Adhesives
Transcription
Adhesives
All you need is Kerr Introduction Restorative Procedure INDEX Restorative procedure steps and products overview 3-6 Bonding: Bonding & Adhesion, Prof. David Watts, Dr. Nick Silikas 7-8 OptiBond Family 1 9-10 OptiBond FL 11-12 OptiBond Solo Plus 13-14 OptiBond All-In-One 15-16 Composites: Aesthetics and composite, Prof. Angelo Putignano 17-20 Herculite XRV Ultra 21-22 Clinical case: Class IV 23-24 Clinical case: Class V 25-26 Clinical case: Class II 27-28 Clinical case: Class I 29 Finishing and Polishing: Finishing and polishing of composite restorations, Prof. Martin Jung 31-33 Surface treatment of composite filling overview 34-36 OptiDisc 37-38 HiLusterPlus Polishing System 39-40 OptiShine 41 Herculite XRV, OptiBond FL References 42 Authors Biographies 43 Achieving good aesthetic results simply, reliably and quickly is an everyday challenge in restorative dentistry. Kerr’s competence in composites and adhesive systems accompanied with smart Hawe restorative tools offer predictable and faster results in any clinical situation. This restorative dentistry guide summarizes the use of different materials, tools and techniques essential for creating high quality restorations with long term clinical success. 2 Your practice is our inspiration.™ All you need is Kerr Introduction Restorative Procedure STEP PRODUCT Caries diagnostic X-rays KERR PRODUCTS Film and Sensor Holder Line Kwik-Bite Cavity preparation Burs SuperBite Posterior Beavers Carbide Jet Burs BlueWhite Diamond Burs Accessories SuperBite Anterior Beavers Carbide Jet Bur BlueWhite Diamond Bur OptiDam™ SoftClamp™ Fixafloss™ OptiDam OptiView™ SoftClamp OptiView Fixafloss 3 STEP PRODUCT KERR PRODUCTS Adhesion Total-Etch OptiBond™ FL OptiBond™ Solo Plus™ Self-Etch Composite Filling Nanohybrid OptiBond™ All-In-One Premise™ Premise™ Packable Herculite® XRV Ultra™ Microhybrid Herculite® XRV™ Point 4™ Flowable Premise™ Flowable Premise Premise Packable Revolution™ Formula 2 Premise Flowable 4 Your practice is our inspiration.™ Herculite XRV Ultra All you need is Kerr Introduction Restorative Procedure STEP PRODUCT Application methods Matrices KERRHAWE PRODUCTS SuperMat® System Hawe Adapt® Matrices Lucifix® Matrices Adapt SuperCap Steel and Transparent Matrices Lucifix Matrice SuperMat System Hawe Adapt® Sectional Matrices Hawe Transparent Cervical Matrices Wedges Hawe Sycamore Wedges Sectional Matrice Cervical Matrices Wedge Dispenser Hand shaping instruments Polymerization Halogen curing lights LED lamps CompoRoller™ CompoRoller OptiLux 501, Demetron LC Demetron A1 and A2 DEMI Demetron A1 and A2 5 Demi Finishing and polishing Flexible disc Abrasive strips OptiDisc® OptiStrip™ OptiDisc Abrasive brushes Polishers Professional cleaning OptiStrip Occlubrush® OptiShine™ Occlubrush OptiShine GlossPlus Polishers HiLusterPlus Polishers HiLuster Polishing System Cleanic® CleanPolish and SuperPolish Pro-Cup® Brushes Pro-Cup Cleanic Mint, Apple and Bubble Gum 6 Your practice is our inspiration.™ All you need is Kerr Adhesives Restorative Procedure Adhesives The mechanism of enamel bonding is based on a micro-mechanical bond between the resin and the phosphoric acid conditioned rough surface of the enamel. Enamel conditioning remains the most commonly used method to bond resin-composites to enamel surface. It provides strong bonds. Enamel conditioning may be regained by re-etching the surface and applying the resin, thus recovering the required shear bond strength at the enamel-resin interface, and allowing the resin to mechanically bond onto its surface. Dentine however has a much more complex structure than enamel. Prior to dentine-bonding, the removal or modification of the smear layer is indicated to clear the openings of the dentine tubules by conditioning the surface of the dentine. Bonding & Adhesion Prof. David Watts, Dr. Nick Silikas, University of Manchester, UK A fluid adhesive is then applied over the dentine and cured, ensuring that optimum wetting of the surface and absorption into the dentinal tubules is achieved; thus creating an inter-penetrating network with the demineralised collagen in the dentinal tubules, hence forming the hybrid layer. Preservation of the hybrid layer prior to the application of the hydrophobic resin restoration is imperative for an efficient bond to form between the resin and dentine. Therefore, any contamination of any region of the adhesive system would evidently jeopardise the integrity of the bond. The mechanism proposed for this material was to bond to the organic component of the dentine, namely the collagen. The first work to investigate the mechanism of bonding to the dentine was by Nakabayashi (1). He first identified a layer between the resin and dentine substrate referred to as “hybrid” dentine, in that it was the organic components of the dentine that had been permeated by resin. The term “hybrid layer” has now become synonymous with bonding of resins to etched dentine. There has been a tremendous amount of research done on the hybrid layer, its structure, formation and how it can be improved. This layer has also been referred to as the “resin-dentine interdiffusion zone” (2). Classification Numerous dentine bonding agents have been commercially introduced. These changes have been referred by some people as “generations”, implying that there was a chronological development. This can be very confusing. A more consistent and logical approach is to classify bonding agents by the number of steps needed to complete the bonding process. “Three-step” or “Conventional” systems This group typically consists of three separate application steps: etching, priming and adhesive resin. They are also known as “etch-and-rinse” 7 systems. Although they were the first ones introduced, they are still widely used and have been shown to provide reliable bonding. Their main drawback seems to be technique sensitivity, since any deviation from the recommended procedure will result in inferior bonding. “Two-step” systems This group can be subdivided into two subgroups: i) They have a separate etch and have combined the priming and bonding steps. These systems are often referred to as “Single-bottle” systems. Similar problems found with the “Three-step” system can also be seen here. ii) Etching and priming steps are combined together and bonding is separate. This is referred to as “Self-etching primers”. An acidic resin etches and infiltrates the dentine simultaneously. The tooth does not need to be rinsed which decreases the clinical application time and also reduces technique sensitivity by eliminating the need to maintain the dentine in a moist state. “One-bottle” or “All-in-one” systems This is when all steps are combined into one process. Their mode of action is similar to that of the “self-etching primers”, but the bonding resin is also incorporated. It is considered that these do not etch as effectively as the previous ones. They are the most recently introduced so limited clinical data is available. Bonding mechanism This micromechanical coupling of restorative materials to dentine, via an intermediate adhesive layer, is referred to as dentine bonding (3). The 8 resin in the primer and bonding step penetrates the collapsed collagen fibrils (after demineralisation), and forms an interpenetrating network. This layer had been described extensively and in great detail (4, 5). The thickness of the hybrid layer ranges from less than 1 µm for the all-in-one systems to up to 5 µm for the conventional systems. The bond strength is not dependent on the thickness of the hybrid layer, as the self-etching priming materials have shown bond strengths greater than many other systems but exhibit a thin hybrid layer. The etching, rinsing and drying process cause the dentine to collapse due to the loss of the supporting hydroxyapatite structure. The collapsed state of collagen fibrils was hindering the successful diffusion of the resin monomers. To overcome this problem, two approaches were introduced. The first one is called “dry-bonding technique” and involves air-drying of dentine after etching and subsequent application of a waterbased primer that can re-expand the collapsed collagen (6, 7). The second one is the “wet bonding technique” in which the demineralized collagen is supported by residual water after washing (8). This allows the priming solution to diffuse throughout the collagen fibre network more successfully. However, when it comes to clinical practice, it is very difficult to find the correct balance of residual moisture. Excess water can be detrimental to bonding and these problems have been described as “overwetting phenomena” (9). Since the “dry-bonding technique” is considered to be significantly less technique sensitive, it should be preferred over the most difficult to standardize “wet bonding technique” (2). Relevant in-vitro bond strength studies can provide a useful indication of the prospective clinical success of a system. However, the highest level of evidence for comparing the efficiency of a bonding system is obtained from randomised clinical trials. Randomised clinical trials with elongated the treatment periods will be very useful in assessing both the effectiveness of a particular group and a particular method of application. References 1. Nakabayashi N, Kojima K, Masuhara E. The promotion of adhesion by the infiltration of monomers into tooth substrates. J Biomed Mater Res 1982;16:265-273. 