- Hellma Optics
Transcription
- Hellma Optics
PRODUCT OVERVIEW ■ CELLS ■ SLIDES ■ OPTICAL COMPONENTS 1. Cells | 1.1 Material and Technical Information 1.1.1 Material Our cells are manufactured from various types of glass. The most important criterion for the choice of a particular type of glass is the spectral range for which the cell is intended as well as the conditions of use. Coloured logos are fused onto each Hellma cell, thus indicating the spectral range over which the cell can be used. In general we divide the glass materials that we use into two groups: Quartz and Optical Glass. Quartz consists exclusively of silicon dioxide (SiO2) and shows some remarkable properties: ■ Quartz displays a high UV transmission, in highly purified synthetic Quartz down to well below 200 nm. ■ The thermal expansion of Quartz is extremely low, its coefficient of thermal expansion being 6 x 10 -7 K -1 between 20 °C and 300 °C. ■ Quartz is chemically very resistant and maintains its shape, even at high temperatures up to approximately 1000 °C. Common criteria for all types of Optical Glass are ■ that the cells made from it are used in the visible range of the spectrum, ■ that the glasses we use are characterised by relatively low values of refractive index and dispersion, ■ that they display good resistance to chemicals. 1.1.2 Tolerances Tolerance for the outer width: Cell types J 103 – J 115 J8–J9F Tolerances + 0/ -0.2 mm + 0/ -0.3 mm Tolerance of the light path: Cells made of Special Optical Glass and Quartz Light path 1 mm to 20 mm ± 0.01 mm Light path 40 mm to 100 mm ± 0.02 mm Cells made of Optical Glass Light path 10 mm to 30 mm Light path 40 mm to 50 mm 2 ± 0.10 mm ± 0.20 mm 1. Cells | 1.1 Material and Technical Information 1.1.3 Material Codes Identification Logos for UV Cells J is the identification logo which indicates that quartz of the highest purity and homogeneity has been used for the window. Because it is produced from a silicon compound, it is also called synthetic quartz. We use quartz from Heraeus Quarzglas GmbH and SCHOTT Lithotec AG, which gives transmission values of more than 80 % over a spectral range of between 200 nm and 2500 nm for an empty cell. Identification Logos for Cells for the Visible Spectrum J indicates that SCHOTT type UK 5 is used for cells referred to in the catalogue as manufactured from “Special Optical Glass”. This crown glass is made from exceptionally pure raw materials, which gives an improved transmission in the near ultraviolet range. An empty cell will give a transmission of more than 80 % over a spectral range of between 320 nm and 2500 nm. J is a trademark that distinguishes cells which are not used in spectrophotometry. Here, a glass is used, which we refer to in the catalogue as “Optical Glass”. We use B 270 Superwite from SCHOTT DESAG and “Borofloat 33” from SCHOTT JENAer Glas GmbH, a colourless highly transparent crown glass in the form of drawn panes with fire-polished surfaces. The quality of the surfaces is so high that the components can be fused using the Hellma process without further grinding and polishing. An empty cell made of B 270 Superwite will give a transmission of more than 80 % over a spectral range of between 360 nm and 2500 nm. For further information see www.hellmaoptik.com 3 1. Cells | 1.1 Material and Technical Information 1.1.4 Transmission Transmission values are established by means of measurements performed on empty cells with windows of 1.25 mm thickness. Depending on the wavelength transmission values will be 5 % to 8 % higher if measurements are carried out with filled cells (distilled water). When comparing the transmission values of cells or of windows made by different companies, you should make sure that the conditions under which measurements were made are the same. It is important to know whether measurements were made with empty or filled cells and how thick the windows were. Material Code Window Material Wavelength yellow green blue red Optical Glass Special Optical Glass UV-Quartz Quartz SUPRASIL 300 360 - 2500 320 - 2500 200 - 2500 200 - 3500 J J J J nm nm nm nm 100 SUPRASIL 300 300 SUPRASIL 90 80 UV-Quartz SUPRASIL HERASIL Transmission (%) Transmission (%) 70 