Toledo, OH, USA
P2-S-797-WE
High-Throughput Sample Preparation and Analysis for Biomarker Verification and
Validation: Towards 1,000 Samples a Day
Brianne Petritis1, Mark Holl2, Deirdre Meldrum2, Matthew Rosenow3, Michael Gaskin1,
Joshua LaBaer1, Konstantinos Petritis3
1,2
Arizona State University, Tempe, AZ, USA;
3
The Translational Genomics Research Institute (TGen), Phoenix, AZ, USA
P2-S-798-TH
Lanthanum (III) Precipitation – A New Highly Selective Sample Preparation Method for
Phosphor and Glycoprotein Isolation and Analysis
Fabio Polato 1, Matthias Rainer 1, Thomas Ringer 1, Rania Bakry 1, Johan Gobom 2,
Henrik Zetterberg 2, Kai Blennow 2, Douglas Djerde 3, Christian W. Huck 1,
Gunther K. Bonn 1
1
Leopold-Franzens University, Innsbruck, A;
2
The Sahlgrenska Academy at the University of Gothenburg, Göteborg, S;
3
PhyNexus, Inc., San Jose, CA, USA
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P2-S-800-TH
Molecularly Imprinted Polymers for Selective Extraction of Selected Mycotoxin in
Various Matrices
Renata Gadzala-Kopciuch, Michal Szumski, Boguslaw Buszewski
Nicolaus Copernicus University, Toruń, PL
P2-S-801-WE
New SPE-Materials Based on Different Fullerene-Derivatives for the Enrichment and
the Fractionation of Phosphopeptides
Martin Fischnaller, Rainer Vallant, Rania Bakry, Günther K. Bonn
Leopold-Franzens University, Innsbruck, A
P2-S-803-WE
Novel Sol-Gel Hybrid Methyltrimethoxysilane-Tetraethoxysilane as Sorbent for Solid
Phase Extraction
Wan Aini Wan Ibrahim, Krishna Veni Veloo, Mohd. Marsin Sanagi
Universiti Teknologi Malaysia, Johor Bahru, MAL
P2-S-804-TH
Optimization of Matrix Solid-Phase Dispersion and LC-MS-MS Confirmatory
Determination of Pesticides Residues in Fish and Shellfish
Rosa A. Lorenzo, Diego García-Rodríguez, Rafael Cela,
Inés Racamonde Antonia M. Carro
University of Santiago de Compostela, Santiago de Compostela, E
P2-S-805-WE
Preparation and Application of New Polar Coatings for Stir Bar Sorptive Extraction of
Polar Contaminants from Complex Environmental Water Samples
N. Fontanals1, D. Bratkowska1, P. A. G. Cormack2, F. Borrull1, R. M. Marce1
1
University Rovira i Virgili, Tarragona, E; 2University of Strathclyde, Glasgow, UK
P2-S-806-TH
Sample Filtration Prior to HPLC: A New Vacuum Based Device Improves Work-Flow
and Ergonomics
Vivek Joshi, Marc Emerick, Chris Scott
Merck-Millipore Corp., Danvers, MA, USA
P2-S-807-WE
Selective Extraction of Nitroaromatic Explosives Residues in Post Blast Samples by
Molecularly Imprinted Silica Sorbents
Sonia Lordel1,2, Florence Chapuis-Hugon1, Véronique Eudes2, Valérie Pichon1
1
ParisTech-CNRS-UPMC, Paris, F;
2
Laboratoire Central de la Prefecture de Police, Paris, F
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P2-S-808-TH
Simple Extraction Procedure for Chromatographic Analysis of Aliphatic Amines in
Fermented Beverages
Inês M. Valente, Manuel P. Cruz, José A. Rodrigues, Aquiles A. Barros
Universidade do Porto, Porto, P
P2-S-809-WE
Simplified Measurement of Partition Coefficient by Means of the Pretreatment
Function in the Auto-Sampler
Yusuke Osaka, Keiko Yamabe, Yoshiaki Maeda, Junichi Masuda, Masatoshi Takahashi,
Yoshihiro Hayakawa
Shimadzu Corporation, Kyoto, J
P2-S-810-TH
Temperature On-Line Preconcentration in Capillary Zone Electrophoresis. Application
to Carboxylic Acids
Marcos Tascón1, Leonardo G. Gagliardi1,2,3, Fernando Benavente3
1
Universidad Nacional de La Plata, La Plata, RA;
2
Centro de Investigacion y Desarrollo en Tecnologia de Pinturas, La Plata, RA;
3
P2-S-811-WE
Thermal Degradation Studies of Alkaloids in Goldenseal during Selective Extraction by
Pressurized Hot Water
Janes Mokgadi1, Charlotta Turner2, Nelson Torto1
1
Rhodes University, Grahamstown, ZA;
2
Lund University, Lund, S
P2-S-812-TH
Three-Phase Hollow Fiber Liquid-Phase Microextraction Applied to Organophosphorous
Nerve Agent Degradation Products in Complex Matrices
Desoubries Charlotte1, Chapuis-Hugon Florence1, Bossée Anne2, Pichon Valérie1
1
UMR PECSA, Paris, F;
2
DGA CBRN, Vert Le Petit, F
Theoretical Models and Insights
P2-S-814-TH
A Theoretical Model to Account for Slow Kinetics in Chromatographic Elution
Juan José Baeza-Baeza, María Celia García-Álvarez-Coque
Universitat de Valencia, Burjassot, E
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P2-S-815-WE
Adsorption Energy of Proteins on Hydrophobic Interaction Chromatography Surfaces