2. Van Landuyt K, De Munck J, Coutinho E, Peumans M, Lambrechts P, Van Meerbeek B. Bonding to Dentin: Smear Layer and the Process of Hybridization. In: Eliades G, Watts DC, Eliades T, editors. Dental Hard Tissues and Bonding Interfacial Phenomena and Related Properties Berlin: Springer; 2005. p. 89-122. 3. Eick JD, Gwinnett AJ, Pashley DH, Robinson SJ. Current concepts on adhesion to dentin. Crit Rev Oral Biol Med 1997;8:306-335. 4. Van Meerbeek B, Braem M, Lambrechts P, Vanherle G. Morphological characterization of the interface between resin and sclerotic dentine. J Dent Res 1994;22:141-146. 5. Van Meerbeek B, Inokoshi S, Braem M, Lambrechts P, Vanherle G. Morphological aspects of the resin-dentin interdiffusion zone with different dentin adhesive systems. J Dent Res 1992;71:1530-1540. 6. Finger WJ, Balkenhol M. Rewetting strategies for bonding to dry dentin with an acetone-based adhesive. J Adhes Dent 2000;2:51-56. 7. Frankenberger R, Krämer N, Petschelt A. Technique sensitivity of dentin bonding: effect of application mistakes on bond strength and marginal adaptation. Oper Dent 2000;25:324-330. 8. Kanca JI. Effect of resin primer solvents and surface wetness on resin composite bond strength to dentin. Am J Dent 1992;5:213-215. 9. Tay FR, Gwinnett JA, Wei SH. Micromorphological spectrum from overdrying to overwetting acid-conditioned dentin in water-free acetonebased, single-bottle primer/adhesives. Dent Mater 1996;12:236-244. Your practice is our inspiration.™ All you need is Kerr Adhesives Restorative Procedure OptiBond™ Respected by leading opinion leaders, perceived as the gold standard of the adhesive technology OptiBond family provides performance, versatility and predictable results. ... the name that stands for adhesive brilliance... Chemistry Behind OptiBond™ Family Total-etch No. of steps Self-etch GPDM Adhesive Monomer 3 2 1 All OptiBond adhesives comprise the unique proprietary chemistry which made OptiBondTM FL the gold standard among bonding agents. Proven GPDM adhesive monomers are effective in creating a superb bond with minimized risk of microleakage and post-operative sensitivity. 4th generation 5th generation 7th generation GPDM = Glycero-Phosphate-1.3 Dimethacrylate Gel Etchant Primer Adhesive 9 Years in market Application Direct procedure Indirect procedure Etching Application time Bond strength Mpa To dentine To enamel Properties Filler load Works on wet or dry dentine Film thickness Radiopacity Solvent Packaging Storage conditions Bottle content Unidose™ content 10 OptiBond™ FL OptiBond™ Solo Plus OptiBond™ All-In-One 15 years 10 years 3 years • Yes 1:30 min. • • Yes 1:10 min. • • No 0:55 min. Filled adhesive technology The technology of filled adhesives was first time ever introduced by Kerr in its OptiBond FL adhesive. Glass Filler in OptiBond Adhesive: • Reinforces the dentin tubules for high bond strengths and protection against microleakage • Releases fluoride over the long-term 32 MPa 33 MPa 31 MPa 34 MPa 36 MPa 26 MPa 48% • ~60 µ 267% Al Water Ethanol 15% • ~10 µ Ethanol 7% • ~5 µ Water, Ethanol, Acetone Ambient temperature Primer Bottle 8 ml Adhesive Bottle 8 ml 0.1 ml Ambient temperature Refrigeration 2 °C to 8 °C 5 ml 5 ml 0.1 ml 0.18 ml • Decreases polymerization shrinkage • Works as a shock absorber and thermal barrier between the restorative material and the tooth • Virtually eliminates post-operative sensitivity • Works well in dry, moist or wet environment Your practice is our inspiration.™ All you need is Kerr Adhesives Restorative Procedure OptiBond™ FL Two-bottle total-etch adhesive system OptiBond FL, from its launch in 1995 established the standard in adhesive technology. Over 15 years it has been successful worldwide, proven in long-term clinical studies and recommended as the gold standard by leading dental universities worldwide. Features After applying OptiBond FL I can achieve a reliable bonding without any post-operative sensitivity. Also I can use successfuly OptiBond FL in any bonding procedure. Prof. Marco Ferrari • Unique structural bond. 48% filler load delivers superior bond strength. • Efficient application flow. One coat primer. One coat adhesive. Wet or dry prep. • Highly radiopaque. 267% radiopacity makes X-ray detection easy. • Delivery options. The only two-bottle adhesive available in bottle and Unidose delivery. • Proven long-term performance. The legend among the adhesives 11 OptiBond™ FL Application Guide Clinical Success OptiBond FL wins REALITY’S 20th Anniversary Legacy Award, emblematic of extraordinary long-term clinical performance. Technique13-year Clinical Study Technique Technique Technique Clinical Evaluation of a Dentin Adhesive Technique Technique Technique Technique 13 Year Results, A. A. Boghosian Summary Summary Summary System: Summary and J.L. Drummond and E. P. Lautenschlager, Summary Summary Summary Summary Northwestern University Feinberg School of Medicine. 1. Etch enamel with Kerr Gel Etchant (35% phosphoric acid) for 15 seconds. 5. Air dry for 5 seconds. 2. Rinse thoroughly for 15 seconds. 6. Using second applicator, apply Adhesive (black rocket for Unidose delivery) with light brushing motion for 15 seconds. 3. Air dry for 3 seconds. Do not dessicate. 7. Air thin for 3 seconds. 4. Apply Primer (yellow rocket for Unidose delivery) with light brushing motion for 15 seconds. 8. Light cure for 20 seconds*. Surface is ready for composite placement. Conclusion: At thirteen years, the OptiBond adhesive system has demonstrated outstanding performance in both retention and sealing of the tooth. OptiBond has further demonstrated effectiveness, in conjunction with composite, eliminating sensitivity resulting from abfraction lesions. Over 10 years posttreament with OptiBond FL. Over 13 years posttreatment with OptiBond FL Cases courtesy of Dr. Alan Boghosian * Recommended Cure Times: Demi 5 sec., L.E.Demetron II 5 sec., L.E.Demetron I, 10 sec. or Optilux 501 in Boost mode 10 sec. 12 Your practice is our inspiration.™ All you need is Kerr Adhesives Restorative Procedure OptiBond™ Solo Plus Single component total-etch adhesive OptiBond Solo Plus is a single component adhesive that combines primer and adhesive in one step. Combining primer and adhesive in one bottle answered the need for a simplerto-use bonding agent that maintained total-etch strength and durability. Features Case courtesy of Prof. Angelo Putignano 13 • Strong bond. Proven performance achieved with simplified application procedure. The durable chemical and micro-mechanical bonds protect against microleakage to ensure superior marginal integrity. • Filled technology. OptiBond Solo Plus is 15%-filled with the same 0.4 micron filler found in Kerr's industry-recognized composites. • Ethanol based. The adhesion promoters are carried in an ethanol solvent, diminishing both the tedious need for multiple coats and constant reapplication commonly found with acetone adhesives. • Versatile. Effective in use for all direct and indirect indications. Use in moist or dry environment. • Unidose™ delivery. Available in bottle and Unidose delivery. High performance easy-touse total-etch adhesive Clinical Research OptiBond™ Solo Plus Application Guide Dentin Shear Bond Strength (MPa) of 5th-Generation Adhesives 35 30 31 25 20 20 21 22 23 23 15 10 5 Table missing 0 Excite® Adper™ Prime® & One Step® OptiBond® Single Bond Bond NT™ Plus Solo Plus™ Published by H. Lu*, H. Bui, X. Qian, D. Tobia, Kerr Corporation, IADR 2008, #401 1. Etch enamel and dentine for 15 seconds. 5. Twist open the unidose. 2. Rinse thoroughly for 15 seconds. 6. Dip brush. Apply OptiBond Solo Plus for 15 seconds using light brushing motion. 3. Air dry for 3 seconds. Do not dessicate. XP Bond™ 4. Shake unidose before dispensing. 7. Air thin for 3 seconds. 8. Light cure for 20 seconds*. Surface is ready for composite placement. STRONG DURABLE BOND. SEM Image shows excellent penetration of OptiBond Solo Plus into demineralized dentin, forming long resin tags and a well-defined hybrid layer, which results in superior bond strength. * Recommended Cure Times: Demi 5 sec., L.E.Demetron II 5 sec., L.E.Demetron I, 10 sec. or Optilux 501 in Boost mode 10 sec. 14 Your practice is our inspiration.