Rock Pile Phase II Environmental Investigation Report

Rock Pile Phase II Environmental Investigation Report

PHASE II
ENVIRONMENTAL
INVESTIGATION
REPORT
Beech Grove Rock Pile Site
Bellefontaine Street and Garstang Street
Beech Grove, Indiana
Schneider Job No. 6892.002
Beech Grove Redevelopment Commission
806 Main Street
Beech Grove, Indiana 46107
Date:
March 28, 2008
Historic Fort Harrison
8901 Otis Avenue
Indianapolis, IN 46216-1037
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March 28, 2008
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Mr. Terry Dilk
Beech Grove Redevelopment Commission
806 Main Street
Beech Grove, Indiana 46107
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Phase II Environmental Investigation
Beech Grove Rock Pile Site
Bellefontaine Street and Garstang Street
Beech Grove, Indiana
Schneider Project No. 6892.002
Dear Mr. Dilk:
In accordance with our proposal dated January 4, 2008, The Schneider
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Corporation (Schneider) recently conducted Phase II environmental sampling
activities at the Rock Pile Site located southwest of the intersection of
Bellefontaine Street and Garstang Street in Beech Grove, Indiana (see
Attachment A for a site vicinity map). The scope of the Phase II sampling
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activities was designed to investigate potential groundwater and soil impacts to
the subject site associated with recognized environmental conditions (RECs)
identified at the site during the completion of a Phase I Environmental Site
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purpose of this letter report is to present the findings of our recent Phase II site
sampling activities.
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Assessment (ESA) for the property (ESA report dated February 11, 2008). The
7
Background Site Information
The subject property, referred to as the Rock Pile Site, is approximately seven
(7) acres in size and is undeveloped with no building structures, though several
large piles of crushed rocks are currently present at the site. The following two
recognized environmental conditions (i.e., evidence of a past, existing, or a
material threat of a future release of hazardous substances or petroleum
products) were identified at the site during the performance of the Phase I
Environmental Site Assessment (ESA) for the site:
)
•
Limited environmental investigation activities were conducted at the study site
in 1992 and 1993 on behalf of former prospective purchasers of the site.
Hydrocarbon contaminated fill material was identified in 1992 during the
completion of geotechnical soil borings at the site. Sampling of the fill material
identified the presence of several polynuclear aromatic hydrocarbons (referred
to as PAHs or by the synonym, PNAs). Subsequent site investigation work
conducted in 1993 reportedly confirmed the presence of PAHs in darkly stained
shallow fill material present at the site.
Up to 1,000 cubic yards of PAH
contaminated fill material was estimated to be present at the study site.
•
Three (3) Leaking Underground Storage Tank (LUST) sites that have reported
soil and groundwater impacts and are actively undergoing investigation and/or
remediation are located within 1/16th mile of the study site. Due to their close
proximity to the study site, it is possible that the groundwater quality of the
study site has been adversely impacted by these sites.
Scope of Phase II Investigation
The scope of the Phase II environmental sampling activities conducted at the study site
consisted of the following:
•
Fourteen (14) soil borings were completed across the study site utilizing a
Geoprobe drilling rig. Each of the borings was completed to the depth of the
uppermost groundwater encountered. Ten (10) of the borings were located
around the perimeter of the study site, while the remaining four (4) borings
were located on the central/eastern portion of the study site (see Attachment B
for a sample location map). One (1) soil sample was collected from each of the
fourteen (14) soil boring locations at varying depth intervals. The depth interval
sampled from each soil boring was determined through the use of a photo
ionization detector (PID), in that the soil depth interval from each boring
resulting in the highest PID total hydrocarbon reading was sampled.
•
Seven (7) samples of the uppermost groundwater at the site were collected
from seven (7) of the fourteen (14) soil borings that were completed as a part of
the soil sampling activities described above (at GP-2, GP-4, GP-6, GP-8, GP10, GP-11, and GP-12) (see Attachment B for sample locations).
The
groundwater samples were collected unfiltered with small diameter bailers from
temporary 1 inch diameter PVC wells that were inserted into the seven (7) soil
boring locations.
•
Borings from eleven (11) additional locations were completed across the site to
a depth of five (5) feet below the ground surface to visually inspect the site for
the presence of darkly stained shallow fill material that was described in
previous site environmental studies. No samples were collected for laboratory
analysis from locations where dark soils were not encountered; these locations
are also illustrated on the sample location figure provided in Attachment B.
•
Each of the fourteen (14) soil samples and seven (7) groundwater samples
collected at the site were submitted under chain-of-custody documentation to
an analytical laboratory (Pace Analytical Services, Inc. of Indianapolis) for the
analysis of volatile organic compounds (VOCs), semi-volatile organic
compounds (SVOCs), polychlorinated biphenyls (PCBs), and RCRA 8 heavy
metals.
The sampling activities described above were conducted at the study site on January 24th,
25th, and 26th, 2008. Results of these sampling activities are discussed below.
Analytical Results
The analytical results from the Phase II sampling activities are summarized in Tables 1 and 2
that are provided in Attachment C. As shown in Table 1, heavy metal compounds were
detected in each of the fourteen (14) site soil samples collected. In four (4) of the site soil
sample locations, one (1) or more organic compounds (i.e., VOCs, SVOCs, and/or PCB
compounds) was also detected (from locations GP-9, GP-10, GP-13, and GP-23).
These
four (4) soil samples were all collected from the eastern portion of the study site. It is noted,
however, that we suspect the lone VOC detection in soil sample GP-13 of acetone, a common
laboratory agent used for cleaning instruments, to be a laboratory artifact rather than
indicative of site conditions. The sample location figure in Attachment B graphically illustrates
the estimated extent of the area with organic impacts in site soils.
As shown in Table 2, heavy metal compounds were detected in each of the seven (7) site
groundwater samples. One (1) organic compound, PCB-1254, was also detected in one (1) of
the groundwater samples (GP-10). The complete analytical laboratory reports for the soil and
groundwater analyses are provided as Attachment D.
For comparative purposes, the tables in Attachment C also include Default Closure Levels
from the Indiana Department of Environmental Management (IDEM) Risk Integrated System
of Closure (RISC) Technical Guide for each of the compounds detected in the site samples. A
sample detection that exceeds one (1) or both of the associated RISC Default Closure Levels
is emphasized with a bold type box in the Attachment C tables. As shown in Table 1, five (5)
compounds detected in site soils exceeded an associated RISC level (arsenic, chromium,
lead, PCB-1254, and benzo(a)pyrene).
Arsenic detections in site soils resulted in an
exceedance of the associated RISC Default Closure Levels for residential and/or industrial
site uses in thirteen (13) of the fourteen (14) soil sample locations. However, the levels of
arsenic detected in site soils, which range from 2.8 milligrams per kilogram (mg/kg) to 9
mg/kg, appear to be in line with typical background levels of arsenic in soil. Lead detections in
site soils resulted in an exceedance of the associated RISC Default Closure Levels in five (5)
of the fourteen (14) soil sample locations (GP-9, GP-10, GP-12, GP-13, and GP-23). These
five (5) soil sample locations are generally located on the eastern portion of the study site.
The chromium detections in site soils that exceeded an associated RISC Default Closure
Level occurred at GP-9 and GP-10; the PCB-1254 detection exceedance occurred at GP-9;
and the benzo(a)pyrene exceedances occurred at GP-9, GP-10, and GP-23.
As shown in Table 2, detections of heavy metal compounds in site groundwater resulted in an
exceedance of an associated RISC Default Closure Level in each of the seven (7) site
groundwater sample locations. The one detection of PCB-1254 at GP-10 also exceeded the
associated RISC Default Closure Levels.
Summary and Conclusions
Phase II environmental sampling activities were conducted at the Rock Pile Site located in
Beech Grove, Indiana on January 24th, 25th, and 26th, 2008 to investigate potential site
impacts to soil and groundwater associated with recognized environmental conditions
previously identified at the site during the completion of a Phase I ESA for the property.
Based on the results of the sampling activities, it appears that impacts to site soils are
generally limited to the eastern portion of the study site. These impacts appear likely to be
associated with fill materials present on this portion of the study site. Five (5) compounds
(arsenic, chromium, lead, PCB-1254, and benzo(a)pyrene) were detected in site soils at
concentrations above one or both of the associated IDEM RISC Default Closure Levels,
though the arsenic soil concentrations appear to be in line with typical soil background
concentrations.
Impacts to the uppermost site groundwater appear to be limited to heavy metal compounds
and one organic compound, PCB-1254.
Concentrations of arsenic, barium, cadmium,
chromium, lead, selenium, and PCB-1254 from groundwater sampling locations across the
study site were found to exceed one or both of the associated RISC Default Closure Levels.
Due to the absence of any detectible levels of VOCs or SVOCs in site groundwater samples, it
appears that the study site groundwater has not been adversely impacted by the nearby
Leaking Underground Storage Tank (LUST) sites that were identified in the Phase I ESA
report.
It has been a pleasure to be of service to you and the Beech Grove Redevelopment
Commission on this project. Please feel free to call us at (317) 826-7292 or (317) 826-7285
respectively, if you have any questions or would like to further discuss the findings of our
Phase II investigation activities.