Agnes Rodler1, René Ueberbacher2, Rainer Hahn1,2, Alois Jungbauer1,2
1
Austrian Centre of Industrial Biotechnology, Vienna, A;
2
University of Natural Resources and Life Sciences Vienna, Vienna, A
P2-S-816-TH
Analysis of Mass Transport in Monoliths: from Physical Reconstruction of Morphology
to Pore-Scale Simulation
Dzmitry Hlushkou, Stephan Bruns, Ulrich Tallarek
P2-S-817-WE
Application of the Linear Solvent Strength Model of Gradient Elution to Short, Steep
Gradients used in LC-MS/MS Analyses: Effect of Flow Rate on Resolution
Anne Aubry, Jian Wang, Jingpin Jia, Mark Arnold, Mohammed Jemal
Bristol-Myers Squibb, Research & Development, Princeton, New Brunswick, NJ, USA
P2-S-818-TH
Characterization of the Adsorption of Racemic Methyl Mandelate on
Tris-(3,5-dimethylphenyl)carbamoyl Cellulose Chiral Stationary Phase
Martin Enmark, Jorgen Samuelsson, Torgny Fornstedt
P2-S-819-WE
Chromatographic Behaviour of Aminoalcohols
Cristina Corral1, Xavier Subirats1, Javier Gotta2, Leonardo G. Gagliardi2,
Cecilia B. Castells2, Clara Ràfols1, Martí Rosés1, Elisabeth Bosch1
1
Universitat de Barcelona, Barcelona, E; 2Universidad Nacional de La Plata, La Plata, RA
P2-S-820-TH
Comparison of Band Broadening and Thermal Behavior of Constant Flow Rate- and
Constant-Pressure HPLC
Ken Broeckhoven1, Matthias Verstraeten1, Gert Desmet1, Konstantin Choikhet2,
Klaus Witt2, Monika Dittmann2
1
VUB, Brussels, B; 2Agilent Technologies, Waldbronn, D
P2-S-821-WE
Composition and Structure of Water-Acetonitrile Mixtures in a Silica Nanopore
Studied by Molecular Dynamics Simulations
Sergey M. Melnikov1, Alexandra Höltzel2, Andreas Seidel-Morgenstern1,3, Ulrich Tallarek2
1
Max-Planck-Institut fur Dynamik komplexer technischer Systeme, Magdeburg, D; 2PhilippsUniversität Marburg, Marburg, D; 3Otto-von-Guericke-Universität Magdeburg, Magdeburg, D
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P2-S-822-TH
Determination of Suitable Column Geometries by Means of Gradient Kinetic Plots for
Method Development in High-Temperature Liquid Chromatography Isotope Ratio Mass
Spectrometry
Paul Ermisch1, Thorsten Teutenberg1, Vanessa Kreuzer2, Harald Weber2
1
2
Niederrhein University of Applied Science, Krefeld, D
P2-S-823-WE
Determination of the 1-Octanol/Water Partition Coefficient (logPo/w) of Basic Drugs
by a Chromatographic Method
Juan M. Pallicer, Joaquim Sales, Martí Rosés, Clara Ràfols, Elisabeth Bosch
P2-S-824-TH
Extra-Column Dispersion Contributions of Individual System Components: Impact on
the Performance of Modern High Efficiency (U)HPLC Columns
Monika M. Dittmann, Konstantin Choikhet
Agilent Technologies GmbH, Waldbronn, D
P2-S-825-WE
High-Performance Computing of Hydrodynamic Dispersion in Cylindrical Packed Beds
of Different Aspect Ratios
Siarhei Khirevich, Alexandra Höltzel, Ulrich Tallarek
P2-S-826-TH
Impact of pH and Ligand Density on Protein Adsorption Capacity on Grafted Cation
Exchangers
Katarzyna Wrzosek, Milan Polakovič
Slovak University of Technology, Bratislava, SK
P2-S-827-WE
Influence of Particle Characteristics on the Radial Heterogeneity, Porosity, and
Column Performance of Slurry-Packed Particulate Columns
Daniela Stoeckel1,2, Stefan Bruns2, Bernd Smarsly1, Ulrich Tallarek2
1
Justus-Liebig-University of Giessen, Giessen, D; 2Philipps-University of Marburg, Marburg, D
P2-S-828-TH
Intrinsic Influence of the Particle Size Distribution on Hydraulic Permeability and Eddy
Dispersion in Bulk Packings
Anton Daneyko, Alexandra Höltzel, Siarhei Khirevich, Ulrich Tallarek
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P2-S-829-WE
Inverse Chromatography for Determination of Surface Energy Hydrophobic Interaction
Chromatography Material
Ingeborg Bednar1, Rupert Tscheliessing1, Eva Berger1, Nika Lendero2, Ales Podgornik2,
Alois Jungbauer1,3
1
Austrian Centre of Industrial Biotechnology, Vienna, A;
2
BiaSeparations, Ljubljana, SLO;
3
University of Natural Resources and Life Sciences Vienna, Vienna, A
P2-S-830-TH
New Simulations in Capillary Isoelectric Focusing
Anna Takácsi-Nagy1, Wolfgang Thormann2, Ferenc Kilár1,3
1,3
University of Pécs, Pécs, H; 2University of Bern, Bern, CH
P2-S-831-WE
Partition Coefficient, Distribution Ratio and Distribution Constant: How Definitions Act
on Benzoic Acid Peak in Countercurrent Chromatography
Alain Berthod, Nazim Mekaoui
P2-S-832-TH
Prediction of Chromatographic Parameters of Multiprogrammed Reversed Phase
HPLC Analyses
János Harangi1, Ákos Pintér2