™ All you need is Kerr Adhesives Restorative Procedure OptiBond™ All-In-One Single step, self-etch adhesive OptiBond All·In·One Self-Etch Adhesive delivers excellent penetration of dentin tubules, providing exceptional bond strength and protection against microleakage and post-op sensitivity. Its unique nano-etching capability enables the most effective enamel etching of any existing single-component adhesive, creating a deeper etched surface for higher mechanical retention and chemical bonding. In addition its low film thickness creates an effective, single-phase adhesive interface for easier seating and better fit of your final restoration. Effective enamel nano-etching SEM image shows clearly exposed nanoscale enamel hydroxyapatite crystals, which present greater rough surface area for micromechanical retention and chemical bonding. 15 Well defined adhesive layer Dentin Interface and Superb Sealing Ability Provides a Well Defined Adhesive. SEM shows the composite, OptiBond All-In-One adhesive layer and dentin bonding interface. Effective bonding in a simple way Clinical Research OptiBond™ All-In-One Application Guide Shear Bond Strength of Single-Component Self-Etch Adhesive Systems to Human Dentine (24 hr)* 35 20 seconds Shear Bond Strength (MPa) 35,0 30 25 20 20,2 15 10 10,3 5 0 Clearfil® S3 Bond 2. Twist open. 3. Dip brush. 4. Apply first application with scrubbing motion. 20 seconds 4. Apply second application with scrubbing motion. 7. Gently air dry, then use medium force to air dry for at least 5 seconds. 8. Light cure for 10 seconds*. iBond™ Xeno® IV 28,2 25 20 21,7 23,0 21,6 15 10 11,3 5 0 GBond™ iBond™ Xeno® IV OptiBond® All•In•One * Study conducted by Dr. James Dunn of Loma Linda University. Trademarks are property of their respective owners. * Recommended Cure Times: Demi 5 sec., L.E.Demetron II 5 sec., L.E.Demetron I, 10 sec. or Optilux 501 in Boost mode 10 sec. 16 OptiBond® All•In•One 30 Clearfil® S3 Bond 5. Dip brush. GBond™ Shear Bond Strength of Single-Component Self-Etch Adhesive Systems to Bovine Enamel (24 hr)* Shear Bond Strength (MPa) 1. Shake. 32,2 30,4 Your practice is our inspiration.™ All you need is Kerr Composites Restorative Procedure COMPOSITES Since the ancient times great philosophers, such as Plato, Baumgarten, Kant, Hegel, Vico and Croce, have sought to place the concept of aesthetics and beauty on a rational and “scientific” basis.The triad of beauty, goodness and truth represents the ideal to which individuals should aspire in the attainment of what is called “perfection”, which perhaps does not exist. Most widely shared concepts on perceived beauty arise from interaction between “sensibility” emotional and instinctive influence, and “intellect” or rational factors. Hutchinson and Shaftesbury defined felicitously aesthetics as the aptitude for perceiving harmony (Inquiry into the origin of our ideas of beauty 1725). Cosmetics is usually regarded as the quest for a stereotype of beauty regardless of the context of the subject. Whereas, aesthetics is an expression of a natural archetype in accordance with mathematical proportions with distinct and measurable ideals of beauty. In this respect, an inate sense of aesthetics has been theorized, defined as the passive ability to receive ideas of beauty from all objects in which there is uniformity in variety (“harmony”) (1). These objective factors, which accept an interaction between the object and the “mental categories” of the observer, provide the rational basis of beauty. Numerous rules of beauty 17 Aesthetics and composite Prof. Angelo Putignano, University of Marche, Ancona, Italy have been applied to anatomy in formulating dentofacial proportions coherent with the “golden section” (Leonardo), or in accordance with anthropometric (cephalometric) parameters adopted from epidemiological studies. However, there are a series of subjective factors peculiar to instinctive emotional and psychological context of the observer, which can significantly condition the sensitivity to beauty. Taste and perception of beauty are correlated with the era and specific historical, cultural and social context which the observer inhabits. Pilkington defined dental aesthetics in 1936 as “the science of copying, harmonising our work with that of nature, seeking to minimise it as much as possible”. A few decades ago, the majority of dentists working in the field of restorative dentistry concentrated on long-term solutions and the appearance of the restorations was of secondary importance (2). In practice, amalgam restorations and gold alloy crowns were utilised as the main and most lasting solutions and patients accepted these dental restorations despite their poor appearance. The evolution of preventive and conservative dentistry has had a great impact on the development of restorative aesthetic dentistry. The success of preventive dentistry has resulted in teeth without caries and therefore white and not restored, with a resulting increase in the demand for aesthetic restorations. Good appearance, together with good overall health, with adequate restoration of function, and an attractive smile play an important role in modern society. In general, a smile is beautiful when the teeth are well characterised in respect to their shape, contour, colour, surface texture and detail, emergence profile, angle and position, and incisal occlusion. A successful aesthetic restoration will appear to be completely natural, provide function, preserve as much healthy tooth structure as possible and support a healthy periodontium. To achieve this objective the clinician must select the most suitable materials for resistance, biocompatibility, and of course aesthetic appearance. Composite resins have been in use for over three decades and nowadays adopted more and more often because of their excellent aesthetics and their improved mechanical properties (3). The term composite refers to a combination of at least two chemically diverse materials, with a distinct interface to separate the two components. Superior properties are exhibited when in combination, as compared to when used separately. When formulating a composite resin, we identify three different components: • Organic matrix; • Inorganic filler; • Binding agent. 18 The organic matrix of the most modern composite resins consists mainly of the monomer developed by Bowen in 1957, through a reaction between one molecule of bisphenol A and two molecules of glycidyl methacrylate (GMA). This yields a viscous monomer of high molecular weight which is called BISGMA. In the composite resin matrix there are other monomers of lower molecular weight in lower percentages such as TEDGMA (triethylene glycol dimethacrylate, the most used), UEDMA (diurethane dimethacrylate, sometimes used as the sole component of the matrix), MMA (methyl methacrylate) and others of less importance. The second component of a composite resin is the inorganic filler, which is added to the matrix to improve its physical properties which are otherwise insufficient, such as hardness, resistance to compression, resistance to wear and impermeability. The fillers can be classified on the basis of their chemical nature into fillers based on silicon dioxide or colloidal silica, quartz, vitreous materials, other metals or zirconium. On the other hand, Bayne in 1994 suggested the following subdivision based on the diameter of the particles: • mega fillers (from 2 to 0.5 mm) • macro fillers (from 100 to 10 µm) • medium fillers (from 10 to 1 µm) • mini fillers (from 1 to 0.1 µm) • micro fillers (from 0.1 to 0.01 µm) • nano fillers (from 0.01 to 0.005 µm) Based on production techniques, conventional or traditional fillers are produced by trituration of the inorganic substances listed above, obtaining a macro filler with particles of irregular shape and size, which require little monomer to become wet, therefore conferring less viscosity, but they make the restoration difficult to finish and polish and also favour the formation of micro fractures. Fillers obtained by precipitation of pyrogenic silica at high temperatures, introduced successively, Your practice is our inspiration.