Sincerely,
Douglas Petroff
Environmental Project Manager
W. Calvin Kelly
Director – Environmental Services and Brownfields Redevelopment
Attachment A
Site Vicinity Map
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Attachment B
Soil and Groundwater Sample Locations Map
LEGEND
GP-21
GP-3
GP-2
GP-X
Soil and groundwater sample
location
GP-Y
Soil sample location
GP-Z
Visual inspection only
GP-22
Estimated extent of organic
compound impacts in soil
GP-4
GP-1
GP-24
GP-19
GP-11
GP-23
GP-5
GP-10
GP-18
GP-13
GP-12
GP-6
GP-7
GP-20
GP-16
GP-17
GP-14
GP-9
GP-25
GP-15
The Schneider Corporation
Historic Fort Harrison
8901 Otis Avenue
Indianapolis, IN 46216
www.schneidercorp.com
866.973.7100
GP-8
Soil Boring Locations with Estimated
Extent of Soil Impacts
Former Rock Pile Site
Beech Grove, Indiana
Schneider Project Number 6892.002
Attachment C
Sample Result Summary Tables
TABLE I
SUMMARY OF SOIL DETECTIONS
Former Rock Pile Site
Bellefontaine Street and Garstang Street
Beech Grove, Indiana
Constituent
Arsenic
Barium
Chromium
Lead
Selenium
Default RISC Level (mg/Kg)
*
PCB-1254
*
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Chrysene
Fluoranthene
Indeno(1,2,3-cd)pyrene
Phenanthrene
Pyrene
Acetone
Naphthalene
Soil (mg/Kg)
Residential
Industrial
GP-1
(12-14)
GP-2
(6-8)
GP-3
(6-8)
GP-4
(2-4)
GP-5
(6-8)
GP-6
(2-4)
GP-7
(6-8)
GP-8
(12-14)
GP-9
(6-8)
GP-10
(2-4)
GP-11
(6-8)
GP-12
(2-4)
GP-13
(2-4)
GP-23
(5-7)
3.9
1,600
38
81
5.2
5.8
10,000
120
230
53
4.8
33.6
7.7
5.8
ND
5.8
54
9.4
8.3
ND
5.5
50.2
9.7
7.6
ND
6.7
52.3
10.6
37.5
2.1
6.8
50.6
13.6
10.7
2.2
9
78.9
16.5
11.2
ND
2.8
59.6
14.9
8.2
ND
4
20.6
9.2
6.2
2.5
5.1
315
97.6
1,160
ND
9
382
149
1,480
3.8
4.5
49
9
7.5
ND
6.7
78.7
17.1
96.7
2.4
5.9
53
15.5
81.8
ND
7.7
52.6
19.8
101
2.1
1.8
18
51
5
0.5
5
-39
25
880
3.1
13
570
28
0.7
5.3
180
51
15
1.5
15
-39
25
880
3.1
170
570
370
170
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
12.7
0.43
0.954
2.09
1.94
2.52
1.3
1.29
2.15
4.4
1.17
1.92
3.63
ND
0.209
1.79
ND
ND
0.544
0.567
0.843
0.38
ND
0.595
1.09
ND
0.636
0.942
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
0.115
ND
ND
ND
0.4
1.02
0.777
0.942
0.44
0.482
1.05
1.69
0.407
0.976
1.31
ND
ND
Notes:
ND = Not Detected
Boxed value exceeds default residential RISC level
Samples Collected January 24, 2008
*PCB and Chromium RISC Level values presented in this table are for Total PCBs and Chromium VI
Dashes (--) indicates a Default RISC Level is not available for this constituent
TABLE 2
SUMMARY OF GROUNDWATER DETECTIONS
Former Rock Pile Site
Bellefontaine Street and Garstang Street
Beech Grove, Indiana
Constituent
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
PCB-1254
Default RISC Level (mg/L)
*
*
Groundwater (mg/L)
Residential
Industrial
GP-2
GP-4
GP-6
GP-8
GP-10
GP-11
GP-12
0.01
2
0.005
0.1
0.015
0.05
0.01
20
0.051
0.31
0.042
0.51
0.16
1.24
0.0132
0.371
0.213
0.0497
0.078
0.86
0.005
0.249
0.114
0.0314
0.0821
0.976
0.0066
0.258
0.112
0.0312
0.519
3.26
0.0295
0.802
0.699
0.161
0.64
8.46
0.0515
1.79
9.6
0.215
0.141
1.08
0.0073
0.269
0.168
0.06
0.166
2.11
0.0101
0.343
0.82
0.0411
0.0005
0.0014
ND
ND
ND
ND
0.0035
ND
ND
Notes:
ND = Not Detected
NA = Not Available
Boxed value exceeds default residential RISC level
Samples Collected January 25 and 26, 2008
All samples were collected unfiltered
*PCB and Chromium RISC Level values presented in this table are for Total PCBs and Chromium VI
Attachment D
Analytical Laboratory Data Reports
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
LIMS USE: FR - DOUG PETROFF
LIMS OBJECT ID: 5011474
February 11, 2008
Mr. Doug Petroff
The Schneider Corporation
8901 Otis Ave
Indianapolis, IN 46216
RE: Project: Beech Grove 6892.002
Pace Project No.: 5011474
Dear Mr. Petroff:
Enclosed are the analytical results for sample(s) received by the laboratory on January 25, 2008.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Donna Spyker
dspyker@pacelabs.com
Project Manager
Illinois/NELAC Certification Number: 100418
Indiana Certification Number: C-49-06
Kansas Certification Number: E-10247
Kentucky Certification Number: 0042
Ohio VAP: CL0065
Pennsylvania: 68-00791
West Virginia Certification Number: 330
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
SAMPLE SUMMARY
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Lab ID
Sample ID
Matrix
Date Collected
Date Received
5011474001
GP-1 (12-14)
Solid
01/24/08 09:00
01/25/08 13:24
5011474002
GP-2(6-8)
Solid
01/24/08 09:30
01/25/08 13:24
5011474003
GP-3(6-8)
Solid
01/24/08 10:00
01/25/08 13:24
5011474004
GP-4(2-4)
Solid
01/24/08 10:20
01/25/08 13:24
5011474005
GP-5(6-8)
Solid
01/24/08 10:45
01/25/08 13:24
5011474006
GP-6(2-4)
Solid
01/24/08 11:00
01/25/08 13:24
5011474007
GP-7(6-8)
Solid
01/24/08 11:30
01/25/08 13:24
5011474008
GP-8(12-14)
Solid
01/24/08 13:00
01/25/08 13:24
5011474009
GP-9(6-8)
Solid
01/24/08 13:30
01/25/08 13:24
5011474010
GP-10(2-4)
Solid
01/24/08 14:00
01/25/08 13:24
5011474011
GP-11(6-8)
Solid
01/24/08 14:30
01/25/08 13:24
5011474012
GP-12(2-4)
Solid
01/24/08 15:30
01/25/08 13:24
5011474013
GP-13(2-4)
Solid
01/24/08 16:00
01/25/08 13:24
5011474014
GP-23(5-7)
Solid
01/24/08 17:30
01/25/08 13:24
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
SAMPLE ANALYTE COUNT
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Lab ID
5011474001
5011474002
5011474003
5011474004
5011474005
5011474006
5011474007
Sample ID
GP-1 (12-14)
GP-2(6-8)
GP-3(6-8)
GP-4(2-4)
GP-5(6-8)
GP-6(2-4)
GP-7(6-8)
Method
Analysts
Analytes
Reported
ASTM D2974-87
ILP
1
EPA 6010
FRW
7
EPA 7471
LLB
1
EPA 8082
SAQ
8
EPA 8260
ALA
73
EPA 8270
KES
66
ASTM D2974-87
ILP
1
EPA 6010
FRW
7
EPA 7471
LLB
1
EPA 8082
SAQ
8
EPA 8260
ALA
73
EPA 8270
KES
66
ASTM D2974-87
ILP
1
EPA 6010
FRW
7
EPA 7471
LLB
1
EPA 8082
SAQ
8
EPA 8260
ALA
73
EPA 8270
KES
66
ASTM D2974-87
ILP
1
EPA 6010
FRW
7
EPA 7471
LLB
1
EPA 8082
SAQ
8
EPA 8260
ALA
73
EPA 8270
KES
66
ASTM D2974-87
ILP
1
EPA 6010
FRW
7
EPA 7471
LLB
1
EPA 8082
SAQ
8
EPA 8260
ALA
73
EPA 8270
KES
66
ASTM D2974-87
ILP
1
EPA 6010
FRW
7
EPA 7471
LLB
1
EPA 8082
SAQ
8
EPA 8260
ALA
73
EPA 8270
KES
66
ASTM D2974-87
ILP
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
SAMPLE ANALYTE COUNT
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Lab ID
5011474008
5011474009
5011474010
5011474011
5011474012
5011474013
Sample ID
GP-8(12-14)
GP-9(6-8)
GP-10(2-4)
GP-11(6-8)
GP-12(2-4)
GP-13(2-4)
Method
Analysts
Analytes
Reported
EPA 6010
FRW
7
EPA 7471
LLB
1
EPA 8082
SAQ
8
EPA 8260
ALA
73
EPA 8270
KES
66
ASTM D2974-87
ILP
1
EPA 6010
FRW
7
EPA 7471
LLB
1
EPA 8082
SAQ
8
EPA 8260
ALA
73
EPA 8270
KES
66
ASTM D2974-87
ILP
1
EPA 6010
FRW
7
EPA 7471
LLB
1
EPA 8082
SAQ
8
EPA 8260
ALA
73
EPA 8270
KES
66
ASTM D2974-87
ILP
1
EPA 6010
FRW
7
EPA 7471
LLB
1
EPA 8082
SAQ
8
EPA 8260
ALA
73
EPA 8270
KES
66
ASTM D2974-87
ILP
1
EPA 6010
FRW
7
EPA 7471
LLB
1
EPA 8082
SAQ
8
EPA 8260
ALA
73
EPA 8270
KES
66
ASTM D2974-87
ILP
1
EPA 6010
FRW
7
EPA 7471
LLB
1
EPA 8082
SAQ
8
EPA 8260
ALA
73
EPA 8270
KES
66
ASTM D2974-87
ILP
1
EPA 6010
FRW
7
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 4 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
SAMPLE ANALYTE COUNT
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Lab ID
Sample ID
Method
EPA 7471
5011474014
GP-23(5-7)
Analysts
LLB
Analytes
Reported
1
EPA 8082
SAQ
8
EPA 8260
ALA
73
EPA 8270
KES
66
ASTM D2974-87
ILP
1
EPA 6010
FRW
7
EPA 7471
LLB
1
EPA 8082
SAQ
8
EPA 8260
ALA
73
EPA 8270
KES
66
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-1 (12-14)
Lab ID: 5011474001
Collected: 01/24/08 09:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
8270 MSSV SHORT LIST
MICROWAVE
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8082 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
70
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
39.7
39.7
39.7
39.7
39.7
39.7
39.7
28-137
1
1
1
1
1
1
1
1
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
02/01/08 13:49
02/01/08 13:49
02/01/08 13:49
02/01/08 13:49
02/01/08 13:49
02/01/08 13:49
02/01/08 13:49
02/01/08 13:49
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
877-09-8
02/01/08 08:52
02/01/08 08:52
02/01/08 08:52
02/01/08 08:52
02/01/08 08:52
02/01/08 08:52
02/01/08 08:52
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
Analytical Method: EPA 6010 Preparation Method: EPA 3050
4.8
33.6
ND
7.7
5.8
ND
ND
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.1
2.1
2.1
2.1
2.1
2.1
2.1
1
1
1
1
1
1
1
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
Analytical Method: EPA 7471 Preparation Method: EPA 7471
ND mg/kg
0.38
1
01/28/08 00:00 01/29/08 16:47 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
375
375
375
375
375
375
375
375
749
375
375
749
749
375
375
375
375
375
375
375
375
375
749
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
91-94-1
Page 6 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-1 (12-14)
Lab ID: 5011474001
Collected: 01/24/08 09:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8270 MSSV SHORT LIST
MICROWAVE
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
79
83
87
77
79
85
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
375
375
375
375
375
1820
1820
375
375
375
375
375
375
375
375
375
375
375
375
375
375
749
375
1820
1820
1820
375
375
1820
375
375
1820
341
375
375
375
375
50-117
56-118
55-118
41-124
35-117
34-122
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
01/31/08 02:35
120-83-2
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
367-12-4
118-79-6
Page 7 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-1 (12-14)
Lab ID: 5011474001
Collected: 01/24/08 09:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
n-Hexane
2-Hexanone
Iodomethane
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
88.6
88.6
88.6
4.4
4.4
4.4
4.4
4.4
4.4
22.1
4.4
4.4
4.4
8.9
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
88.6
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
8.9
4.4
4.4
88.6
88.6
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
110-57-6
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
97-63-2
87-68-3
110-54-3
591-78-6
74-88-4
Page 8 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-1 (12-14)
Lab ID: 5011474001
Collected: 01/24/08 09:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Dibromofluoromethane (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
98
98
101
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
4.4
4.4
17.7
22.1
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
88.6
4.4
8.9
82-130
81-120
65-117
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
01/29/08 14:12
0.10
1
02/01/08 11:29
98-82-8
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
1868-53-7
2037-26-5
460-00-4
Analytical Method: ASTM D2974-87
11.9 %
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-2(6-8)
Lab ID: 5011474002
Collected: 01/24/08 09:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
8270 MSSV SHORT LIST
MICROWAVE
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8082 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
79
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
39.4
39.4
39.4
39.4
39.4
39.4
39.4
28-137
1
1
1
1
1
1
1
1
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
02/01/08 13:58
02/01/08 13:58