60 Special Optisches Optical Glass Spezialglas 50 Optical Optisches Glass Glas 40 30 20 Borofloat Borofloat 10 150 200 250 300 400 2000 3000 4000 5000 Wavelength λ (nm) Wellenlänge (nm) Transmission of empty cells made of different materials 1.1.5 Spectral Measurements As a result of the improvements in glass production and through the perfection of the polishing process, all cells are produced with transmission values, which within the limits of the measuring uncertainty, agree with the theoretical transmission. On request all cells can be spectrally calibrated and assembled into sets of equal transmission values (measuring uncertainty ± 1 %). These cells are provided with a three digit calibration code number containing coded data about the material and the transmission at a wavelength typical for the cell material. In the case of a repeat order please be aware that, through usage, your cells will probably not have the same high transmission values as the new cells. 4 1. Cells | 1.2 Standard Cells 1.2.1 Absorption Cells macro | with lids Catalogue Number Window Material Light Path mm Outside Dim. HxWxD mm Inside Width mm Base Thickn. mm Volume µl Number of Windows Remarks J 103 Optical Glass 10 20 40 50 45 45 45 45 x x x x 12.5 12.5 12.5 12.5 x x x x 12.5 22.5 42.5 52.5 9.5 9.5 9.5 9.5 1.5 1.5 1.5 1.5 3500 7000 14000 17500 2 2 2 2 without without without without J 100-OS Special Optical Glass 1 2 5 10 20 40 50 100 45 45 45 45 45 45 45 45 x x x x x x x x 12.5 12.5 12.5 12.5 12.5 12.5 12.5 12.5 x x x x x x x x 3.5 4.5 7.5 12.5 22.5 42.5 52.5 102.5 9.5 9.5 9.5 9.5 9.5 9.5 9.5 9.5 1.5 1.5 1.5 1.5 1.5 1.5 1.5 1.5 350 700 1750 3500 7000 14000 17500 35000 2 2 2 2 2 2 2 2 J 100-Q Quartz 1 2 5 10 20 40 50 100 45 45 45 45 45 45 45 45 x x x x x x x x 12.5 12.5 12.5 12.5 12.5 12.5 12.5 12.5 x x x x x x x x 3.5 4.5 7.5 12.5 22.5 42.5 52.5 102.5 9.5 9.5 9.5 9.5 9.5 9.5 9.5 9.5 1.5 1.5 1.5 1.5 1.5 1.5 1.5 1.5 350 700 1750 3500 7000 14000 17500 35000 2 2 2 2 2 2 2 2 J 6030-UV Quartz 10 45 x 12.5 x 45 9.5 1.5 3500 2 lid lid lid lid without lid Light path 10 ± 0.1 macro | with stoppers J 110-OS Special Optical Glass 5 10 20 50 46 46 46 46 x x x x 12.5 12.5 12.5 12.5 x x x x 7.5 12.5 22.5 52.5 9.5 9.5 9.5 9.5 1.5 1.5 1.5 1.5 1750 3500 7000 17500 2 2 2 2 J 110-Q Quartz 5 10 20 40 50 46 46 46 46 46 x x x x x 12.5 12.5 12.5 12.5 12.5 x x x x x 7.5 12.5 22.5 42.5 52.5 9.5 9.5 9.5 9.5 9.5 1.5 1.5 1.5 1.5 1.5 1750 3500 7000 14000 17500 2 2 2 2 2 J 103 J 100-OS J 100-Q For further information see www.hellmaoptik.com J 6030-UV J 110-OS J 110-Q 5 1. Cells | 1.2 Standard Cells 1.2.1 Absorption Cells semi-micro | with lids or stoppers Catalogue Number Window Material Light Path mm Outside Dim. HxWxD mm Inside Width mm Base Thickn. mm Volume µl Number of Windows J 104-OS J 104-Q Special Optical Glass Quartz 10 10 45 x 12.5 x 12.5 45 x 12.5 x 12.5 4 4 3.2 3.2 1400 1400 2 2 J 114-OS J 114-Q Special Optical Glass Quartz 10 10 46 x 12.5 x 12.5 46 x 12.5 x 12.5 4 4 3.2 3.2 1400 1400 2 2 Remarks micro | with lids or stoppers J 104.002-OS J 104.002-Q Special Optical Glass Quartz 10 10 45 x 12.5 x 12.5 45 x 12.5 x 12.5 2 2 3.2 3.2 700 700 2 2 J 115-OS J 115-Q Special Optical Glass Quartz 10 10 40 x 12.5 x 12.5 40 x 12.5 x 12.5 2 2 1.25 1.25 400 400 2 2 1.2.2 Fluorescence Cells macro | with lids or stoppers Catalogue Number Window Material Light Path mm Outside Dim. HxWxD mm Inside Width mm Base Thickn. mm Volume µl Number of Windows J 101-OS J 101-Q Special Optical Glass Quartz 10 10 45 x 12.5 x 12.5 45 x 12.5 x 12.5 10 10 1.25 1.25 3500 3500 4 4 J 111-OS J 111-Q Special Optical Glass Quartz 10 10 46 x 12.5 x 12.5 46 x 12.5 x 12.5 10 10 1.25 1.25 3500 3500 4 4 J 104 6 J 114 J 104.002 J 115 J 101 J 111 Remarks 1. Cells | 1.3 Cells for “Spekol”- analysis equipment 1.3.1 Absorption Cells macro | without lids Catalogue Number Window Material Light Path mm Outside Dim. HxWxD mm Inside Width mm Base Thickn. mm Volume µl Number of Windows Remarks J 8* Optical Glass 1 2 5 10 20 30 50 30 30 30 30 30 30 30 6 7 10 15 25 35 55 8.5 8.5 8.5 8.5 8.5 8.5 8.5 2.5 2.5 2.5 2.5 2.5 2.5 2.5 200 400 1000 2000 4000 6000 10000 2 2 2 2 2 2 2 with lid on request J 8-OS Special Optical Glass 5 10 30 