™ All you need is Kerr Composites Restorative Procedure consist of spherical particles of microfiller (between 0.04 and 0.06 µm). One of the most innovative products in this family of materials is the micro filler composite with prepolymerized spherical particles. The micro fillers in general are able to provide a significant advance in the qualities of the composite; in addition, this particular type of micro filler confers further advantages due to the spherical shape of the filler: • Better matrix-filler bond; • Less internal matrix-filler tension as there are prepolymerized spheres loaded with evenly distributed SiO2; • Consequent improvement in wear and fatigue characteristics. However, this class of materials does not represent the solution to all the requirements of a dental restoration, as even they are affected by technical gaps: the micro fillers are not capable of supporting high occlusal loads, especially because of the lower resistance of the pyrogenic silica when compared with fillers based on glass and above all quartz. Moreover, contraction due to polymerization represents one of the major weak points of the micro fillers; this can compromise the toothrestoration interface, the most critical zone of a restorative treatment (4,5). The experience obtained with traditional macro composites (TC) and micro fillers, both homogeneous and non-homogeneous (HMC and IMC), has provided the manufacturers with the knowledge base needed for achieving a material that can now be used in all classes of dental cavities, as it has both the physical 19 characteristics of the former and the aesthetic characteristics of the latter: the hybrid composites. Hybrid composites are highly loaded materials (over 70% in volume). The technology of the hybrids is based on the presence of a double dispersed phase, consisting of ceramic-vitreous macro particles similar to the macro fillers, though of more limited dimensions (for the most part between 10 and 50 µm), as well as micro particles consisting of pyrogenic silica, which are typical of the micro fillers (approximate dimensions 0.04-0.06 µm) (6). The mixed filler provides a clear improvement in the material in both the physical characteristics and the aesthetic benefit. The macro particles are responsible for the increased mechanical resistance of the material because they have a higher elasticity modulus compared to that of the matrix with which they form a single body. In this way, an applied force should induce flexion of the particles before it can act on the resin, which is the real weak point during the application of loads. Furthermore, the high filling value reduces the percentage of resin employed, consequently reducing the contraction on polymerization. The improved aesthetic benefit is a function of the presence of the micro filler, which guarantees better polishing and an extremely wide range of shades (7, 8). The third component of composite is a silane coupling agent, a bifunctional molecule capable of binding two different materials. Silane is an organic silicon glue which has two functional groups, one of which binds to the methacrylate groups of the resin, the other to the silicon dioxide of the filler. Composite resins harden when the monomers form long chain polymers. This is called polymerization. In addition, there is an initiator in the resin, a molecule that, when activated, provides the free radicals necessary for polymerization to progress. The most commonly used initiator employs visible light or UV rays to become activated (9). Those belonging to the second group, now fallen into disuse, are basically represented by benzoinodimethyl ether, whereas a diketone is the most widely used molecule in the most common and recent composites: camphoroquinone together with NN-dimethylaminoethylmethacrylate. Activation of the diketone initiator is by a lamp using visible light with a wavelength between 430 and 480 nm. These molecules initiate polymerization by forming a three-dimensional network with many cross-links; while the reticulation process is proceeding, the levels of free radicals and the dimethacrylate molecules not involved in the process tend to drop drastically, preventing complete conversion of the double bonds of the dimethacrylate. When the composite hardens, the degree of conversion (DC), which is the percentage of monomers that undergo polymerization, hardly exceeds 75% under standard conditions. The degree of conversion is a determinant for a series of physical properties of the composite, such as hardness and resistance to wear. When two monomers combine the molecular structure is shortened. Therefore the greater degree of conversion will increase the percentage of contraction, because the overall length of a polymer is less than that of the individual monomers. In fact, the monomers combine with covalent bonds, assuming a distance between one another that is three times lower than that of the Van der Waals bonds that exist between one monomer and another. A composite will contract more when used in a single mass (bulk fill) than with minimal successive increments (incremental fill). The direction of contraction depends on the shape of the cavity and the strength of adhesion. In fact, adhesive placed on the walls of the cavity opposes the contraction of the composite, so that the surface of the material that is in contact with a wall of the cavity cannot contract because of the prevailing effect of the adhesive. Therefore, if the composite is in contact with one wall only, the contraction takes place towards it and involves all the other free surfaces. If there are two walls, the remaining unsupported surface will be left free to contract; if all the walls of a cavity are present, the composite adheres to them and the only wall free to contract is the occlusal one. Therefore, the greater the number of walls to which the composite adheres, the greater is the C-factor, that is, the relationship between the adhesive surface and the free surface and thus the greater is the stress to which the material will be subjected when contracting, as Feilzer stated in 1987. The stress within the tooth-composite interface has been measured at about 4 MPa for each surface. 20 During polymerization, there are two phases, one called the pre-gel phase in which contraction of the composite is compensated by the intrinsic flowing of the material, so as to diminish the contraction and reduce stress; the second is called the post-gel phase, separated from the former by a gel point, in which the material is no longer able to run to compensate the contraction so that stress is produced. A rigid composite will have a higher modulus of elasticity or Young’s modulus, and will develop more stress during polymerization, having a shorter pre-gel phase; conversely, a fluid composite will have a lower modulus of elasticity with a longer pre-gel phase. Although the composites are regarded as optimal materials, they certainly have certain limits that may potentially frustrate the aims of a restoration. The main deficiency, and this applies for all classes of composite including the hybrids, is contraction on polymerization, that is, the reduction in volume that the resin undergoes during the polyaddition phase. As a result there is potential that a marginal defect will form between the tooth and the filling caused by the contraction. On the other hand, the absence of the formation of a fissure introduces tensile forces into the restoration that will strain the tooth walls, with the risk of fracturing them, or strain the restoration itself with subsequent failure of the restoration. In order to avoid this, clinical cases considered for direct restorative treatment with composite resins should be assessed carefully. Appropriate techniques must be used to compensate for the limitations, albeit reduced in the case of hybrids resin systems. Even if the evolution of the composites is approaching its technological limit, there is certainly scope for improvement and it is possible that in the near future there may be a self-adhesive composite resin, that will be the material of choice in aesthetic reconstructions. The hybrids come closest to the ideal material from the aesthetic point of view although, like all composites, they have some undesirable physical properties which have not yet been fully resolved. References 1. Ceruti A, Mangani F, Putignano A. Odontoiatria estetica adesiva – Didattica Multimediale. Ed. Quintessence. 2008 Cap.1; p:18-20. 2. Christensen GJ. Longevity versus Esthetics. The Great Restorative Debate. JADA 2007, 138, 1013-1015. 3. Raj V, Macedo GV, Ritter AV. Longevity of Posterior Composite Restorations. Journal Compilation 2007, 19(1), 3-5. 4. Abe Y, Lambrechts P, Inoue S, et al. Dynamic elastic modulus of “packable” composites. Dent Mater 2001;17:520-5. 5. Burgess JO, Walker R, Davidson JM. Posterior resin-based composite: review of the literature. Pediatr Dent 2002;24:465-79. Review. 6. Dino R, Cerutti A, Mangani F, Putignano A. Restauri estetico-adesivi indiretti parziali nei settori posteriori. Ed.U.T.E.T. 2007 Cap. 2; p: 18-22. 7. Christensen GJ. Preventing postoperative tooth sensitivity in class I, II and V restorations. J Am Dent Assoc 2002;133:229-31. 8. Fabianelli A, Goracci C, Ferrari M. Sealing ability of packable resin composites in class II restorations. J Adhes Dent 2003 Fall; 5:217-23 9. Lee IB, Son HH, Um CM. Rheologic properties of flowable, conventional hybrid, and condensable composite resins. Dent Mater 2003;19:298-307. Your practice is our inspiration.