02/01/08 13:58
02/01/08 13:58
02/01/08 13:58
02/01/08 13:58
02/01/08 13:58
02/01/08 13:58
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
877-09-8
02/01/08 09:20
02/01/08 09:20
02/01/08 09:20
02/01/08 09:20
02/01/08 09:20
02/01/08 09:20
02/01/08 09:20
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
Analytical Method: EPA 6010 Preparation Method: EPA 3050
5.8
54.0
ND
9.4
8.3
ND
ND
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.2
2.2
2.2
2.2
2.2
2.2
2.2
1
1
1
1
1
1
1
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
Analytical Method: EPA 7471 Preparation Method: EPA 7471
ND mg/kg
0.39
1
01/28/08 00:00 01/29/08 16:51 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
372
372
372
372
372
372
372
372
743
372
372
743
743
372
372
372
372
372
372
372
372
372
743
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
91-94-1
Page 10 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-2(6-8)
Lab ID: 5011474002
Collected: 01/24/08 09:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8270 MSSV SHORT LIST
MICROWAVE
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
83
86
87
82
83
88
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
372
372
372
372
372
1800
1800
372
372
372
372
372
372
372
372
372
372
372
372
372
372
743
372
1800
1800
1800
372
372
1800
372
372
1800
338
372
372
372
372
50-117
56-118
55-118
41-124
35-117
34-122
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
01/31/08 02:14
120-83-2
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
367-12-4
118-79-6
Page 11 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-2(6-8)
Lab ID: 5011474002
Collected: 01/24/08 09:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
n-Hexane
2-Hexanone
Iodomethane
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
84.5
84.5
84.5
4.2
4.2
4.2
4.2
4.2
4.2
21.1
4.2
4.2
4.2
8.5
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
84.5
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
8.5
4.2
4.2
84.5
84.5
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
110-57-6
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
97-63-2
87-68-3
110-54-3
591-78-6
74-88-4
Page 12 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-2(6-8)
Lab ID: 5011474002
Collected: 01/24/08 09:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Dibromofluoromethane (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
105
97
102
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
4.2
4.2
16.9
21.1
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
84.5
4.2
8.5
82-130
81-120
65-117
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
01/29/08 14:51
0.10
1
02/01/08 11:29
98-82-8
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
1868-53-7
2037-26-5
460-00-4
Analytical Method: ASTM D2974-87
11.2 %
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 13 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-3(6-8)
Lab ID: 5011474003
Collected: 01/24/08 10:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
8270 MSSV SHORT LIST
MICROWAVE
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8082 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
78
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
40.6
40.6
40.6
40.6
40.6
40.6
40.6
28-137
1
1
1
1
1
1
1
1
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
02/01/08 14:06
02/01/08 14:06
02/01/08 14:06
02/01/08 14:06
02/01/08 14:06
02/01/08 14:06
02/01/08 14:06
02/01/08 14:06
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
877-09-8
02/01/08 09:26
02/01/08 09:26
02/01/08 09:26
02/01/08 09:26
02/01/08 09:26
02/01/08 09:26
02/01/08 09:26
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
Analytical Method: EPA 6010 Preparation Method: EPA 3050
5.5
50.2
ND
9.7
7.6
ND
ND
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.1
2.1
2.1
2.1
2.1
2.1
2.1
1
1
1
1
1
1
1
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
Analytical Method: EPA 7471 Preparation Method: EPA 7471
ND mg/kg
0.37
1
01/28/08 00:00 01/29/08 16:53 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
382
382
382
382
382
382
382
382
765
382
382
765
765
382
382
382
382
382
382
382
382
382
765
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
91-94-1
Page 14 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-3(6-8)
Lab ID: 5011474003
Collected: 01/24/08 10:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8270 MSSV SHORT LIST
MICROWAVE
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
75
76
80
75
76
82
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
382
382
382
382
382
1850
1850
382
382
382
382
382
382
382
382
382
382
382
382
382
382
765
382
1850
1850
1850
382
382
1850
382
382
1850
348
382
382
382
382
50-117
56-118
55-118
41-124
35-117
34-122
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
01/31/08 02:56
120-83-2
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
367-12-4
118-79-6
Page 15 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-3(6-8)
Lab ID: 5011474003
Collected: 01/24/08 10:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
n-Hexane
2-Hexanone
Iodomethane
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
84.6
84.6
84.6
4.2
4.2
4.2
4.2
4.2
4.2
21.1
4.2
4.2
4.2
8.5
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
84.6
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
8.5
4.2
4.2
84.6
84.6
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
110-57-6
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
97-63-2
87-68-3
110-54-3
591-78-6
74-88-4
Page 16 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-3(6-8)
Lab ID: 5011474003
Collected: 01/24/08 10:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Dibromofluoromethane (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
99
100
103
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
4.2
4.2
16.9
21.1
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
84.6
4.2
8.5
82-130
81-120
65-117
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
01/29/08 15:30
0.10
1
02/01/08 11:34
98-82-8
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
1868-53-7
2037-26-5
460-00-4
Analytical Method: ASTM D2974-87
13.7 %
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 17 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-4(2-4)
Lab ID: 5011474004
Collected: 01/24/08 10:20
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
8270 MSSV SHORT LIST
MICROWAVE
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8082 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
22
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
207
207
207
207
207
207
207
28-137
5
5
5
5
5
5
5
5
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/06/08 14:37
02/06/08 14:37
02/06/08 14:37
02/06/08 14:37
02/06/08 14:37
02/06/08 14:37
02/06/08 14:37
02/06/08 14:37
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
877-09-8
02/01/08 09:31
02/01/08 09:31
02/01/08 09:31
02/01/08 09:31
02/01/08 09:31
02/01/08 09:31
02/01/08 09:31
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
1d
S4
Analytical Method: EPA 6010 Preparation Method: EPA 3050
6.7
52.3
ND
10.6
37.5
2.1
ND
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.2
2.2
2.2
2.2
2.2
2.2
2.2
1
1
1
1
1
1
1
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
Analytical Method: EPA 7471 Preparation Method: EPA 7471
ND mg/kg
0.39
1
01/28/08 00:00 01/29/08 16:54 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
3890
3890
3890
3890
3890
3890
3890
3890
7770
3890
3890
7770
7770
3890
3890
3890
3890
3890
3890
3890
3890
3890
7770
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
91-94-1
Page 18 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-4(2-4)
Lab ID: 5011474004
Collected: 01/24/08 10:20
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8270 MSSV SHORT LIST
MICROWAVE
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
48
44
46
43
45
41
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
3890
3890
3890
3890
3890
18800
18800
3890
3890
3890
3890
3890
3890
3890
3890
3890
3890
3890
3890
3890
3890
7770
3890
18800
18800
18800
3890
3890
18800
3890
3890
18800
3530
3890
3890
3890
3890
50-117
56-118
55-118
41-124
35-117
34-122
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
01/31/08 04:19
120-83-2
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
367-12-4
118-79-6
2d
S4
S4
S4
Page 19 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-4(2-4)
Lab ID: 5011474004
Collected: 01/24/08 10:20
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
n-Hexane
2-Hexanone
Iodomethane
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
90.1
90.1
90.1
4.5
4.5
4.5
4.5
4.5
4.5
22.5
4.5
4.5
4.5
9.0
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
90.1
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
9.0
4.5
4.5
90.1
90.1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
110-57-6
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
97-63-2
87-68-3
110-54-3
591-78-6
74-88-4
Page 20 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-4(2-4)
Lab ID: 5011474004
Collected: 01/24/08 10:20
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Dibromofluoromethane (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
100
99
100
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
4.5
4.5
18.0
22.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
90.1
4.5
9.0
82-130
81-120
65-117
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
01/29/08 16:09
0.10
1
02/01/08 11:35
98-82-8
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
1868-53-7
2037-26-5
460-00-4
Analytical Method: ASTM D2974-87
15.4 %
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 21 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-5(6-8)
Lab ID: 5011474005
Collected: 01/24/08 10:45
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
8270 MSSV SHORT LIST
MICROWAVE
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8082 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
61
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
40.3
40.3
40.3
40.3
40.3
40.3
40.3
28-137
1
1
1
1
1
1
1
1
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/06/08 14:45
02/06/08 14:45
02/06/08 14:45
02/06/08 14:45
02/06/08 14:45
02/06/08 14:45
02/06/08 14:45
02/06/08 14:45
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
877-09-8
02/01/08 09:49
02/01/08 09:49
02/01/08 09:49
02/01/08 09:49
02/01/08 09:49
02/01/08 09:49
02/01/08 09:49
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
Analytical Method: EPA 6010 Preparation Method: EPA 3050
6.8
50.6
ND
13.6
10.7
2.2
ND
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.1
2.1
2.1
2.1
2.1
2.1
2.1
1
1
1
1
1
1
1
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
Analytical Method: EPA 7471 Preparation Method: EPA 7471
ND mg/kg
0.40
1
01/28/08 00:00 01/29/08 16:55 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
380
380
380
380
380
380
380
380
760
380
380
760
760
380
380
380
380
380
380
380
380
380
760
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
91-94-1
Page 22 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-5(6-8)
Lab ID: 5011474005
Collected: 01/24/08 10:45
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8270 MSSV SHORT LIST
MICROWAVE
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
72
77
78