x 13.5 x 10 30 x 13.5 x 15 8.5 8.5 2.5 2.5 1000 2000 2 2 with lid on request JC Optical Glass 5 10 20 30 x 23 x 10 30 x 23 x 15 30 x 23 x 25 18.5 18.5 18.5 2.5 2.5 2.5 2250 4500 9000 2 2 2 with lid on request JC-OS Special Optical Glass 5 10 30 x 23 x 10 30 x 23 x 15 18.5 18.5 2.5 2.5 2250 4500 2 2 with lid on request x x x x x x x 13.5 13.5 13.5 13.5 13.5 13.5 13.5 x x x x x x x *For light paths of 10, 20 and 50 mm quartz is also available upon request 1.3.2 Fluorescence Cells macro | without lids Catalogue Number Window Material Light Path mm Outside Dim. HxWxD mm Inside Width mm Base Thickn. mm Volume µl Number of Windows Remarks J8F Optical Glass 10 ± 0.1 30 x 13 x 14 8.5 2.5 2000 4 with lid on request J9F Optical Glass 20 ± 0.1 53.5 x 35 x 25 30.5 2.5 25000 4 J8 J 8-OS For further information see www.hellmaoptik.com JC JC-OS J8F J9F 7 1. Cells | 1.4 Other Supplies and Accessories 1.4.1 Other Supplies Besides the standard cells shown here we also make cells for special purposes according to our customers’ specifications. Of special interest are our cells made of CaF2 used, for instance, in DUV applications. The well known selection of cells from our parent company, Hellma GmbH & Co. KG, 79371 Müllheim, Germany, represents an additional range of cells available to our customers. On request we would be happy to send you information about these. Items available include standard and flow-through cells, fibre-optical probes, and calibration standards for all kinds of applications. 1.4.2 Mirror Coating For some purposes (e.g. fluorescence measurements) mirror coated cells are used. Both the rear window to the incident light and the left adjacent window are mirror-coated on the outside. The standard mirror coating consists of a layer of vacuum-evaporated aluminium that has a degree of reflection of more than 80 % over the spectral range between 190 nm and 2500 nm. This coating is covered with a protective layer which is extremely hard and durable. Additionally, the mirror-coated windows are protected against external scratches by a layer of black lacquer. On request we can also supply metal coatings with different reflective properties and with the coated surfaces in other positions. Reflectance of an aluminium layer 1.4.3 Accessories Replacement lids and stoppers made of PTFE are available for cells with an external width of 12.5 mm. 1.4.4 Cleaning of Cells Hellmanex® II is an alkaline liquid concentrate for the efficient cleaning of cells and other optical parts made of quartz and glass. It automatically and completely removes even the most stubborn contaminants such as fats, oils, waxes, dried blood, proteins, pigments, silicon oil, and traces of many other organic and inorganic substances. 8 2. Slides Slides made of quartz are chemically very durable and are well suited for UV applications. We also offer slides made of high-index optical glass, which can be used if the difference in refractive indexes is a problem. Slides made of optical glass supplied by SCHOTT can be made upon request. Here is a selection of slides with standardised dimensions. Cat.-No. Material Outside Dim. Thickness J 106-OS J 106-Q J 106-LA Special Optical Glass (UK 5) Quartz LaSFN 9 48 x 14 mm 48 x 14 mm 76 x 25 mm 1.25 1.25 1.50 3. Optical Components and Special Optics Additionally we offer our customers diverse flat optics (substrates, spacers, retarders, prisms, wedges, etc.), cylindrical lenses, torical lenses, parts with conical surfaces (cones) and optical filters. Generally speaking optical components can be made of any glass offered in SCHOTT’s catalogues (“SCHOTT Optical Glass” and “SCHOTT Optical Glass Filters”). Additionally the materials SCHOTT Borofloat, SCHOTT Duran, SCHOTT Zerodur and DESAG 270 as well as quartz from SCHOTT Lithotec and from Heraeus or any equivalent materials from other producers can be used. Other materials: CaF2, sapphire, silicon, germanium, etc. Using modern equipment and the advantages of new techniques we are able to offer components with polished surfaces of such high quality that they are well-suited for laser technologies. In order to avoid misunderstandings which can arise due to unclear or incomplete specifications, one