™ All you need is Kerr Composites Restorative Procedure Herculite® XRV Ultra™ The legacy of Herculite For 25 years Herculite XRV has been the industry standard for composite restoratives. Herculite XRV Ultra is a nanohybrid version of Herculite XRV (microhybrid), that incorporates more biomimetic, “tooth-like” features into a restoration. Based on the latest nanofiller technology, in addition to offering improved handling, polishability and wear resistance, Herculite XRV Ultra delivers an improved lifelike appearance to final restorations by replicating the opalescence and fluorescence of the natural tooth. Herculite restoration after 13 years Case courtesy of A. A. Boghosian, J. L. Drummond and E.P. Lautenschlager – Study conducted by Northwestern University The Advantages of Nanotechnology Herculite Ultra’s advanced nanotechnology delivers additional benefits that can’t be found in traditional microhybrid composites. As a nanohybrid composite, Herculite XRV Ultra combines conventional hybrid fillers with smaller filler particles in size of about 50 nm. These smaller particles enable Herculite XRV Ultra to deliver improved polish and clinical gloss, better aesthetics and superior mechanical strength. 21 Compared to Other Composites Plucking, or natural wear over time, tends to occur faster in restorations with larger particles, decreasing the overall life and esthetics of the restoration. When polymerized, the large prepolymerized particles virtually disappear and the surface is easily polishable. The polished surface consists only of nanohybrid particles below the wavelength of visible light. Nanohybrid composite Improved Handling Clinical Research Gloss Retention Handling Comparison Map Over time, resin in a composite restoration wears off, exposing glass fillers and creating a rough surface. If the filler size is smaller than the average wavelength of light (as in the case of Herculite Ultra, Premise™, and Point 4™), light will be diffused uniformly and the surface will appear glossy, resulting in superior gloss retention over time despite resin wear. Sticky Z100™ TPH3 Esthet X Venus Point 4 Filtek Z250 Herculite XRV ™ Grandio Creamy Stiff Premise ™ Gradia™ Direct Toothbrush test, University of Leeds Filtek™ Supreme Plus 90 Herculite XRV Ultra 73 80 70 69.1 65.2 62.3 51.1 60 50 Non-Sticky Map was created with input from various clinicians and Kerr R&D. 40 30 20 10 0 Here’s what clinicians are saying about Herculite XRV Ultra Herculite® Ultra Kerr Herculite Ultra 5 4,85 4,54 Miris™ Coltene Whaledent Venus Before “Adapts really well, not sticky at all, really sculptable”. “Superb for a nanohybrid. Best composite ever”. 4 Tetric EvoCeram® Ivoclar 4,69 4,77 4,77 4,69 Thickness Adaptability Compression w/ Instrument Adherence to Instrument 4,92 3 After 2 1 Worst 0 Handling Stickiness/ Tackiness Resistance to Slumping Photographs courtesy of University of Leeds 22 Filtek™ Z250 3M Gloss meter readings were taken using a gloss meter at 600 minutes after the initial reading. 90% of focus group attendees said they would purchase Herculite Ultra over their current composite. Best Venus® Heraeus Kulzer Your practice is our inspiration.™ Tetric Evoceram All you need is Kerr Composites Restorative Procedure Herculite XRV Ultra in Clinical Cases Class IV Case courtesy of Prof. Angelo Putignano. 23 1) Initial case. 2) Teeth models taken for diagnostic wax-up. 3) Silicne key from diagnostic wax-up. 4) Silicone key located. 5) The case with applied OptiDam. 6) Silicone key with OptiDam. 24 7) Etching for 15 seconds with Gel Etchant. 8) Palatinal wall A2 Enamel mass, small amount of A3 dentin on the most coronal part of the injury was placed. 9) A2 dentin mass was applied to cover the former layer and sculpted with grooves. 10) The incisal mass is used both around and between the grooves to create a translucent effect and to highlight the grooves. 11) The most coronal part is then slightly pigmented with orange, while whitish areas are designed with Kolor + Plus® White. 12) Labial A2 enamel mass applied in a very fine layer. 13) The case after fininishing and polishing. 14) The completed case after the 10-day follow-up. Your practice is our inspiration.™ All you need is Kerr Composites Restorative Procedure Class V Case courtesy of Prof. Angelo Putignano. The present case concerns a 30 year old patient with multiple erosions from particular dietary habits and inadequate oral hygiene: 25 1) Initial situation, erosions on 1.1 and 2.1. 2) RubberDam isolation. 3) Gentle roughening of sclerotic dentin with rounded carbide bur. 4) Finishing line with 20 micron diamond bur. 5) Etching with 37% phosphoric acid. 6) OptiBond Solo Plus adhesive applied with scrubbing motion for 15 seconds; light cured for 10 seconds with Demi. 7) Application of a thin layer of Premise Flow A3.5; light cure for 20 seconds with Demi. 8) First layer of Herculite XRV Ultra, A3 Enamel, on cervical part; light cure for 20 seconds. 9) Second and last layer of Herculite XRV Ultra, A3 Enamel; light cure for 20 seconds. 10) Finishing with OptiDisc Coarse/Medium, small size. 11) Polishing with GlossPlus Polisher Minipoint. 12) High gloss polishing with HiLuster Dia Polisher Minipoint. 13) Final case after RubberDam removal. 26 Your practice is our inspiration.™ All you need is Kerr Composites Restorative Procedure Class II Case courtesy of Prof. Angelo Putignano. 27 1) Initial case. 2) Preliminary preparation. 3) Cavity smoothing with Pasteless prophy without fluoride. 4) Cavity preparation after caries removal revealing sclerotic dentin. 5) Etching with Gel Etchant 15 seconds. 6) Bonding with OptiBond Solo Plus. Apply for 15 seconds and light cure for 10 seconds. 7) A thin layer of Premise Flow. 8) Build-up of interproximal wall. 28 9) First layer of Herculite XRV Ultra, Dentin A3,5, light cured for 20 seconds. 10) Buccal dentin masses A3, light cured for 10 seconds. 11) Lingual dentin masses A3, light cured for 10 seconds. 12) A thin layer of Enamel A3 under glycerin to avoid air inhibition. 13) Interproximal emergence profile of restoration. 14) Finishing procedure with multi-blade bur. 15) Occlusal check. 16) Polishing with OptiShine. 17) Final result. Your practice is our inspiration.™ All you need is Kerr Composites Restorative Procedure Class I Case courtesy of Prof. Angelo Putignano. 29 1) Initial case. 2) Prepared cavity. 3) Etching with Gel Etchant 15 seconds. 4) Bonding with OptiBond Solo Plus, apply for 15 seconds and light cure for 10 seconds. 5) Dentin layer A3, light cured for 20 seconds. 6) Final result. 30 Your practice is our inspiration.™ All you need is Kerr Finishing and Polishing Restorative Procedure Finishing and Polishing Superior aesthetics is one of the key features of dental composite restorations. Shading, optical appearance and surface texture of a tooth coloured restoration is crucial for patient’s satisfaction and comfort [Jones et al., 2004]. The behaviour of composites in the biological environment of the oral cavity are strongly influenced by surface quality. Surface irregularities enhance plaque accumulation [Ikeda et al., 2007], which in turn can lead to secondary caries and inflammation of the adjacent gingival tissues. Especially in case of restorations that are exposed to strong occlusal load and parafunctional activity, surface roughness affects the wear resistance and the abrasivity of dental composites [Willems et al., 1991; Mandikos et al., 2001]. Rough composite surfaces are liable to discoloration and staining [Patel et al., 2004; Lu et al., 2005]. Moreover, material properties such as mechanical and flexural strength as well as microhardness of resin based composites are improved by minimizing surface roughness [Gordan et al., 2003; Venturini et al., 2006; Lohbauer et al., 2008]. Thus accomplishing a superior surface finish is a 31 Finishing and polishing of composite restorations Prof. Martin Jung, Justus-Liebig-University, Giessen, Germany prerequisite for patient’s satisfaction and for the longevity of a composite restoration. Composite surfaces, that are cured against a mylar matrix, show minimum surface roughness [Yap et al., 1997; Ergücü and Türkün, 2007; Üctasli et al., 2007; Korkmaz et al., 2008] Clinically, most composite restorations require further finishing and polishing after placement. Finishing includes elimination of excessive material, adjustment of surface morphology and removal of occlusal interferences. This causes a roughening of surfaces, which must be eliminated by subsequent polishing. Rotary polishing instruments must be equally effective when exposed to hard filler particles and soft resin matrix, without damaging the composite surface. Instruments for finishing require a degree of cutting efficiency without leaving the surfaces rough. Finally, rotary instruments for