74
75
79
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
380
380
380
380
380
1840
1840
380
380
380
380
380
380
380
380
380
380
380
380
380
380
760
380
1840
1840
1840
380
380
1840
380
380
1840
345
380
380
380
380
50-117
56-118
55-118
41-124
35-117
34-122
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
01/31/08 03:17
120-83-2
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
367-12-4
118-79-6
Page 23 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-5(6-8)
Lab ID: 5011474005
Collected: 01/24/08 10:45
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
n-Hexane
2-Hexanone
Iodomethane
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
98.4
98.4
98.4
4.9
4.9
4.9
4.9
4.9
4.9
24.6
4.9
4.9
4.9
9.8
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
98.4
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
9.8
4.9
4.9
98.4
98.4
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
110-57-6
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
97-63-2
87-68-3
110-54-3
591-78-6
74-88-4
Page 24 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-5(6-8)
Lab ID: 5011474005
Collected: 01/24/08 10:45
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Dibromofluoromethane (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
99
96
99
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
4.9
4.9
19.7
24.6
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
4.9
98.4
4.9
9.8
82-130
81-120
65-117
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
01/29/08 16:48
0.10
1
02/01/08 11:35
98-82-8
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
1868-53-7
2037-26-5
460-00-4
Analytical Method: ASTM D2974-87
13.2 %
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 25 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-6(2-4)
Lab ID: 5011474006
Collected: 01/24/08 11:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
8270 MSSV SHORT LIST
MICROWAVE
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8082 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
57
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
42.0
42.0
42.0
42.0
42.0
42.0
42.0
28-137
1
1
1
1
1
1
1
1
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/06/08 14:53
02/06/08 14:53
02/06/08 14:53
02/06/08 14:53
02/06/08 14:53
02/06/08 14:53
02/06/08 14:53
02/06/08 14:53
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
877-09-8
02/01/08 09:54
02/01/08 09:54
02/01/08 09:54
02/01/08 09:54
02/01/08 09:54
02/01/08 09:54
02/01/08 09:54
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
Analytical Method: EPA 6010 Preparation Method: EPA 3050
9.0
78.9
ND
16.5
11.2
ND
ND
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.2
2.2
2.2
2.2
2.2
2.2
2.2
1
1
1
1
1
1
1
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
Analytical Method: EPA 7471 Preparation Method: EPA 7471
ND mg/kg
0.39
1
01/28/08 00:00 01/29/08 16:57 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
396
396
396
396
396
396
396
396
792
396
396
792
792
396
396
396
396
396
396
396
396
396
792
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
91-94-1
Page 26 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-6(2-4)
Lab ID: 5011474006
Collected: 01/24/08 11:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8270 MSSV SHORT LIST
MICROWAVE
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
71
72
72
69
70
76
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
396
396
396
396
396
1920
1920
396
396
396
396
396
396
396
396
396
396
396
396
396
396
792
396
1920
1920
1920
396
396
1920
396
396
1920
360
396
396
396
396
50-117
56-118
55-118
41-124
35-117
34-122
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
01/30/08 21:22
120-83-2
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
367-12-4
118-79-6
Page 27 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-6(2-4)
Lab ID: 5011474006
Collected: 01/24/08 11:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
n-Hexane
2-Hexanone
Iodomethane
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
87.0
87.0
87.0
4.4
4.4
4.4
4.4
4.4
4.4
21.8
4.4
4.4
4.4
8.7
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
87.0
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
8.7
4.4
4.4
87.0
87.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
110-57-6
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
97-63-2
87-68-3
110-54-3
591-78-6
74-88-4
Page 28 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-6(2-4)
Lab ID: 5011474006
Collected: 01/24/08 11:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Dibromofluoromethane (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
97
100
102
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
4.4
4.4
17.4
21.8
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
87.0
4.4
8.7
82-130
81-120
65-117
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
01/29/08 17:27
0.10
1
02/01/08 11:35
98-82-8
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
1868-53-7
2037-26-5
460-00-4
Analytical Method: ASTM D2974-87
16.6 %
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 29 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-7(6-8)
Lab ID: 5011474007
Collected: 01/24/08 11:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
8270 MSSV SHORT LIST
MICROWAVE
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8082 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
69
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
43.6
43.6
43.6
43.6
43.6
43.6
43.6
28-137
1
1
1
1
1
1
1
1
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/06/08 15:01
02/06/08 15:01
02/06/08 15:01
02/06/08 15:01
02/06/08 15:01
02/06/08 15:01
02/06/08 15:01
02/06/08 15:01
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
877-09-8
02/01/08 10:00
02/01/08 10:00
02/01/08 10:00
02/01/08 10:00
02/01/08 10:00
02/01/08 10:00
02/01/08 10:00
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
Analytical Method: EPA 6010 Preparation Method: EPA 3050
2.8
59.6
ND
14.9
8.2
ND
ND
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.3
2.3
2.3
2.3
2.3
2.3
2.3
1
1
1
1
1
1
1
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
Analytical Method: EPA 7471 Preparation Method: EPA 7471
ND mg/kg
0.43
1
01/28/08 00:00 01/29/08 16:58 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
410
410
410
410
410
410
410
410
820
410
410
820
820
410
410
410
410
410
410
410
410
410
820
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
91-94-1
Page 30 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-7(6-8)
Lab ID: 5011474007
Collected: 01/24/08 11:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8270 MSSV SHORT LIST
MICROWAVE
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
74
76
76
70
73
77
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
410
410
410
410
410
1990
1990
410
410
410
410
410
410
410
410
410
410
410
410
410
410
820
410
1990
1990
1990
410
410
1990
410
410
1990
373
410
410
410
410
50-117
56-118
55-118
41-124
35-117
34-122
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
01/30/08 22:46
120-83-2
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
367-12-4
118-79-6
Page 31 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-7(6-8)
Lab ID: 5011474007
Collected: 01/24/08 11:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
n-Hexane
2-Hexanone
Iodomethane
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
103
103
103
5.2
5.2
5.2
5.2
5.2
5.2
25.8
5.2
5.2
5.2
10.3
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
103
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
10.3
5.2
5.2
103
103
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
110-57-6
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
97-63-2
87-68-3
110-54-3
591-78-6
74-88-4
Page 32 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-7(6-8)
Lab ID: 5011474007
Collected: 01/24/08 11:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Dibromofluoromethane (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
101
96
99
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
5.2
5.2
20.7
25.8
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
5.2
103
5.2
10.3
82-130
81-120
65-117
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
01/29/08 18:07
0.10
1
02/01/08 11:36
98-82-8
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
1868-53-7
2037-26-5
460-00-4
Analytical Method: ASTM D2974-87
19.8 %
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 33 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-8(12-14)
Lab ID: 5011474008
Collected: 01/24/08 13:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
8270 MSSV SHORT LIST
MICROWAVE
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8082 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
63
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
38.5
38.5
38.5
38.5
38.5
38.5
38.5
28-137
1
1
1
1
1
1
1
1
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/06/08 15:09
02/06/08 15:09
02/06/08 15:09
02/06/08 15:09
02/06/08 15:09
02/06/08 15:09
02/06/08 15:09
02/06/08 15:09
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
877-09-8
02/01/08 10:06
02/01/08 10:06
02/01/08 10:06
02/01/08 10:06
02/01/08 10:06
02/01/08 10:06
02/01/08 10:06
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
Analytical Method: EPA 6010 Preparation Method: EPA 3050
4.0
20.6
ND
9.2
6.2
2.5
ND
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.1
2.1
2.1
2.1
2.1
2.1
2.1
1
1
1
1
1
1
1
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
Analytical Method: EPA 7471 Preparation Method: EPA 7471
ND mg/kg
0.35
1
01/28/08 00:00 01/29/08 17:00 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
363
363
363
363
363
363
363
363
726
363
363
726
726
363
363
363
363
363
363
363
363
363
726
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
91-94-1
Page 34 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-8(12-14)
Lab ID: 5011474008
Collected: 01/24/08 13:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8270 MSSV SHORT LIST
MICROWAVE
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
78
79
76
74
78
77
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
363
363
363
363
363
1760
1760
363
363
363
363
363
363
363
363
363
363
363
363
363
363
726
363
1760
1760
1760
363
363
1760
363
363
1760
330
363
363
363
363
50-117
56-118
55-118
41-124
35-117
34-122
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
01/30/08 21:02
120-83-2
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
367-12-4
118-79-6
Page 35 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-8(12-14)
Lab ID: 5011474008
Collected: 01/24/08 13:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
n-Hexane
2-Hexanone
Iodomethane
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
77.5
77.5
77.5
3.9
3.9
3.9
3.9
3.9
3.9
19.4
3.9
3.9
3.9
7.7
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
77.5
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
7.7
3.9
3.9
77.5
77.5
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
110-57-6
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
97-63-2
87-68-3
110-54-3
591-78-6
74-88-4
Page 36 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-8(12-14)
Lab ID: 5011474008
Collected: 01/24/08 13:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Dibromofluoromethane (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