1
University of Pannonia, Veszprém, H; 2University of Debrecen, Debrecen, H
P2-S-833-WE
Recent Developments on the Elution by Characteristic Points Method for Rapid and
Accurate Determination of Adsorption Isotherms
Jörgen Samuelsson, Torgny Fornstedt
P2-S-834-TH
Retention and Mass-Transfer Properties of Insulin on Porous and Core-Shell Packing
Materials
Ibolya Kiss, Attila Felinger
P2-S-835-WE
Surface Heterogeneity below an Adsorbed Multilayer
Péter Vajda1, Krisztián Horváth2, Attila Felinger1
1
2
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P2-S-836-TH
The Optimal Designs for Reversed-Phase High Performance Liquid Chromatography
Experiments
Paweł Wiczling, Roman Kaliszan
Medical University of Gdansk, Gdansk, PL
P2-S-837-WE
The Tracer-Pulse Experience – “Reviling the Invisible Iceberg”
Torgny Fornstedt, Jörgen Samuelsson
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Vendor Seminars
Time: every day
13:30–14:30
István Halász
Hall
Szabolcs Nyiredy
Hall
Liszt
Hall
Mozart
Hall
Monday,
20 June
Waters
Shimadzu
Bruker
Daltonik
Chiral
Technologies
Tuesday,
21 June
Agilent
Technologies
Sigma Aldrich
Phenomenex
Beckman
Coulter
Thermo Scientific
Merck
Waters
Dionex
Wednesday,
22 June
Thursday,
23 June
AB SCIEX/
Eksigent
Vendor Workshop
Organised by
Workshop Schedule
Sunday, 19 June 2011
12:00–13:00 Workshop Lunch (Restaurant Côte Jardin)
13:00–15:30 Workshop Lectures and discussion (István Halász Hall)
Advance registration was required.
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Instruction for speakers
Authors are kindly requested to give their presentation file to the technicians in the file
upload room (Brahms Hall), preferably a half day before the beginning of the corresponding
session. This is necessary of course only in case the file is not sent to us until 16 June.
Opening hours of the file upload room: during the normal working hours of the symposium.
Sunday, 19 June: 12:00–19:00; Monday–Thursday, 20–23 June: 8:00–18:00
The file will be copied to a central ftp server from where the projection is handled. The
name of the file should be that of the “lecturecode_lastname” e.g. PL01_Guiochon.ppt. The
file will be copied to the appropriate directory of the lecture room by the technicians.
Power Point software will be installed on all the computers. Preferred file format is in PPT
for MS Office (Office XP, Office 2003 or 2007 etc.). Please, do not use MAC file format,
if possible.
If you edited your presentation in a MAC, you are advised to have a pdf version with you,
as pdf versions can be projected without any problem. Make sure to bring your presentation file written on a properly closed CD ROM, or USB flash drive. It is recommended that
you ensure a backup file as well. There will be technicians in the file upload room as well as
in the lecture rooms to assist you with your presentation.
Optimal conditions of presentation files:
Presentation file: Microsoft Powerpoint
Resolution: 1024 x 768 XGA
In your slides: Do not use letters smaller than 12 pt.
If you use animations please embed them, if it is a special animation send the codec also
and bring all the files on a CD to the Symposium.
If you have a Macintosh computer, it can be plugged in having a conventional, 15-pin
socket. If your computer does not have this connection, please bring an appropriate converter with you.
Software installed on presentation laptops:
Microsoft Windows XP Professional SP3 or Microsoft Windows 7 SP1 • Microsoft Office
2007 SP2 • Acrobat Reader X • VLC player • K-Lite Codec Pack Full • Windows Media
Player 12 • Adobe Flash • Java.
Speakers should be aware of the time limit of 20 minutes, devoted to session talks, and
kindly asked to keep the time of their presentations. The duration of plenary and keynote
talks is 30 minutes and that of the tutorial lectures is 45 minutes including Q&A. It is
essential that speakers leave ample time for discussion of their work.
184
Instruction for poster presenters
The useful area of the poster board is 90 cm at width and 125 cm at height. The recommended size for your poster is about the standing A/0 standard (cca. 84 x 119 cm). Pins
and adhesive tapes are to be provided to fix the posters. Posters will be identified by
posters numbers, which are printed in this programme booklet. Poster presenters are
kindly requested to hang up and remove their posters according to the following schedule.