finishing and polishing must work on different types of surface morphology (flat, convex concave surfaces). There are two types of burs recommended for initial finishing of composite restorations; they are diamond and tungsten carbide finishing burs. Finishing diamonds are characterized by a comparatively high cutting efficiency, depending on the size of the abrasive diamond particles [Jung, 1997]. Due to the aggressive effect of the diamond particles, finishing diamonds leave composite surfaces in a rough state [Jung et al., 2007b]. Case courtesy of Prof. Angelo Putignano Tungsten carbide finishing burs vary with respect to the number and orientation of the cutting flutes. These instruments are characterized by a limited cutting efficiency and achieve a smooth composite surface with only little remaining roughness [Jung, 1997; Barbosa et al., 2005; Turssi et al., 2005]. There is some controversy in the literature as to whether there are significant differences between different types of tungsten carbide finishing burs with respect to the resultant surface quality [Jung, 1997; Radlanski and Best, 2007]. After initial finishing and contouring the composite surfaces are in a variably rough state, depending on the extent and amount of corrective work and on the number and type of burs used. In order to accomplish a superior aesthetic result, maximum reduction of remaining roughness is necessary by subsequent polishing. surfaces [Tjan and Clayton, 1989; Wilson et al., 1990; Hoelscher et al., 1998; Setcos et al., 1999; Roeder et al., 2000; Üctasli et al., 2007]. Because of their shape, flexible discs are efficient on flat or convex surfaces; they are not recommended for application on concave surfaces [Chen et al., 1988; Tjan and Clayton, 1989]. Discs of different diameter and thickness can be adapted to several clinical situations. Most disc systems are available in three or four working steps, permitting a high cutting efficiency and effective roughness reduction. For this reason, flexible discs represent the only technique which can be used both for finishing and polishing. There are a great number of polishing techniques available for composite restorations. Polishing systems vary with respect to the shape and size of the individual instruments, and the number of working steps. Flexible discs generally yield well smoothened composite surfaces and permit an effective reduction of remaining roughness. For this reason, flexible discs were regarded as some kind of clinical polishing standard for composite 32 Case courtesy of Dr. Joseph Sabbagh Rubber polishers are supplied in various sizes and shapes enabling the application of rubber polishers to both convex and concave composite restoration surfaces. Most of the products in this group are made of rubber-like silicon matrix. The abrasive particles which are integrated into the matrix are usually made of silicon carbide or dioxide, aluminium oxide or diamond particles in different grain sizes. The way these rubber polishers are used differs considerably. It varies from a single-step application to two, three or four working steps. The polishing efficiency is dependent on the individual products used. Many systems achieved a good composite surface quality, comparable to or even better than flexible discs [Jung et al., 2003; Jung et al., 2007a]. Other products caused less favourable polishing results [Ergücü and Türkün, 2007; Cenci et al., 2008]. The efficiency of one-step vs. multi-step systems is discussed in the literature [Da Costa et al., 2007; Jung et al., 2007a]. Polishing brushes represent a different approach towards minimizing composite roughness. Silicon carbide abrasive particles are integrated into the matrix of special synthetic filaments. This enables a universal application of polishing brushes on different types of composite surface morphology. Polishing brushes are one-step systems; their polishing efficiency is favourable but depends on the quality of initial finishing [Krejci et al., 1999; Jung et al., 2007a]. Your practice is our inspiration.™ All you need is Kerr Finishing and Polishing Restorative Procedure Felt wheels are another one-step polishing system, with abrasive diamond particles attached to a felt matrix with wax. Felt wheels can be used on various types of composite surfaces because of the soft matrix. Felt wheels must be discarded after a single use for infection control. The polishing results depend strongly on the kind of initial finishing [Jung et al., 1997; Jung et al., 2003; Scheibe et al., 2009]. Finally, gels are an alternative for polishing composites. Their application in a single or few steps is possible on all types of surfaces. Polishing gels are used on discs, plastic tips or brushes. A diamond based polishing paste achieved favourable results on a hybrid composite [Jung, 2002]. Polishing pastes based on diamond particles achieved lower roughness compared to aluminium-oxide gels [Kaplan et al., 1996]. The use of gels as a final polishing step is recommended [Turssi et al., 2000; Radlanski and Best, 2007]. 33 For rotary instruments there is only limited access to proximal surfaces. This special situation requires the use of manual finishing and polishing strips, although their polishing efficiency seems to be limited [Whitehead et al., 1990]. Alternatively diamond-coated oscillating finishing files may be used in cases with greater amounts of excess composite material in the proximal-cervical area of composite restorations. Oscillating diamond files caused rough areas after application to cervical margins of composite-inlays. A subsequent use of polishing paste on plastic files achieved a reduction of remaining surface roughness [Small et al., 1992]. The choice of an appropriate system for finishing and polishing of composite restorations depends on a several factors; there is no universal system for all clinical indications. The accessibility and morphology (convex or concave) of surfaces and the need and extent for initial finishing is of great importance. Finally the choice of a particular polishing system should be made based on the texture and roughness of the surfaces after initial finishing. The success of one-step polishing systems is strongly dependent on the surface roughness after initial finishing. Polishing systems with two or more working steps are less sensitive to the kind of initial finishing. All references are available upon request. Surface treatment of composite filling Surface Roughness Occlusal / Concave Surfaces CONTOURING Adjust primary geometric form. Carbide Bur 12 Blades Diamond 40 µm Dia: sRa=1.25 µm Carbide Bur 30 Blades Diamond 20 µm Dia: sRa=0.56 µm FINISHING Remove composite excesses. Shape Occlusal anatomy, lingual fissures, secondary anatomy. POLISHING Eliminate surface scratches. Reduce surface roughness below Ra = 0.35 µm. Occlubrush and OptiShine is universal polishing tool for all occlusal and concave posterior surfaces Occlubrush OptiShine Gloss GlossP: sRa=0.26 µm HiLuster HiLust: sRa=0.10 µm HIGH GLOSS POLISHING Reduce surface roughness to high gloss below Ra = 0.2 µm. 34 Your practice is our inspiration.™ All you need is Kerr Finishing and Polishing Restorative Procedure Surface Roughness Convex / Flat Surfaces CONTOURING Adjust primary geometric form. Carbide Bur 12 Blades Diamond 40 µm OptiDisc Extra-Coarse Disc: sRa=1.20 µm Carbide Bur 30 Blades Diamond 20 µm OptiDisc Coarse-Medium Disc: sRa=0.63 µm FINISHING Remove composite excess. Shape Occlusal anatomy, lingual fissures, secondary anatomy. POLISHING Eliminate surface scratches. Reduce surface roughness below Ra = 0.35 µm. OptiDisc Fine OptiShine Gloss Polisher Disc: sRa=0.33 µm HiLuster Polisher Disc: sRa=0.12 µm HIGH GLOSS POLISHING Reduce surface roughness to high gloss below Ra = 0.2 µm. OptiDisc Extra-Fine 35 Surface Roughness Interproximal Surfaces CONTOURING Adjust primary geometric form. Diamond strip not recommended for anterior application Diamond 40 µm Diamond Strip Strip: sRa=0.90 µm Diamond 20 µm Finishing OptiStrip Strip: sRa=0.58 µm FINISHING Remove composite excesses. Shape Occlusal anatomy, lingual fissures, secondary anatomy. POLISHING Eliminate surface scratches. Reduce surface roughness below Ra = 0.35 µm. OptiDisc can also be used interproximally Polishing OptiStrip OptiShine OptiDisc OShine: sRa=0.25 µm HiLuster HiLust: sRa=0.10 µm HIGH GLOSS POLISHING Reduce surface roughness to high gloss below Ra = 0.2 µm. 36 Your practice is our inspiration.