98
99
100
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
3.9
3.9
15.5
19.4
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
3.9
77.5
3.9
7.7
82-130
81-120
65-117
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
01/29/08 18:46
0.10
1
02/01/08 11:36
98-82-8
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
1868-53-7
2037-26-5
460-00-4
Analytical Method: ASTM D2974-87
9.1 %
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 37 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-9(6-8)
Lab ID: 5011474009
Collected: 01/24/08 13:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
8270 MSSV SHORT LIST
MICROWAVE
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8082 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
12700
ND
0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
3900
3900
3900
3900
3900
3900
3900
28-137
100
100
100
100
100
100
100
100
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/06/08 16:44
02/06/08 16:44
02/06/08 16:44
02/06/08 16:44
02/06/08 16:44
02/06/08 16:44
02/06/08 16:44
02/06/08 16:44
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
877-09-8
02/01/08 10:11
02/01/08 10:11
02/01/08 10:11
02/01/08 10:11
02/01/08 10:11
02/01/08 10:11
02/01/08 10:11
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
S4
Analytical Method: EPA 6010 Preparation Method: EPA 3050
5.1
315
ND
97.6
1160
ND
ND
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.1
2.1
2.1
2.1
2.1
2.1
2.1
1
1
1
1
1
1
1
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
Analytical Method: EPA 7471 Preparation Method: EPA 7471
ND mg/kg
0.38
1
01/28/08 00:00 01/29/08 17:01 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
430
954
2090
1940
2520
1300
1290
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
2150
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
367
367
367
367
367
367
367
367
735
367
367
735
735
367
367
367
367
367
367
367
367
367
735
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
91-94-1
Page 38 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-9(6-8)
Lab ID: 5011474009
Collected: 01/24/08 13:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8270 MSSV SHORT LIST
MICROWAVE
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
4400
ND
ND
ND
ND
ND
1170
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1920
ND
3630
ND
ND
71
72
75
71
72
80
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
367
367
367
367
367
1780
1780
367
367
367
367
367
367
367
367
367
367
367
367
367
367
735
367
1780
1780
1780
367
367
1780
367
367
1780
334
367
367
367
367
50-117
56-118
55-118
41-124
35-117
34-122
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
01/31/08 00:29
120-83-2
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
367-12-4
118-79-6
Page 39 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-9(6-8)
Lab ID: 5011474009
Collected: 01/24/08 13:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
n-Hexane
2-Hexanone
Iodomethane
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
84.7
84.7
84.7
4.2
4.2
4.2
4.2
4.2
4.2
21.2
4.2
4.2
4.2
8.5
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
84.7
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
8.5
4.2
4.2
84.7
84.7
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
110-57-6
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
97-63-2
87-68-3
110-54-3
591-78-6
74-88-4
Page 40 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-9(6-8)
Lab ID: 5011474009
Collected: 01/24/08 13:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Dibromofluoromethane (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
209
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
97
100
95
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
4.2
4.2
16.9
21.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
4.2
84.7
4.2
8.5
82-130
81-120
65-117
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
01/29/08 19:25
0.10
1
02/01/08 11:37
98-82-8
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
1868-53-7
2037-26-5
460-00-4
Analytical Method: ASTM D2974-87
10.2 %
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 41 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-10(2-4)
Lab ID: 5011474010
Collected: 01/24/08 14:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
8270 MSSV SHORT LIST
MICROWAVE
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8082 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
1790
ND
0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
803
803
803
803
803
803
803
20-130
20
20
20
20
20
20
20
20
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/08/08 15:30
02/08/08 15:30
02/08/08 15:30
02/08/08 15:30
02/08/08 15:30
02/08/08 15:30
02/08/08 15:30
02/08/08 15:30
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
877-09-8
02/01/08 10:17
02/01/08 10:17
02/01/08 10:17
02/01/08 10:17
02/01/08 10:17
02/01/08 10:17
02/01/08 10:17
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
S4
Analytical Method: EPA 6010 Preparation Method: EPA 3050
9.0
382
ND
149
1480
3.8
ND
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.2
2.2
2.2
2.2
2.2
2.2
2.2
1
1
1
1
1
1
1
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
Analytical Method: EPA 7471 Preparation Method: EPA 7471
ND mg/kg
0.38
1
01/28/08 00:00 01/29/08 17:02 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
544
567
843
380
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
595
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
379
379
379
379
379
379
379
379
757
379
379
757
757
379
379
379
379
379
379
379
379
379
757
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
91-94-1
Page 42 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-10(2-4)
Lab ID: 5011474010
Collected: 01/24/08 14:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8270 MSSV SHORT LIST
MICROWAVE
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1090
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
636
ND
942
ND
ND
71
75
77
69
67
72
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
379
379
379
379
379
1840
1840
379
379
379
379
379
379
379
379
379
379
379
379
379
379
757
379
1840
1840
1840
379
379
1840
379
379
1840
344
379
379
379
379
50-117
56-118
55-118
41-124
35-117
34-122
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
01/31/08 00:09
120-83-2
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
367-12-4
118-79-6
Page 43 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-10(2-4)
Lab ID: 5011474010
Collected: 01/24/08 14:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
n-Hexane
2-Hexanone
Iodomethane
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
95.9
95.9
95.9
4.8
4.8
4.8
4.8
4.8
4.8
24.0
4.8
4.8
4.8
9.6
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
95.9
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
9.6
4.8
4.8
95.9
95.9
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
110-57-6
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
97-63-2
87-68-3
110-54-3
591-78-6
74-88-4
Page 44 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-10(2-4)
Lab ID: 5011474010
Collected: 01/24/08 14:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Dibromofluoromethane (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
98
99
94
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
4.8
4.8
19.2
24.0
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
4.8
95.9
4.8
9.6
82-130
81-120
65-117
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
01/29/08 20:04
0.10
1
02/01/08 11:37
98-82-8
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
1868-53-7
2037-26-5
460-00-4
Analytical Method: ASTM D2974-87
12.8 %
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 45 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-11(6-8)
Lab ID: 5011474011
Collected: 01/24/08 14:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
8270 MSSV SHORT LIST
MICROWAVE
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8082 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
61
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
42.5
42.5
42.5
42.5
42.5
42.5
42.5
28-137
1
1
1
1
1
1
1
1
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/06/08 15:37
02/06/08 15:37
02/06/08 15:37
02/06/08 15:37
02/06/08 15:37
02/06/08 15:37
02/06/08 15:37
02/06/08 15:37
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
877-09-8
02/01/08 10:23
02/01/08 10:23
02/01/08 10:23
02/01/08 10:23
02/01/08 10:23
02/01/08 10:23
02/01/08 10:23
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
Analytical Method: EPA 6010 Preparation Method: EPA 3050
4.5
49.0
ND
9.0
7.5
ND
ND
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.3
2.3
2.3
2.3
2.3
2.3
2.3
1
1
1
1
1
1
1
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
Analytical Method: EPA 7471 Preparation Method: EPA 7471
ND mg/kg
0.40
1
01/28/08 00:00 01/29/08 17:04 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
401
401
401
401
401
401
401
401
801
401
401
801
801
401
401
401
401
401
401
401
401
401
801
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
91-94-1
Page 46 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-11(6-8)
Lab ID: 5011474011
Collected: 01/24/08 14:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8270 MSSV SHORT LIST
MICROWAVE
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
68
71
69
71
71
73
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
401
401
401
401
401
1940
1940
401
401
401
401
401
401
401
401
401
401
401
401
401
401
801
401
1940
1940
1940
401
401
1940
401
401
1940
364
401
401
401
401
50-117
56-118
55-118
41-124
35-117
34-122
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
01/30/08 20:41
120-83-2
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
367-12-4
118-79-6
Page 47 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-11(6-8)
Lab ID: 5011474011
Collected: 01/24/08 14:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
n-Hexane
2-Hexanone
Iodomethane
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
90.4
90.4
90.4
4.5
4.5
4.5
4.5
4.5
4.5
22.6
4.5
4.5
4.5
9.0
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
90.4
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
9.0
4.5
4.5
90.4
90.4
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
110-57-6
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
97-63-2
87-68-3
110-54-3
591-78-6
74-88-4
Page 48 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-11(6-8)
Lab ID: 5011474011
Collected: 01/24/08 14:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Dibromofluoromethane (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
98
98
97
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
4.5
4.5
18.1
22.6
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
90.4
4.5
9.0
82-130
81-120
65-117
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
01/29/08 20:43
0.10
1
02/01/08 11:37
98-82-8
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
1868-53-7
2037-26-5
460-00-4
Analytical Method: ASTM D2974-87
17.6 %
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 49 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-12(2-4)
Lab ID: 5011474012
Collected: 01/24/08 15:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