POSTER ENCODING
HPLC 2011 poster encoding helps poster presenters to identify the place and the time of
their poster presentation(s). As more than 400 posters are presented in one session, the
poster sessions will be held in two places. The majority of the posters is on display at the
Gallery of the Congress Center (BCWTC) whereas there will be a significant number of
posters that can be visited at the gallery of the Sportmax Hall where the lunch will be
served for HPLC 2011 participants.
Time of the attended poster sessions: 13:30–15:30 on Monday to Wednesday and
13:30–15:00 on Thursday.
Presenting authors having odd poster numbers in Poster Session 1 should be at their
posters on Monday.
Presenting authors having even poster numbers in Poster Session 1 should be at their
posters on Tuesday.
Presenting authors having odd poster numbers in Poster Session 2 should be at their
posters on Wednesday.
Presenting authors having even poster numbers in Poster Session 2 should be at their
posters on Thursday.
Examples for poster numbers:
P1-G-001-MO (Poster session 1, at the Gallery of BCWTC, odd poster number presentation on Monday)
P2-S-750-TH (Poster session 2, at the Sportmax Hall, even poster number presentation
on Thursday)
POSTER SESSION 1
From Monday morning (20 June) until Tuesday afternoon (21 June)
Poster presenters can mount their posters from Sunday afternoon (19 June) and should
remove them latest by Tuesday evening before the end of the session (21 June). Posters
of the following topics are scheduled for Poster Session 1.
• Advances in separation techniques (P1-G-001–031)
• Biomarker discovery (P1-S-332–346)
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•
•
•
•
•
•
•
•
•
•
•
•
•
•
Biopharmaceutical and biomedical analysis (P1-S-347–418)
Chip based separations, microfluidics, microscale detection systems (P1-G-032–058)
Chiral separations (P1-G-059–091)
Clinical, forensic, and toxicological analysis (P1-G-092–118)
Electrodriven separations (P1-G-119–149)
High-temperature LC (P1-G-150–154)
Hyphenated separations: LC-MS, CE-MS, and LC-NMR (P1-G-155–189)
Natural product analysis (P1-G-190–255)
New instrumentation for LC (P1-G-256–265)
Oligonucleotide separations (P1-G-266–267)
Planar chromatography (P1-G-268–274)
Polymer analysis (P1-S-419–422)
Proteomics, metabolomics, glycomics (P1-G-275–312)
Ultra-high pressure LC (P1-G-313–331)
POSTER SESSION 2
From Wednesday morning (22 June) until Thursday evening (23 June)
Poster presenters can mount their posters from Tuesday evening (21 June) and should
remove them latest by Thursday evening before the end of the session (23 June). Posters
of the following topics are scheduled for Poster Session 2.
• Column technology and stationary phases (P2-G-423–522)
• Data analysis and chemometrics (P2-S-749–765)
• Environmental analysis, food safety, agricultural analysis (P2-G-523–639)
• Industrial aspects of separations (P2-G-640–651)
• Pharmaceutical analysis (P2-G-652–748)
• Retention mechanisms and retention models (P2-S-766–778)
• Sample preparation (P2-S-779–813)
• Theoretical models and insights (P2-S-814–837)
There are organised attended poster sessions; thereby we intend to facilitate a more
intense communication of poster presenters and attendees. They can fix appointments for
further personal discussions, e.g. presenters may prepare an envelope for business cards.
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Symposium Proceedings
Contributors to HPLC 2011 are cordially invited to submit their paper for potential publication in a special issue
of the JOURNAL OF CHROMATOGRAPHY A, devoted to
the conference.
All manuscripts will be subject to the usual selection
process including the peer review procedure; therefore
acceptance for presentation at the conference is not a
guarantee of inclusion in the special issue.
To enable us to deal with the manuscripts as fast and efficiently as possible, authors are
kindly invited to submit their article via the journal’s online submission and reviewing system which is accessible at: http://ees.elsevier.com/chroma. Below please see instructions for submitting your manuscript:
To submit:
• Go to: http://ees.elsevier.com/chroma
• Click on the “Submit Paper” option from the top menu
• Enter your user name and password (first time users will have to register)
• After entering the title of your manuscript, please select HPLC 2011 as the ‘Article
Type’
• Follow the remaining step-by-step instructions to submit your paper
Points to note:
• The deadline to submit your manuscript to the HPLC 2011 symposium issue of Journal
of Chromatography A is 30th August 2011.
• When preparing your manuscript please carefully follow the journal’s Guide to Authors,
which you can find on the online submission site: http://ees.elsevier.com/chroma
• In your cover letter please mention that your manuscript is intended for the HPLC 2011
special issue
If you experience any technical problems or have any technical questions during the submission process, please contact Elsevier Author’s Support: authorsupport@elsevier.com.
If you have any questions on the submission and reviewing process, please contact the
Editorial Office: chrom-eo@elsevier.com
We sincerely hope you will contribute to the special issue – which will be a lasting tribute to
the meeting.