™ All you need is Kerr Finishing and Polishing Restorative Procedure OptiDisc® The first translucent finishing and polishing disc that is both gentle and more efficient. The flexible discs are used for finishing and polishing of composites, glass-ionomers, amalgams, semiprecious and precious metals. The use of the complete system gives the restoration a final polish equal to the natural dentition. OptiDisc KERR Sof-Lex XTTM 3M ESPE Features • Unique fixation between disc and mandrel. Optimal torque transmission to disc, no sliding and no rpm sensitive. • Optimized disc flexibility. For excellent adaptation to tooth anatomy. • Translucent discs. Good view of the working area. • Colour coded stages of abrasivity. Easy recognition of grit size. • Ready to use abrasive layer. High efficiency. Uncoated cutting edges for high efficiency from the start. Disc: sRa=1.20 µm Disc: sRa=0.63 µm Disc: sRa=0.33 µm Ø 37 15.9mm 12.6mm 9.6mm Disc: sRa=0.12 µm The Mandrel • Metal mandrel • Patented mandrel design. Mandrel is placed below the surface of the disc to avoid contact with the tooth. • Special coating of the mandrel. Protection against metal marking of restoration. Abrasive coating OptiDisc Kerr 200 µm < > Extra-Coarse Coarse-Medium Fine OptiDisc can be turned on the mandrel in order to have an easy access of active side on mesial and distal surface of the tooth. Extra-Fine 200 µm < > Coarse Medium Sof-Lex XTTM 3M ESPE Super Fine Fine SEM pictures show comparison of abrasive coating of 2 competitive materials. Mass removal after each application of 20 sec. on Point4 SEM pictures courtesy of Dr. Jean-Pierre Salomon, France 0.0160 0.0140 3M Soft-Lex OptiDisc Glue Glue Abrasive Polyester Foil Mass removal (g) 0.0120 Abrasive 0.0100 0.0080 0.0060 0.0040 0.0020 OptiDisc TM Sof-Lex XT 3M ESPE OptiDisc has a ready to use abrasive layer - uncoated cutting edges for high efficiency from the start. 38 0.0000 3M Coarse 3M Medium Hawe Extra coarse Hawe Medium/Coarse Your practice is our inspiration.™ Fine Super Fine All you need is Kerr Finishing and Polishing Restorative Procedure HiLusterPlus Polishing system 2-step polishing system for composites Features • High-gloss results in only 2 steps. Smooth surface and high gloss in two steps. • Efficient. Pre- and gloss polishing in one single step by efficient GlossPLUS polishers, final roughness after first step around sRa 0.25 µm. • Diamond particles. Outstanding final result thanks to diamond particles integrated in the HiLusterPLUS polisher, final roughness around sRa 0.10 µm is achieved after second step. • Optimum flexibility. The flexibility of the polishers is optimized for excellent adaptation to the tooth anatomy. • Good adhesion between the mandrel and the polisher. Avoids detachment of abrasive parts. • Hygienic. Can be autoclaved at 134 °C. GlossPLUS Polishers Flame Part. No. 2651 Minipoint Part. No. 2652 Cup Part. No. 2653 Disc Part. No. 2654 Material of Polisher: GlossPlus Polisher: HiLusterPlus Dia Polisher: Material of Mandrel: Aluminium oxide particles embedded into a silicone elastomer. (mean particle size: 20 microns) Silicone carbide and diamond particles (5 microns) embedded into a silicon elastomer. Golden coated mandrel HiLusterPLUS Dia Polishers Flame Part. No. 2661 Minipoint Part. No. 2662 Cup Part. No. 2663 Disc Part. No. 2664 39 GlossP: sRa=0.26 µm HiLust: sRa=0.10 µm Usage on different surfaces Comparison HiLuster Polishing System and Enhance+PoGo polishing system used on Herculite XRV Ultra 1: Reference surface OptiDisc coarse/medium GlossPlus Polisher OptiDisc sRa: 0.56 µm 2: Polishing Flame Minipoint Minipoint Enhance + PoGo HiLusterPLUS Polishing system Enhance sRa: 0.6 µm GlossPLUS sRa: 0.27 µm PoGo HiLusterPLUS Polishing system Enhance sRa: 0.32 µm HiLusterPLUS Dia sRa: 0.14 µm Cup 2: High Gloss Polishing HiLusterPlus Dia Polisher Enhance is a very aggressive polisher, leaving high surface roughness. PoGo polisher has the ability to smooth the surface after Enhance but the final surface roughness sRa = 0.32 µm is not considered as high gloss surface. A much smoother and high gloss surface of sRa = 0.14 µm is achieved with 2-step HiLuster Polishing system. Flame 40 Minipoint Minipoint Cup Your practice is our inspiration.™ All you need is Kerr Finishing and Polishing Restorative Procedure OptiShine The first concave-shaped polishing brush Features • Efficient in practice. The concave shape of the brush is efficient on all tooth surfaces, also on less accessible surfaces like interproximal and occlusal fissures. • Universal use. Always produces excellent polishing results for all restorations due to the concave shape of the brush. Reduce the surface roughness without changing the anatomical shape and the micro surface texture. • Excellent polish. The polishing effect is created by polishing particles embedded in the bristles (silicone carbide), therefore no paste is necessary. • Durable for multiple use. Autoclavable at 134 °C, at least 3 min. No effect on the polishing performance. Good accessibility due to concave shape of OptiShine. Each bristle is a polishing instrument. Specialfibres with in-built silicon-carbide abrasive particles. Not liable to confusion. Easily recognisable by the golden shaft. OShine: sRa=0.25 µm Good accesses to the fissures and occlusal surfaces. 41 Herculite XRV References OptiBond FL References 1. 1. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. 20. Effect of delivering light in specific narrow bandwidths from 394 to 515nm on the micro-hardness of resin composites. Price RB, Felix CA. Dent Mater. 2009 Feb 23. Shear strength evaluation of composite-composite resin associations. Ribeiro JC, Gomes PN, Moysés MR, Dias SC, Pereira LJ, Ribeiro JG. J Dent. 2008 May;36(5):326-30. Epub 2008 Mar 11. Polymerization stress of resin composites as a function of system compliance. Gonçalves F, Pfeifer CS, Meira JB, Ballester RY, Lima RG, Braga RR. Dent Mater. 2008 May;24(5):645-52. Epub 2007 Aug 24. Cytotoxicity of resin composites as a function of interface area. Franz A, König F, Skolka A, Sperr W, Bauer P, Lucas T, Watts DC, Schedle A. Dent Mater. 2007 Nov;23(11):1438-46. Epub 2007 Aug 3. The evaluation of direct composite restorations for the worn mandibular anterior dentition - clinical performance and patient satisfaction. Poyser NJ, Briggs PF, Chana HS, Kelleher MG, Porter RW, Patel MM. J Oral Rehabil. 2007 May;34(5):361-76. Surface texture of four nanofilled and one hybrid composite after finishing. Jung M, Sehr K, Klimek J. Oper Dent. 2007 Jan-Feb;32(1):45-52. Residual stress in composites with the thin-ring-slitting approach. Park JW, Ferracane JL. J Dent Res. 2006 Oct;85(10):945-9. Effect of light-curing method on marginal adaptation, microleakage, and microhardness of composite restorations. Ritter AV, Cavalcante LM, Swift EJ Jr, Thompson JY, Pimenta LA. J Biomed Mater Res B Appl Biomater. 2006 Aug;78(2):302-11. The effects of thermocycling on the flexural strength and flexural modulus of modern resin-based filling materials. Janda R, Roulet JF, Latta M, Rüttermann S. Dent Mater. 2006 Dec;22(12):1103-8. Epub 2006 Jan 10. A clinical evaluation of posterior composite restorations: 17-year findings. da Rosa Rodolpho PA, Cenci MS, Donassollo TA, Loguércio AD, Demarco FF. J Dent. 2006 Aug;34(7):427-35. Epub 2005 Nov 28. Polishing occlusal surfaces of direct Class II composite restorations in vivo. Jung M, Hornung K, Klimek J. Oper Dent. 2005 Mar-Apr;30(2):139-46. The survival and clinical performance of resin-based composite restorations used to treat localised anterior tooth wear. Redman CD, Hemmings KW, Good JA. Br Dent J. 2003 May 24;194(10):566-72; discussion 559. In vivo comparison of a microfilled and a hybrid minifilled composite resin in Class III restorations: 2-year follow-up. Reusens B, D'hoore W, Vreven J. Clin Oral Investig. 1999 Jun;3(2):62-9. Tooth wear treated with direct composite restorations at an increased vertical dimension: results at 30 months. Hemmings KW, Darbar UR, Vaughan S. J Prosthet Dent. 2000 Mar;83(3):287-93. A 4-year retrospective clinical study of Class I and Class II composite restorations. Geurtsen W, Schoeler U. J Dent. 1997 May-Jul;25(3-4):229-32. Stratification of composite restorations: systematic and durable replication of natural aesthetics. Magne P, Holz J. Pract Periodontics Aesthet Dent. 1996 Jan-Feb;8(1):61-8; quiz 70. A clinical evaluation of posterior composite resin restorations. Bryant RW, Hodge KL. Aust Dent J. 1994 Apr;39(2):77-81. Clinical evaluation of a highly wear resistant composite. Dickinson GL, Gerbo LR, Leinfelder KF. Am J Dent. 1993 Apr;6(2):85-7. Two-year evaluation in vivo and in vitro of Class 2 composites. Fuks AB, Chosack A, Eidelman E. Oper Dent. 1990 Nov-Dec;15(6):219-23. Cuspal deformation and fracture resistance of teeth with dentin adhesives and composites. Sheth JJ, Fuller JL, Jensen ME. J Prosthet Dent. 1988 Nov;60(5):560-9. 2. 3. 4. 5. 6. 7. 8. 9. 10. 11. 12. 13. 14. 15. 16. 17. 18. 19. 