8270 MSSV SHORT LIST
MICROWAVE
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8082 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
0
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
199
199
199
199
199
199
199
28-137
5
5
5
5
5
5
5
5
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/06/08 15:45
02/06/08 15:45
02/06/08 15:45
02/06/08 15:45
02/06/08 15:45
02/06/08 15:45
02/06/08 15:45
02/06/08 15:45
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
877-09-8
02/01/08 10:28
02/01/08 10:28
02/01/08 10:28
02/01/08 10:28
02/01/08 10:28
02/01/08 10:28
02/01/08 10:28
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
3d
S4
Analytical Method: EPA 6010 Preparation Method: EPA 3050
6.7
78.7
ND
17.1
96.7
2.4
ND
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.2
2.2
2.2
2.2
2.2
2.2
2.2
1
1
1
1
1
1
1
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
Analytical Method: EPA 7471 Preparation Method: EPA 7471
ND mg/kg
0.37
1
01/28/08 00:00 01/29/08 17:08 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
3750
3750
3750
3750
3750
3750
3750
3750
7500
3750
3750
7500
7500
3750
3750
3750
3750
3750
3750
3750
3750
3750
7500
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
91-94-1
Page 50 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-12(2-4)
Lab ID: 5011474012
Collected: 01/24/08 15:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8270 MSSV SHORT LIST
MICROWAVE
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
76
83
83
79
77
77
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
3750
3750
3750
3750
3750
18200
18200
3750
3750
3750
3750
3750
3750
3750
3750
3750
3750
3750
3750
3750
3750
7500
3750
18200
18200
18200
3750
3750
18200
3750
3750
18200
3410
3750
3750
3750
3750
50-117
56-118
55-118
41-124
35-117
34-122
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
10
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
01/31/08 01:53
120-83-2
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
367-12-4
118-79-6
4d
Page 51 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-12(2-4)
Lab ID: 5011474012
Collected: 01/24/08 15:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
n-Hexane
2-Hexanone
Iodomethane
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
89.7
89.7
89.7
4.5
4.5
4.5
4.5
4.5
4.5
22.4
4.5
4.5
4.5
9.0
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
89.7
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
9.0
4.5
4.5
89.7
89.7
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
110-57-6
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
97-63-2
87-68-3
110-54-3
591-78-6
74-88-4
Page 52 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-12(2-4)
Lab ID: 5011474012
Collected: 01/24/08 15:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Dibromofluoromethane (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
98
97
96
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
4.5
4.5
17.9
22.4
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
4.5
89.7
4.5
9.0
82-130
81-120
65-117
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
01/29/08 21:22
0.10
1
02/01/08 11:37
98-82-8
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
1868-53-7
2037-26-5
460-00-4
Analytical Method: ASTM D2974-87
12.0 %
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 53 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-13(2-4)
Lab ID: 5011474013
Collected: 01/24/08 16:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
8270 MSSV SHORT LIST
MICROWAVE
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8082 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
65
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
41.7
41.7
41.7
41.7
41.7
41.7
41.7
28-137
1
1
1
1
1
1
1
1
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/07/08 13:25
02/07/08 13:25
02/07/08 13:25
02/07/08 13:25
02/07/08 13:25
02/07/08 13:25
02/07/08 13:25
02/07/08 13:25
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
877-09-8
02/01/08 10:34
02/01/08 10:34
02/01/08 10:34
02/01/08 10:34
02/01/08 10:34
02/01/08 10:34
02/01/08 10:34
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
Analytical Method: EPA 6010 Preparation Method: EPA 3050
5.9
53.0
ND
15.5
81.8
ND
ND
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.2
2.2
2.2
2.2
2.2
2.2
2.2
1
1
1
1
1
1
1
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
Analytical Method: EPA 7471 Preparation Method: EPA 7471
ND mg/kg
0.40
1
01/28/08 00:00 01/29/08 16:23 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
393
393
393
393
393
393
393
393
786
393
393
786
786
393
393
393
393
393
393
393
393
393
786
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
91-94-1
Page 54 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-13(2-4)
Lab ID: 5011474013
Collected: 01/24/08 16:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8270 MSSV SHORT LIST
MICROWAVE
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
69
70
73
68
69
72
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
393
393
393
393
393
1900
1900
393
393
393
393
393
393
393
393
393
393
393
393
393
393
786
393
1900
1900
1900
393
393
1900
393
393
1900
357
393
393
393
393
50-117
56-118
55-118
41-124
35-117
34-122
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
01/30/08 23:27
120-83-2
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
367-12-4
118-79-6
Page 55 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-13(2-4)
Lab ID: 5011474013
Collected: 01/24/08 16:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
n-Hexane
2-Hexanone
Iodomethane
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
115
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
87.7
87.7
87.7
4.4
4.4
4.4
4.4
4.4
4.4
21.9
4.4
4.4
4.4
8.8
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
87.7
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
8.8
4.4
4.4
87.7
87.7
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
110-57-6
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
97-63-2
87-68-3
110-54-3
591-78-6
74-88-4
Page 56 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-13(2-4)
Lab ID: 5011474013
Collected: 01/24/08 16:00
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Dibromofluoromethane (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
97
98
96
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
4.4
4.4
17.5
21.9
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
4.4
87.7
4.4
8.8
82-130
81-120
65-117
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
01/29/08 21:41
0.10
1
02/01/08 11:38
98-82-8
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
1868-53-7
2037-26-5
460-00-4
Analytical Method: ASTM D2974-87
16.0 %
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 57 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-23(5-7)
Lab ID: 5011474014
Collected: 01/24/08 17:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7471 Mercury
Mercury
8270 MSSV SHORT LIST
MICROWAVE
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8082 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
57
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
39.3
39.3
39.3
39.3
39.3
39.3
39.3
20-130
1
1
1
1
1
1
1
1
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/05/08 00:00
02/08/08 09:40
02/08/08 09:40
02/08/08 09:40
02/08/08 09:40
02/08/08 09:40
02/08/08 09:40
02/08/08 09:40
02/08/08 09:40
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
877-09-8
02/01/08 10:40
02/01/08 10:40
02/01/08 10:40
02/01/08 10:40
02/01/08 10:40
02/01/08 10:40
02/01/08 10:40
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
Analytical Method: EPA 6010 Preparation Method: EPA 3050
7.7
52.6
ND
19.8
101
2.1
ND
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.2
2.2
2.2
2.2
2.2
2.2
2.2
1
1
1
1
1
1
1
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
01/31/08 00:00
Analytical Method: EPA 7471 Preparation Method: EPA 7471
ND mg/kg
0.36
1
01/28/08 00:00 01/29/08 16:25 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
400
1020
777
942
440
482
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1050
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
371
371
371
371
371
371
371
371
742
371
371
742
742
371
371
371
371
371
371
371
371
371
742
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
91-94-1
Page 58 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-23(5-7)
Lab ID: 5011474014
Collected: 01/24/08 17:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8270 MSSV SHORT LIST
MICROWAVE
2,4-Dichlorophenol
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3546
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
1690
ND
ND
ND
ND
ND
407
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
976
ND
1310
ND
ND
66
82
77
70
77
77
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
371
371
371
371
371
1800
1800
371
371
371
371
371
371
371
371
371
371
371
371
371
371
742
371
1800
1800
1800
371
371
1800
371
371
1800
337
371
371
371
371
50-117
56-118
55-118
41-124
35-117
34-122
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
02/01/08 20:55
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
02/04/08 14:24
120-83-2
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
367-12-4
118-79-6
Page 59 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-23(5-7)
Lab ID: 5011474014
Collected: 01/24/08 17:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
n-Hexane
2-Hexanone
Iodomethane
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
91.8
91.8
91.8
4.6
4.6
4.6
4.6
4.6
4.6
23.0
4.6
4.6
4.6
9.2
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
91.8
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
9.2
4.6
4.6
91.8
91.8
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
67-64-1
107-02-8
107-13-1
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
110-57-6
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
97-63-2
87-68-3
110-54-3
591-78-6
74-88-4
Page 60 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
Sample: GP-23(5-7)
Lab ID: 5011474014
Collected: 01/24/08 17:30
Received: 01/25/08 13:24
Matrix: Solid
Results reported on a "dry-weight" basis
Parameters
8260 MSV 5035A VOA
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Dibromofluoromethane (S)
Toluene-d8 (S)
4-Bromofluorobenzene (S)
Percent Moisture
Percent Moisture
Date: 02/11/2008 03:29 PM
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
97
97
99
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
4.6
4.6
18.4
23.0
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
4.6
91.8
4.6
9.2
82-130
81-120
65-117
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
01/30/08 00:55
0.10
1
02/01/08 11:39
98-82-8
99-87-6
75-09-2
108-10-1
1634-04-4
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
1868-53-7
2037-26-5
460-00-4
Analytical Method: ASTM D2974-87
11.0 %
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 61 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
QC Batch:
MERP/1508
Analysis Method:
EPA 7471
QC Batch Method:
EPA 7471
Analysis Description:
7471 Mercury
Associated Lab Samples:
METHOD BLANK:
5011474013, 5011474014
126575
Associated Lab Samples:
5011474013, 5011474014
Parameter
Mercury
mg/kg
LABORATORY CONTROL SAMPLE:
126576
Parameter
Mercury
Blank
Result
Units
ND
Spike
Conc.