should be sure to pay attention to the following points. The quality of polished surfaces is characterised by two mutually independent criteria: first the surface must be free of any flaws such as scratches and holes as well as any dull, unpolished spots. Secondly the evenness of the glass surface must be considered. For demanding jobs such as occurs with interferometer mirrors, the requirements for evenness should take into consideration what kinds of deformations are acceptable for an even wave, which is reflected from or which passes through an “uneven” surface. For further information see www.hellmaoptik.com 9 3. Optical Components and Special Optics The designation of acceptable wavefront deformations in windows is especially important because it accounts for the influence of both glass surfaces and by doing so the designation of evenness of both surfaces and their parallelism to one another becomes superfluous. Various specifications The thickness of a window in this case only has to conform to mechanical criteria (pressure resistance, installation standards) – tolerances can be made correspondingly larger. The designation of wavefront deformation should also be made for wedges in analogous fashion. If so desired, the flat optical parts can also be supplied with mirror coatings or AR coatings. For AR coatings, please include the wavelength range and the required reflection percentage so that the optimal layer system can be determined. For mirror coatings, we offer a standard aluminium layer which is protected by a layer of evaporated quartz in order to improve durability. Please send us your technical drawings including all important dimensions and the desired quantity so that we can prepare an individualised price estimate. If you are interested in these products simply request our product overview “Flat Optics / Cylindrical Optics”. 4. General Information Packaging All cells shown here are delivered in a plastic case. If so desired we can also deliver cells in a special velvet-lined case at an additional charge. Ordering Information Please check the following list when making out your order to make sure you have included all information: ■ the catalogue number ■ the type of material ■ the light path ■ the quantity required ■ any measurements required ■ type of packaging required (separate case) 10 4. General Information Your way to Hellma Optik GmbH Jena Jena is conveniently located on motorway A4 between Erfurt and Dresden. By train you can get to Jena by way of the Berlin-Munich line (ICE train station in Jena) and by way of the Frankfurt-Leipzig line (ICE train station in Weimar with a connecting train to Jena). By car the ICE train station in Weimar is 30 minutes away and the ICE train station in Jena 5 minutes. The airport in Leipzig is roughly 80 km away. If you are arriving by train or by plane, we will be happy to pick you up at the train station or the airport. If you are arriving by car please refer to the map below for directions. Address Hellma Optik GmbH Jena Mühlenstraße 30 07745 Jena / Germany Phone + 49 (0) 36 41/ 60 98 14 Fax + 49 (0) 36 41/ 60 98 15 www.hellmaoptik.com sales@hellmaoptik.com For further information see www.hellmaoptik.com 11 4. General Information Delivery and Payment Conditions All deliveries take place ex works. With only a few exceptions packaging is not billed. We endeavour to use the least inexpensive manner of shipping whether post, parcel service or freight forwarding. The general terms and conditions of business of Hellma Optik GmbH Jena are binding and are available on request. We ask for payment within 14 days for a 2 % cash discount or within 30 days at the net price. Please bring claims to our attention as soon as possible, but at the latest within three months after having received the products. With regard to technological innovations all information in this catalogue is subject to change. Hellma Optik GmbH Jena · Postfach 100403 · 07704 Jena Phone + 49 (0) 36 41 / 60 98 14 · Fax + 49 (0) 36 41 / 60 98 15 · www. hellmaoptik.com · sales@hellmaoptik.com © by Hellma Optik GmbH Jena · J 105/04-GB-1 · Printed in Germany The delivered goods remain our property until payment is made in full.