42 A randomized controlled clinical trial of a HEMA-free all-in-one adhesive in non-carious cervical lesions at 1 year. Van Landuyt KL, Peumans M, Fieuws S, De Munck J, Cardoso MV, Ermis RB, Lambrechts P, Van Meerbeek B. J Dent. 2008 Oct;36(10):847-55. In vitro cytotoxicity of different desensitizers under simulated pulpal flow conditions. Wiegand A, Buchholz K, Werner C, Attin T. J Adhes Dent. 2008 Jun;10(3):227-32. Bonding effectiveness and interfacial characterization of a HEMA/TEGDMA-free three-step etch&rinse adhesive. Mine A, De Munck J, Van Landuyt KL, Poitevin A, Kuboki T, Yoshida Y, Suzuki K, Lambrechts P, Van Meerbeek B. J Dent. 2008 Oct;36(10):767-73. Direct dentin bonding technique sensitivity when using air/suction drying steps. Magne P, Mahallati R, Bazos P, So WS. J Esthet Restor Dent. 2008;20(2):130-8 Micropermeability of current self-etching and etch-and-rinse adhesives bonded to deep dentine: a comparison study using a double-staining/confocal microscopy technique. Sauro S, Pashley DH, Mannocci F, Tay FR, Pilecki P, Sherriff M, Watson TF. Eur J Oral Sci. 2008 Apr;116(2):184-93. Marginal integrity: is the clinical performance of bonded restorations predictable in vitro? Frankenberger R, Krämer N, Lohbauer U, Nikolaenko SA, Reich SM. J Adhes Dent. 2007;9 Suppl 1:107-16. Erratum in: J Adhes Dent. 2007 Dec;9(6):546. Bond strength of self-etch adhesives to dentin prepared with three different diamond burs. Ermis RB, De Munck J, Cardoso MV, Coutinho E, Van Landuyt KL, Poitevin A, Lambrechts P, Van Meerbeek B. Dent Mater. 2008 Jul;24(7):978-85. Bonding BisGMA to dentin--a proof of concept for hydrophobic dentin bonding. Tay FR, Pashley DH, Kapur RR, Carrilho MR, Hur YB, Garrett LV, Tay KC. J Dent Res. 2007 Nov;86(11):1034-9. Immediate dentin sealing supports delayed restoration placement. Magne P, So WS, Cascione D. J Prosthet Dent. 2007 Sep;98(3):166-74. Influence of dentin cavity surface finishing on micro-tensile bond strength of adhesives. Cardoso MV, Coutinho E, Ermis RB, Poitevin A, Van Landuyt K, De Munck J, Carvalho RC, Van Meerbeek B. Dent Mater. 2008 Apr;24(4):492-501. Marginal integrity of class V restorations: SEM versus dye penetration. Ernst CP, Galler P, Willershausen B, Haller B. Dent Mater. 2008 Mar;24(3):319-27. Bonding to ground versus unground enamel in fluorosed teeth. Ermis RB, De Munck J, Cardoso MV, Coutinho E, Van Landuyt KL, Poitevin A, Lambrechts P, Van Meerbeek B. Dent Mater. 2007 Oct;23(10):1250-5. Polymerization kinetics of dental adhesives cured with LED: correlation between extent of conversion and permeability. Breschi L, Cadenaro M, Antoniolli F, Sauro S, Biasotto M, Prati C, Tay FR, Di Lenarda R. Dent Mater. 2007 Sep;23(9):1066-72. Restoring cervical lesions with flexible composites. Peumans M, De Munck J, Van Landuyt KL, Kanumilli P, Yoshida Y, Inoue S, Lambrechts P, Van Meerbeek B. Dent Mater. 2007 Jun;23(6):749-54. Effect of water storage on the bonding effectiveness of 6 adhesives to Class I cavity dentin. De Munck J, Shirai K, Yoshida Y, Inoue S, Van Landuyt K, Lambrechts P, Suzuki K, Shintani H, Van Meerbeek B. Oper Dent. 2006 Jul-Aug;31(4):456-65. Immediate dentin sealing of onlay preparations: thickness of pre-cured Dentin Bonding Agent and effect of surface cleaning. Stavridakis MM, Krejci I, Magne P. Oper Dent. 2005 Nov-Dec;30(6):747-57. Degree of conversion and permeability of dental adhesives. Cadenaro M, Antoniolli F, Sauro S, Tay FR, Di Lenarda R, Prati C, Biasotto M, Contardo L, Breschi L. Eur J Oral Sci. 2005 Dec;113(6):525-30. Self-etch vs etch-and-rinse adhesives: effect of thermo-mechanical fatigue loading on marginal quality of bonded resin composite restorations. Frankenberger R, Tay FR. Dent Mater. 2005 May;21(5):397-412. Influence of c-factor and layering technique on microtensile bond strength to dentin. Nikolaenko SA, Lohbauer U, Roggendorf M, Petschelt A, Dasch W, Frankenberger R. Dent Mater. 2004 Jul;20(6):579-85. Your practice is our inspiration.™ All you need is Kerr Authors Biographies in alphabetic order Prof. Martin Jung, DDS Policlinic for Conservative and Preventive Dentistry Faculty of Dentistry, Justus-Liebig University, Giessen, Germany martin.jung@dentist.med.uni-giessen.de Dr. Nick Silikas, BSc, MPhil, PhD, FADM Lecturer in Dental Biomaterials Science University of Manchester, UK nick.silikas@manchester.ac.uk Study of Dentistry at the Justus-Liebig-University, Giessen, Germany, 1979-1984. Approbation for Dentistry, 1984. Scientific Assistant in the Policlinic for Conservative and Preventive Dentistry at the Faculty of Dentistry, Justus-Liebig-University in Giessen, Germany, 1985. Promovation (thesis: “effects of rotary instrumentation on surface of human teeth”) 1989. Assistant Medical Director in the Policlinic for Conservative and Preventive Dentistry, 1992. Habilitation (“Finishing and polishing of indirect ceramic- and composite-inlays in-vitro and in-vivo”) at the Faculty of Dentistry, Justus-Liebig-University, 1999. Professor for Conservative Dentistry, 2005. Specialist for Clinical endodontics, 2006. Main scientific activities: dental materials, surface quality of restorative materials, oral hygiene products, endodontics. Dr. Nick Silikas is currently a Lecturer in Dental Biomaterials Science in the School of Dentistry at The University of Manchester. He was born in Greece but has completed all his Higher Education studies in Manchester where he obtained a BSc (Hons) in Chemistry, an MPhil in Pharmacy, and a PhD in Dental Biomaterials. He is an Editorial Advisor of Dental Materials-Journal for Oral and Craniofacial Biomaterials Sciences [Elsevier Science]. He is a Fellow of the Academy of Dental Materials (FADM) and a member of the International Association of Dental Research (IADR). His research interests lie in surface Imaging & Analysis. His expertises are in characterizing interfaces using several techniques like Atomic Force Microscopy (AFM), X-ray Photoelctron Spectroscopy (XPS), FEG-SEM, Fourier Transform Infra-Red Spectroscopy (FTIR) etc. He is also involved in studying mechanical properties of materials using nanoindentation and traditional mechanical testing (3-point bending, compression, flexure etc.). Prof. Angelo Putignano, MD, DDS Professor of Restorative Dentistry, Head of Endodontic and Operative Dentistry Dept., Dean School of Dental Hygienist Polytechnic University of Marche, Ancona, Italy aputi@tin.it; a.putignano@univpm.it Prof. David Watts, DSc, PhD, FInstP, FRSC, FADM Head of Biomaterials/Biomechanics Research Group University of Manchester, UK david.watts@man.ac.uk M.D. degree and D.D.S. post graduate certificate from the University of Ancona, Italy. Full professor in Restorative Dentistry at School of Dentistry Polytechnic University of Marche, Ancona. Head of the Operative Dentistry and Endodontic department at School of Dentistry Polytechnic University of Marche, Ancona. Dean School of Dental Hygienist Polytechnic University of Marche, Ancona. Active Member of the Italian Society of Operative Dentistry (SIDOC), as well as of the European Academy of Esthetic Dentistry (EAED). Founding Member of the Academy of Minimally Invasive Dentistry (ACAMID). Private practice in Restorative Dentistry, in Ancona. Co-author of the book “Adhesive Dentistry: the Key to success” edited by Quintessence International. Professor David Watts, PhD leads the internationally-reputed Biomaterials/Biomechanics Research Group in the University of Manchester, School of Dentistry, investigating basic hard-tissue structure/properties, biomimetic-composites, new scientific instruments, photon science and developments with dental/orthopaedic industries. He has successfully supervised 40 PhD Theses and has 250+ peer-reviewed research papers. Professor Watts holds Fellowships of the Royal Society of Chemistry, the Institute of Physics and the Academy of Dental Materials and is also Research Professor at Oregon Health and Sciences University, USA. He received a Doctorate of Science from the University of Athens and the 2003 IADR Distinguished Scientist [Souder] Award for research in dental biomaterials. He became Editor-in-Chief of Dental Materials – Journal for Oral and Craniofacial Biomaterials Sciences [Elsevier] in 1998. Since 1986 he has served as UK Principal Expert to International Standards Organization TC 106 (Dentistry), on ceramics, resin-composites and photo-polymerization. I wish to thank sincerely our eminent authors, Prof. Martin Jung, Prof. Angelo Putignano, Dr. Nick Silikas and Prof. David Watts for the valuable support, scientific contribution and guidance to the realization of the Kerr Restorative Clinical Booklet. Heartfelt thanks also to the Kerr Innovation and Product Management Teams for the significant input and collaboration. Manuela Brusoni Clinical Affairs Manager Europe manuela.brusoni@kerrhawe.com 43 © 2009 KerrHawe SA - V.01-06-’09 KerrHawe SA | Via Strecce 4 | P.O.Box 268 | CH-6934 Bioggio | Phone ++41 91 610 05 05 | Fax ++41 91 610 05 14 | www.KerrHawe.com
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