Units
mg/kg
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
Parameter
Mercury
Date: 02/11/2008 03:29 PM
Units
mg/kg
Reporting
Limit
0.33
LCS
Result
.5
ND
LCS
% Rec
0.51
126577
5011473001
Result
Qualifiers
% Rec
Limits
101
Qualifiers
80-120
126578
MS
Spike
Conc.
.62
MSD
Spike
Conc.
.62
MS
Result
0.72
MSD
Result
MS
% Rec
0.66
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
110
MSD
% Rec
101
% Rec
Limits
75-125
Max
RPD RPD
8
Qual
20
Page 62 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
QC Batch:
MERP/1509
Analysis Method:
EPA 7471
QC Batch Method:
EPA 7471
Analysis Description:
7471 Mercury
Associated Lab Samples:
METHOD BLANK:
5011474001, 5011474002, 5011474003, 5011474004, 5011474005, 5011474006, 5011474007, 5011474008,
5011474009, 5011474010, 5011474011, 5011474012
126579
Associated Lab Samples:
Parameter
5011474001, 5011474002, 5011474003, 5011474004, 5011474005, 5011474006, 5011474007, 5011474008,
5011474009, 5011474010, 5011474011, 5011474012
Blank
Reporting
Units
Result
Limit
Qualifiers
Mercury
mg/kg
LABORATORY CONTROL SAMPLE:
126580
Parameter
Mercury
ND
mg/kg
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
Parameter
Mercury
Date: 02/11/2008 03:29 PM
Units
mg/kg
LCS
Result
Spike
Conc.
Units
0.33
.5
0.50
126581
5011471001
Result
ND
% Rec
Limits
LCS
% Rec
101
Qualifiers
80-120
126582
MS
Spike
Conc.
.53
MSD
Spike
Conc.
.53
MS
Result
0.53
MSD
Result
MS
% Rec
0.53
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
101
MSD
% Rec
100
% Rec
Limits
75-125
Max
RPD RPD
1
Qual
20
Page 63 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
QC Batch:
OEXT/5896
Analysis Method:
EPA 8270
QC Batch Method:
EPA 3546
Analysis Description:
8270 Solid MSSV Microwave Short Spike
Associated Lab Samples:
METHOD BLANK:
5011474006, 5011474007, 5011474008, 5011474009, 5011474010, 5011474011, 5011474012, 5011474013
126796
Associated Lab Samples:
Parameter
5011474006, 5011474007, 5011474008, 5011474009, 5011474010, 5011474011, 5011474012, 5011474013
Blank
Reporting
Units
Result
Limit
Qualifiers
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
2-Nitroaniline
2-Nitrophenol
3&4-Methylphenol(m&p Cresol)
3,3'-Dichlorobenzidine
3-Nitroaniline
4,6-Dinitro-2-methylphenol
4-Bromophenylphenyl ether
4-Chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenylphenyl ether
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
bis(2-Ethylhexyl)phthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenz(a,h)anthracene
Dibenzofuran
Diethylphthalate
Date: 02/11/2008 03:29 PM
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
330
330
330
330
1600
330
330
330
330
330
330
1600
330
660
660
1600
1600
330
660
660
330
1600
1600
330
330
330
330
330
330
330
330
660
330
330
330
330
330
330
330 J
330
330
330
330
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 64 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
METHOD BLANK:
126796
Associated Lab Samples:
Parameter
5011474006, 5011474007, 5011474008, 5011474009, 5011474010, 5011474011, 5011474012, 5011474013
Blank
Reporting
Units
Result
Limit
Qualifiers
Dimethylphthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
LABORATORY CONTROL SAMPLE:
126797
Parameter
2,4-Dinitrotoluene
2-Chlorophenol
4-Chloro-3-methylphenol
4-Nitrophenol
Acenaphthene
N-Nitroso-di-n-propylamine
Pentachlorophenol
Phenol
Pyrene
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
Date: 02/11/2008 03:29 PM
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
73
79
77
73
72
77
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
Spike
Conc.
3330
3330
3330
3330
3330
3330
3330
3330
3330
330
330
330
330
330
330
330
330
330
330
330
330
330
1600
300
330
330
34-122
56-118
35-117
50-117
41-124
55-118
LCS
Result
2750
2730
2640
2880
2870
2640
2310
2830
2850
% Rec
Limits
LCS
% Rec
82
82
79
86
86
79
69
85
85
79
82
81
78
81
82
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
54-124
56-111
61-115
42-122
57-113
52-128
24-132
54-117
51-119
34-122
56-118
35-117
50-117
41-124
55-118
Page 65 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
Parameter
2,4-Dinitrotoluene
2-Chlorophenol
4-Chloro-3-methylphenol
4-Nitrophenol
Acenaphthene
N-Nitroso-di-n-propylamine
Pentachlorophenol
Phenol
Pyrene
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
Date: 02/11/2008 03:29 PM
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
126809
5011538002
Result
ND
ND
ND
ND
ND
ND
ND
ND
563
126810
MS
Spike
Conc.
4370
4370
4370
4370
4370
4370
4370
4370
4370
MSD
Spike
Conc.
4370
4370
4370
4370
4370
4370
4370
4370
4370
MS
Result
4940
5320
4620
5280
5890
5680
3470
5160
5170
MSD
Result
MS
% Rec
3120
2930
2630
3200
3480
3380
2000J
2930
5360
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
113
122
106
121
135
130
79
118
105
53
67
62
62
55
51
MSD
% Rec
71
67
60
73
80
77
46
67
110
68
75
68
67
70
68
% Rec
Limits
57-121
35-125
55-120
27-130
55-114
40-133
10-135
36-130
51-121
34-122
56-118
35-117
50-117
41-124
55-118
Max
RPD RPD
45
58
55
49
51
51
55
4
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Qual
R1
R1
R1
R1
M0,R1
R1
R1
R1
R1
R1,S0
Page 66 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
QC Batch:
OEXT/5909
Analysis Method:
EPA 8270
QC Batch Method:
EPA 3546
Analysis Description:
8270 Solid MSSV Microwave Short Spike
Associated Lab Samples:
METHOD BLANK:
5011474001, 5011474002, 5011474003, 5011474004, 5011474005
127147
Associated Lab Samples:
Parameter
5011474001, 5011474002, 5011474003, 5011474004, 5011474005
Blank
Reporting
Units
Result
Limit
Qualifiers
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
2-Nitroaniline
2-Nitrophenol
3&4-Methylphenol(m&p Cresol)
3,3'-Dichlorobenzidine
3-Nitroaniline
4,6-Dinitro-2-methylphenol
4-Bromophenylphenyl ether
4-Chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenylphenyl ether
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
bis(2-Ethylhexyl)phthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenz(a,h)anthracene
Dibenzofuran
Diethylphthalate
Date: 02/11/2008 03:29 PM
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
330
330
330
330
1600
330
330
330
330
330
330
1600
330
660
660
1600
1600
330
660
660
330
1600
1600
330
330
330
330
330
330
330
330
660
330
330
330
330
330
330
330 J
330
330
330
330
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 67 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
METHOD BLANK:
127147
Associated Lab Samples:
Parameter
5011474001, 5011474002, 5011474003, 5011474004, 5011474005
Blank
Reporting
Units
Result
Limit
Qualifiers
Dimethylphthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
LABORATORY CONTROL SAMPLE:
127148
Parameter
2,4-Dinitrotoluene
2-Chlorophenol
4-Chloro-3-methylphenol
4-Nitrophenol
Acenaphthene
N-Nitroso-di-n-propylamine
Pentachlorophenol
Phenol
Pyrene
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
Date: 02/11/2008 03:29 PM
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
83
83
84
80
84
87
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
Spike
Conc.