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List of Exhibitors
AB SCIEX / Eksigent (Booth# C13)
ABL&E-JASCO Magyarország Kft. (Booth# A6)
ACE Advanced Chromatography Technologies (Booth# E7)
Advanced Chemistry Development, Inc. (ACD/Labs) (Booth# A5)
Agilent Technologies (Booth# M8–9–10)
Avantor Performance Materials B.V. (Booth# A22)
Akzo Nobel / Kromasil (Booth# A9)
Beckman Coulter (Booth# A4)
Biosolve BV (Booth# E1)
Biotech AB (Booth# M20–21–22)
Bruker Daltonik GmbH/Bruker BioSpin GmbH (Booth# A1)
C&EN (Booth# C3)
CETAC Technologies (Booth# E15)
Chiral Technologies Europe (Booth# E10)
Chromatography Today (table top)
ChromSword Baltic (Booth# M6–7)
CTC Analytics AG (Booth# A3)
DAISO Co., Ltd. (Booth# C2)
Dionex Corporation (Booth# M16–17)
Elsevier B.V. (Booth# E2)
Fortis Technologies (Booth# M19)
GenTech Scientific, Inc. (Booth# E17)
GL Sciences Inc. (Booth# E9)
Hamilton Bonaduz AG (Booth# C8)
HPLC2011 Dalian, China (Booth# C1a)
HPLC2012 Anaheim, CA, USA (Booth# C9)
HPLC2013 Amsterdam, The Netherlands (Booth# C1b)
KNAUER – Wissenschaftliche Gerätebau Dr. Ing. Herbert Knauer GmbH (Booth# A20–21)
LABOMATIC Instruments AG (Booth# E8)
LCGC Group (Booth# C6)
MACHEREY-NAGEL GmbH & Co. KG (Booth# E14)
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191
Molnar-Institute for Applied Chromatography (Booth# A2)
Merck (Booth# A23–24–25)
Nacalai Tesque, Inc. (Booth# E13)
Peak Scientific Instruments Ltd. (Booth# E12)
Perkin Elmer (Booth# M1–2)
Phenomenex (Booth# A7–8)
Postnova Analytics GmbH (Booth# E4)
Quant Technologies (Booth# C12)
RECIPE Chemicals + Instruments GmbH (Booth# E6)
Restek Corporation (Booth# E5)
Sarstedt AG&Co (Booth# C7)
SCAT Europe GmbH (Booth# A10)
SEDERE SAS (Booth# M3–4)
SelectScience Ltd. (Booth# C10)
Separation Science (table top)
SGE Europe Ltd. (Booth# E16)
Shant Laboratories (Booth# E3)
Shimadzu Europa GmbH (Booth# M13–14)
Showa Denko Europe GmbH (Booth# E11)
Sigma Aldrich (Booth# A17–18–19)
Spark Holland B.V. (Booth# M5)
Thermo Scientific (Booth# M11–12)
Tosoh Bioscience GmbH (Booth# M18)
VICI AG International (Booth# E18)
VWR International GmbH (Booth# C4–5)
Waters Corporation (Booth# A11–16)
Wiley-VCH Verlag GmbH & Co. KGaA (table top)
World Courier (Booth# C11)
YMC Europe GmbH (Booth# M15)
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Welcome Reception
19:00–21:00 Sunday, 19 June, 2011
The official welcome reception of HPLC 2011 will be held in the foyer of the Csaba Horváth
Hall and in the Aula at BCWTC, symposium venue. Admission is free for all registered
delegates, accompanying persons and exhibitors with registration fee.
Event sponsor
Organ Concert in the St. Stephen Basilica
19:30–20:00 Monday, 20 June, 2011
This organ concert is organised exclusively for participants of HPLC 2011 in the St. Stephen
Basilica in the city centre. Admission is free for all registered delegates, accompanying
persons and exhibitors with registration fee.
Suggested individual route to reach the Basilica: Take tram No. 61 to Moszkva (Széll
Kálmán) Square, change to metro to Deák Square (towards Örs vezér Square) and walk to
Basilica.
Event sponsors
Symposium Dinner
18:00–22:30 Wednesday, 22 June, 2011
The official symposium dinner of HPLC 2011 will be held in the Lázár Equestrian Park,
Domony Valley, about 30 km to Budapest. The price includes all transfer costs.
Continuous departure by bus from the parking lot of the Congress Venue from 18:00.
After the dinner, bus transfer will be provided back to the Official Symposium Hotels.
Dress code: Casual dress
Price: 50 Euro / person
194
Farewell reception
17:00–18:00 Thursday, 23 June, 2011
All participants are invited to attend the Farewell reception in the Aula and Mirror corridor
at BCWTC, where you can reflect on your experience in Budapest and make plans to keep
in touch with new friends.
OPTIONAL PROGRAMMES
Budapest Sightseeing with Synagogue
9:00–13:00 Monday, 20 June, 2011
Departure from the parking place of the Symposium Venue. Gathering point at the main
entrance of the venue (opposite to the registration desk).
The first programme will be a sightseeing in the Buda side of the city by bus. Among
several famous sights, the following places will be visited: Buda Castle, Fisherman’s bastion, etc. The tour continues with the visit of the Synagogue. After a guided tour in the
largest Synagogue in Europe, the sightseeing will continue in the Pest side: Heroes’
Square, Basilica, Opera House etc. Tentative arrival is after the official Symposium lunch.
Lunch is included in the programme at the venue place.
Price of the ticket is 45 Euro / person
Excursion to Szentendre
9:00–13:00 Tuesday, 21 June, 2011
Departure from the parking place of the Symposium Venue. Gathering point at the main
entrance of the venue (opposite to the registration desk).
The tour includes a visit to Szentendre, the artists’ town with its cobbled-stone squares
and picturesque old streets and alleys. After the guided tour in the city, you will visit
more sights of the town, e.g. Kovács Margit Ceramic Museum, which will be followed by
a short shopping at the local handicraft shops. Tentative arrival is after the official Symposium lunch.
Lunch is included in the programme at the venue place.
Price of the ticket is 50 Euro / person
195
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General Information
Date and Venue
The Symposium is held at the Budapest Congress and World Trade Center (BCWTC) from
the 19 to 23 June, 2011.
Symposium and Exhibition Venue
Budapest Congress and World Trade Center
Address: H-1123 Budapest, Jagelló út 1–3.
Phone: +36 1 372 5400, Fax: + 36 1 466 5636
Website: www.bcwtc.hu
Symposium Secretariat
If you need any help during the congress you can find the staff of Diamond Congress at the
registration desk.
In case of emergency please call this mobile phone number: +36 20 936 2969.
After the symposium you can reach us at the following address:
Phone: + 36 1 214 7701, Fax: +36 1 201 2680
E-mail: diamond@diamond-congress.hu
Website: www.diamond-congress.hu
Symposium Assistance
The Colleagues of the Symposium secretariat will be recognisable by their badge and
T-shirts with a sign: HELP DESK. They will help you in all practical aspects of the participation. In addition, Symposium assistants will be at your service, wearing yellow T-shirts with
the Symposium logo.
Registration and Information Desk
The registration desk is located on the entrance level of the Congress Venue (BCWTC).
Opening hours:
8:00–21:00 Sunday, 19 June, 2011
8:00–18:00 from Monday, 20 June – till Thursday, 23 June
Symposium delegates and their companions will receive their badges, symposium materials, social event tickets at the registration desk.
Subscription for optional tours also takes place in this area.
197
Badges
All participants and accompanying persons will receive a personal badge upon registration. You
are kindly requested to wear your name badge when attending the meeting or social events.
Only participants who are wearing their name badge will be admitted to the lecture halls.
Please note that accompanying persons and exhibitors will not be admitted to the scientific
sessions.
NAME BADGES HAVE BEEN COLOUR-CODED AS FOLLOWS
Committees, attendees, press
The following services are included:
• Participation in the scientific programme
• Admission to the exhibition
• Electronic version of the Book of Abstracts
• Symposium bag with conference materials
• Welcome reception (Sunday, 19 June, Symposium Venue)
• Coffee breaks
• Lunch from Monday to Thursday
• Farewell reception (Thursday, 23 June, Symposium Venue)
• Participation in the cultural event (Monday, 20 June, Basilica – organ concert)
Daily registration
• Participation in the scientific programme
• Admission to the exhibition
• Electronic version of the Book of Abstracts
• Symposium bag with conference materials
• Coffee break on the selected day
• Lunch on the selected day
Exhibitor
• Admission to the Opening ceremony
• Coffee breaks
• Copy of the final programme
• Exhibition catalogue
• Admission to the exhibition and free broadband wifi zone
• Participation in the cultural event (Monday, 20 June, Basilica – Organ concert)
Admission to the scientific sessions and lunches are not included in this registration
category.
198
Exhibitor (upgraded exhibition badge)
• Admission to the Opening and Closing ceremony
• Coffee breaks
• Copy of the final programme
• Admission to the exhibition and free broadband wifi zone
Admission to the scientific sessions is not included in this registration category.
Visitor
• Admission to the exhibition, coffee break and free broadband wifi zone
Accompanying person
• Farewell reception (Thursday, 23 June, Symposium Venue)
Admission to the scientific sessions is not included in this registration category.
On-site Registration
Deadline for the payment of the early bird registration fee was 15 April 2011. On-line
registration was open until 15 June 2011. After that, on-site fees should be paid on spot.
On-site registration fees*
Participant from industry
Participant from academia
Daily fee for participants from industry
Daily fee for participants from academia
Student**
Accompanying person
Daily fee for exhibition visitor
Paid after
975
725
450
350
375
250
75
15 April
Euro
Euro
Euro
Euro
Euro
Euro
Euro
*Fees include 25% VAT
**Proof of student status is required
199
Programme Changes
The organisers cannot assume liability for any changes in the programme due to external
or unforeseen circumstances.
Message
Personal message can be placed on the message board located at the registration area.
Internet Room
As a courtesy to all delegates, internet terminals are available in Brahms Hall in BCWTC.
Opening hours: Monday, 20 June – Thursday, 23 June, 8:00–18:00
A complimentary wireless internet service is provided throughout the Congress Center.
Username: HPLC, password: 2011
Car Parking
Parking space is available in front of the Congress Center (BCWTC).
Price: 200 HUF/hour (cca 0.7 Euro)
Mobile Phones
Delegates are politely requested to keep their mobile phones switched off in the meeting
rooms during all sessions.
Smoking
HPLC 2011 is a non-smoking symposium. Therefore, the organisers would like to thank
the participants in advance for not smoking in the Congress Center.
First Aid and Pharmacy
There is a First Aid room in the Conference site, which is open between 9:00–18:00
between 20–23 June, 2011. Please contact the info desk next to the registration desk.
The nearest Pharmacy can be found next to the Congress Center (5 minutes on foot) in
the shopping mall of MOM PARK.
200
Catering Services during HPLC
• Welcome reception – BCWTC Symposium venue 19 June (included in the registration
fees)
• Lunch – Budapest Sportmax Hall 20–21–22–23 June (included in the appropriate
registration fees)
• Coffee breaks – BCWTC / Exhibition area (included in the registration fees)
• Symposium Dinner – Lázár Equestrian Park, 22 June (not included in any type of registration fees)
• Farewell reception – BCWTC Symposium venue 23 June (included in the registration
fees)
Cancellation Policy
Registration fee
For registration cancellations received prior to 30 April 2011, the refund was 100%.
From 1 to 21 May 2011, the refund was 50%.
No refund was possible for cancellations submitted on or after 21 May 2011.
Hotel accommodation
For hotel reservation cancellations received prior to 30 April 2011, the refund was 100%.
If received between 1 and 20 May 2011, the prepaid hotel deposit was kept and the rest
of the payment was refunded.
Refund was not guaranteed for cancellations submitted on or after 21 May 2011.
201
Accommodation Information
Hotel prices are in Euro, per room per night, including breakfast and all kinds of taxes.
Check in time from 2 pm, check out time till 10 am.
For the location of the hotels, please refer to the map on the next page.
Novotel Budapest Congress****
(Conference venue)
Address: H-1123 Budapest, Alkotás u. 63–67.
Phone: +36 1 372 5400
Website: www.accorhotels.com
Access to symposium venue: 1 minute on foot
Villa Hotel Kristal***
H-1118 Budapest, Társ utca 9.
Phone: +36 1 466 9043
Website: www.kristal.hu
Access to symposium venue: 5 minutes walk on foot
Jagelló Business Hotel***
H-1124 Budapest, Jagelló út 38.
Phone: +36 1 248 2780
Website: www.jagellobusinesshotel.hu
Access to symposium venue: 3 minutes walk on foot
Hotel Mediterran****
Address: H-1118 Budapest, Budaörsi út 20/a.
Phone: +36 1 372 7020
Website: www.hotelmediterran.hu
Access to symposium venue: 4 minutes on foot
Hotel Bara***
Address: H-1118 Budapest, Hegyalja út 34–36.
Phone: +36 1 385 3445
Website: www.hotelbara.hu
Hotel Charles***
Address: H-1016 Budapest, Hegyalja út 23.
Phone: +36 1 212 9169
Website: www.charleshotel.hu
202
203
Gold Hotel Buda****
Address: H-1016 Budapest, Hegyalja út 14.
Phone: +36 1 209 4775
Website: www.goldhotel.hu
Ramada Budapest***
Address: H-1094 Budapest, Tompa utca 30–34.
Phone: +36 1 477 7200
Website: www.ramadabudapest.com
Access to symposium venue: 20 minutes by public transport
Zara Hotel Boutique****
Address: H-1056 Budapest, Só utca 6.
Phone: +36 1 577 0700
Website: www.boutiquehotelzara.com/hu
Access to symposium venue: 15–20 minutes by public transportation
Hotel Mercure Buda****
Address: H-1013 Budapest, Krisztina körút 41–43.
Phone: +36 1 488 8100
Access to symposium venue: 15 minutes by public transportation
Novotel Budapest Danube****
Address: H-1027 Budapest, Bem rkp. 33–34.
Phone: +36 1 458 4900
Hilton Budapest*****
Address: H-1014 Budapest, Hess András tér 1–3.
Phone: +36 1 888 8200
Website: www.budapest.hilton.com
204
Liability and insurance
The organisers cannot accept liability for personal accidents, loss of belongings or damage
to private property of participants and accompanying persons that may occur during the
Congress. Participants are advised to make their own arrangements to obtain health,
travel and property insurance before their departure to the HPLC 2011.
Foreign Exchange, Banking Facilities
The official national Hungarian currency is the Hungarian Forint (HUF). All the major credit
cards are accepted in Hungary in places displaying the emblem at the entrance. Though
Hungary is a member of the European Union, only a few shops and restaurants accept
Euros (EUR) for payment. Currency exchange booths are available in Budapest at the
airport terminals, railway stations, travel agencies, banks and various places in the city.
The exchange rates applied may vary. Traveller’s cheques and convertible currency may be
exchanged at these facilities. Major credit cards are usually accepted in most hotels,
restaurants and certain shops in the city. Obtaining cash against ATM or credit cards is
very easy from the ATM cash machines that can be found at almost every office, hotel or
on the street.
Shopping in Budapest (opening hours)
Food shops are open from 7 am – 6 pm Mon – Fri, 8 am – 1 pm Sat (but there are several larger stores open on Sunday morning and a number of small 24-hour shops).
Other shops are open between 10 am – 6 pm Mon – Fri, 10 am – 1 pm Sat. Most shopping centres are open 10 am – 8 pm even on Sunday. Tesco is open 24 hours a day,
seven days a week.
Office hours: generally from 8 am – 4 pm Mon – Fri.
Post offices: Mon – Fri: 8 am – 6 pm, Sat: 8 am – 1 pm.
Banks: Mon – Thu: 8 am – 3 pm, Fri: 8 am – 1 pm.
Transportation
There are daily direct flights from most European and from some North American cities.
The Budapest Liszt Ferenc (Ferihegy) International Airport is situated on the SE margin of
Budapest, 20 km from the city centre and is a popular destination for many low fare air
carriers. The Airport Minibus service is relatively cheap and reliable. Public transport
buses (#200E, air conditioned, from Terminal 1 also #93) circulate between the terminals
and the Kőbánya-Kispest terminal of the Metro line 3 (“blue line”) at 8–15-minute intervals
in daytime. As an alternative, trains from Terminal 1 leave for Nyugati railway station
205
frequently. Főtaxi has exclusive rights for operation of a taxi service from (and to) the
airport for fixed prices according to distance zones (hence the name) based on a contract
with Budapest Airport Ltd.
The airport has three terminals (practically two as 2B is directly connected to 2A):
Terminal 1: terminal for budget airlines,
Terminal 2A: terminal for all MALÉV Hungarian Airlines flights and some foreign airlines,
Terminal 2B: arrival and departure terminal for most foreign airlines.
Public transport in Budapest
Public transport in Budapest is provided by Budapest Transport Ltd. (known to all Hungarians simply as BKV). Budapest has an efficient public transport network. In general
the buses, trams and trolleybuses operate between 4:30 am and 11 pm. All night bus
service operates on the major thoroughfares in the city (night bus timetables are posted at stops and in most metro stations). The three metro lines intersect at Deák
Square in the centre of the town. Metros run at 2–15 minutes intervals from about
4:30 am to 11:15 pm. There are also five suburban railway lines (HÉV) serving the
outskirts of the city.
Taxis in Budapest
Budapest taxis have yellow number plates and a taxi sign in yellow. All cars must have a
taximeter installed, and these also print out a receipt. Taxi drivers are required to give an
invoice on request. Tipping: in general 10% of the fare is acceptable. It is worth calling a
taxi by phone because most of the taxi companies charge lower rates in this case than in
the case of hailing a taxi in the street.
Advice for your departure
Airport Minibus
Participants leaving from Budapest Ferenc Liszt International Airport are advised to use
the Airport Minibus shuttle service, which takes one from any address in Budapest for a
fee of 2990 HUF/person (cca. 12 EUR).
You may order your Airport Minibus at the Information Desk (entrance level) or at your
hotel at least one day before your departure. Telephone number: +36 1 296 8555.
Taxi
Taking a taxi – the tariffs of the taxi companies may differ but share a fixed common tariff
ceiling. If you take a taxi, you can find the tariff chart on both dashboard and on the right
rear window.
206
Phone numbers of some taxi companies: Főtaxi 222-2222, City Taxi 211-1111, Radio
Taxi 377-7777, Taxi 2000 200-0000. During the symposium the congress secretariat
has entered a contract with City Taxi.
Telephone
The international code for Hungary is 36, the area code for Budapest is 1. To call a number within Hungary, first dial 06. Budapest telephone numbers have seven digits, all other
areas have six digits (in addition to the area codes). To make an international call from
Hungary, first dial 00, then the country code followed by the area code and the subscriber’s telephone number. Public telephones accept either coins (20, 50, and 100 HUF) or
phone cards (available from tobacconists, newsagents, post offices, and petrol stations).
To call a (Hungarian) mobile phone, from a public telephone first dial 06, followed by the
subscriber’s seven-digit number starting with 20-, 30- or 70-.
Important phone numbers
(English is usually spoken at the emergency numbers listed below. In case English is not
spoken, dial 112)
General enquiries: 197
Ambulance: 104
Inland enquiries: 198
Fire brigade: 105
International enquiries: 199
Police: 107
Hungarian Automobile Club help number: 188
Central help number: 112
Time
Hungary is in the Central European Time Zone. In the summer months clocks are set at
GMT + 2 hours.
Weather
The weather in Hungary in June is usually sunny and warm. Temperatures are usually in
the range between 23 and 28 °C during the day. Rain showers may occur during the day,
however.
Hungarian Society for Separation Sciences, Pécs, Hungary, 2011
This book is working material for the 36th International Symposium on High-Performance Liquid Phase
Separations and Related Techniques (HPLC 2011 Budapest Symposium).
All rights reserved, except for the authors’ right to publish their materials wherever they decide.
Printed by: OOK Press Ltd., H-8200 Veszprém, Pápai út 37/A, Hungary
207
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Final Programme book is uploaded

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