3330
3330
3330
3330
3330
3330
3330
3330
3330
330
330
330
330
330
330
330
330
330
330
330
330
330
1600
300
330
330
34-122
56-118
35-117
50-117
41-124
55-118
LCS
Result
2670
2540
2370
2710
2640
2650
2490
2600
2840
% Rec
Limits
LCS
% Rec
80
76
71
81
79
80
75
78
85
80
79
76
74
77
82
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
54-124
56-111
61-115
42-122
57-113
52-128
24-132
54-117
51-119
34-122
56-118
35-117
50-117
41-124
55-118
Page 68 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
Parameter
2,4-Dinitrotoluene
2-Chlorophenol
4-Chloro-3-methylphenol
4-Nitrophenol
Acenaphthene
N-Nitroso-di-n-propylamine
Pentachlorophenol
Phenol
Pyrene
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
Date: 02/11/2008 03:29 PM
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
127149
5011565001
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
127150
MS
Spike
Conc.
3960
3960
3960
3960
3960
3960
3960
3960
3960
MSD
Spike
Conc.
3960
3960
3960
3960
3960
3960
3960
3960
3960
MS
Result
2500
2440
2320
2650
2470
2530
2200
2470
2510
MSD
Result
MS
% Rec
2290
2460
2240
2430
2520
2700
2130
2580
2380
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
63
62
58
67
62
64
56
62
63
64
66
68
62
64
68
MSD
% Rec
58
62
56
61
63
68
54
65
60
60
63
68
64
62
60
% Rec
Limits
57-121
35-125
55-120
27-130
55-114
40-133
10-135
36-130
51-121
34-122
56-118
35-117
50-117
41-124
55-118
Max
RPD RPD
9
1
3
9
2
6
3
4
5
Qual
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Page 69 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
QC Batch:
MSV/7190
Analysis Method:
EPA 8260
QC Batch Method:
EPA 8260
Analysis Description:
8260 MSV 5035A Volatile Organics
Associated Lab Samples:
METHOD BLANK:
5011474001, 5011474002, 5011474003, 5011474004, 5011474005, 5011474006, 5011474007, 5011474008,
5011474009, 5011474010, 5011474011, 5011474012
127302
Associated Lab Samples:
Parameter
5011474001, 5011474002, 5011474003, 5011474004, 5011474005, 5011474006, 5011474007, 5011474008,
5011474009, 5011474010, 5011474011, 5011474012
Blank
Reporting
Units
Result
Limit
Qualifiers
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
Date: 02/11/2008 03:29 PM
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
25.0
5.0
100
5.0
25.0
100
100
100
5.0
5.0
5.0
5.0
5.0
5.0
10.0
5.0
5.0
5.0
5.0
5.0
5.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 70 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
METHOD BLANK:
127302
Associated Lab Samples:
Parameter
5011474001, 5011474002, 5011474003, 5011474004, 5011474005, 5011474006, 5011474007, 5011474008,
5011474009, 5011474010, 5011474011, 5011474012
Blank
Reporting
Units
Result
Limit
Qualifiers
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Ethyl methacrylate
Ethylbenzene
Hexachloro-1,3-butadiene
Iodomethane
Isopropylbenzene (Cumene)
Methyl-tert-butyl ether
Methylene chloride
n-Butylbenzene
n-Hexane
n-Propylbenzene
Naphthalene
p-Isopropyltoluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
trans-1,4-Dichloro-2-butene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Xylene (Total)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Toluene-d8 (S)
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
LABORATORY CONTROL SAMPLE:
127303
Parameter
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
Date: 02/11/2008 03:29 PM
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
98
100
99
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Spike
Conc.
50
50
50
50
50
50
50
50
5.0
5.0
5.0
5.0
10.0
5.0
5.0
100
5.0
5.0
20.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
100
5.0
5.0
100
5.0
10.0
65-117
82-130
81-120
LCS
Result
LCS
% Rec
43.8
48.6
55.9
55.2
48.7
51.9
48.7
47.1
% Rec
Limits
88
97
112
110
97
104
97
94
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
69-124
67-129
68-130
72-129
68-128
65-138
71-126
63-130
Page 71 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
LABORATORY CONTROL SAMPLE:
127303
Parameter
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Ethyl methacrylate
Ethylbenzene
Hexachloro-1,3-butadiene
Iodomethane
Isopropylbenzene (Cumene)
Methyl-tert-butyl ether
Methylene chloride
n-Butylbenzene
n-Hexane
n-Propylbenzene
Naphthalene
Date: 02/11/2008 03:29 PM
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Spike
Conc.
50
50
50
50
50
50
50
50
50
50
50
50
250
50
250
50
250
250
1000
1000
50
50
50
50
50
50
100
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
100
50
50
50
50
50
LCS
Result
51.6
40.8
45.3
50.5
44.9
52.0
51.7
45.1
44.4
53.2
47.2
41.5
286
46.4
297
43.5
275
280
3600
1120
49.2
48.1
57.1
45.8
38.0
56.9
97.1
41.6
45.6
58.3
48.4
47.6
51.4
41.4
41.5
52.8
41.7
56.0
46.8
44.3
96.8J
43.2
111
52.5
42.9
54.0
46.7
52.2
LCS
% Rec
% Rec
Limits
103
82
91
101
90
104
103
90
89
106
94
83
114
93
119
87
110
112
360
112
98
96
114
92
76
114
97
83
91
117
97
95
103
83
83
106
83
112
94
89
97
86
111
105
86
108
93
104
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
52-131
59-132
72-129
71-126
72-128
63-130
73-124
72-132
73-130
71-127
71-125
61-134
59-150
73-135
46-150
72-130
54-146
41-150
50-150 L0
50-150
72-129
72-127
63-144
71-128
62-124
45-144
63-171
59-130
73-125
60-140
67-127
38-141
76-132
61-114
70-131
75-132
50-179
50-150
77-131
70-133
70-130
72-128
66-139
48-121
68-132
70-130
74-136
60-131
Page 72 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
LABORATORY CONTROL SAMPLE:
127303
Parameter
p-Isopropyltoluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
trans-1,4-Dichloro-2-butene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Xylene (Total)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Toluene-d8 (S)
Date: 02/11/2008 03:29 PM
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
Spike
Conc.
50
50
50
50
50
50
50
50
50
50
50
200
50
150
LCS
Result
37.0
46.7
44.9
37.0
43.7
49.7
50.1
41.2
39.9J
50.7
44.2
181
41.7
134
LCS
% Rec
% Rec
Limits
74
93
90
74
87
99
100
82
80
101
88
91
83
89
101
101
100
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
69-134
74-135
75-125
69-124
55-123
75-127
71-131
62-114
50-150
72-123
62-150
50-150
54-136
70-130
65-117
82-130
81-120
Page 73 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
QC Batch:
MSV/7193
Analysis Method:
EPA 8260
QC Batch Method:
EPA 8260
Analysis Description:
8260 MSV 5035A Volatile Organics
Associated Lab Samples:
METHOD BLANK:
5011474013
127310
Associated Lab Samples:
5011474013
Parameter
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Date: 02/11/2008 03:29 PM
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Blank
Result
Reporting
Limit
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Qualifiers
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
25.0
5.0
100
5.0
25.0
100
100
100
5.0
5.0
5.0
5.0
5.0
5.0
10.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 74 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
METHOD BLANK:
127310
Associated Lab Samples:
5011474013
Parameter
Units
Dibromomethane
Dichlorodifluoromethane
Ethyl methacrylate
Ethylbenzene
Hexachloro-1,3-butadiene
Iodomethane
Isopropylbenzene (Cumene)
Methyl-tert-butyl ether
Methylene chloride
n-Butylbenzene
n-Hexane
n-Propylbenzene
Naphthalene
p-Isopropyltoluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
trans-1,4-Dichloro-2-butene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Xylene (Total)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Toluene-d8 (S)
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
LABORATORY CONTROL SAMPLE:
127311
Parameter
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
Date: 02/11/2008 03:29 PM
Reporting
Limit
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
98
99
99
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Blank
Result
Spike
Conc.
50
50
50
50
50
50
50
50
50
50
50
Qualifiers
5.0
5.0
10.0
5.0
5.0
100
5.0
5.0
20.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
100
5.0
5.0
100
5.0
10.0
65-117
82-130
81-120
LCS
Result
LCS
% Rec
41.3
47.3
50.9
55.0
50.6
53.1
51.0
48.2
48.5
44.4
43.8
% Rec
Limits
83
95
102
110
101
106
102
96
97
89
88
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
69-124
67-129
68-130
72-129
68-128
65-138
71-126
63-130
52-131
59-132
72-129
Page 75 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
LABORATORY CONTROL SAMPLE:
127311
Parameter
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Ethyl methacrylate
Ethylbenzene
Hexachloro-1,3-butadiene
Iodomethane
Isopropylbenzene (Cumene)
Methyl-tert-butyl ether
Methylene chloride
n-Butylbenzene
n-Hexane
n-Propylbenzene
Naphthalene
p-Isopropyltoluene
sec-Butylbenzene
Styrene
Date: 02/11/2008 03:29 PM
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Spike
Conc.
50
50
50
50
50
50
50
50
50
250
50
250
50
250
250
1000
1000
50
50
50
50
50
50
100
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
100
50
50
50
50
50
50
50
50
LCS
Result
51.1
46.6
52.7
53.3
44.1
44.4
52.8
45.4
42.1
292
46.1
283
43.6
265
286
3700
1150
50.1
49.0
53.8
44.6
37.3
49.4
101
41.0
46.5
38.2
49.5
42.5
52.2
39.2
39.5
54.8
41.6
50.9
47.3
43.1
93.1J
45.2
114
50.4
42.2
52.7
46.2
51.6
42.1
45.6
44.1
LCS
% Rec
% Rec
Limits
102
93
105
107
88
89
106
91
84
117
92
113
87
106
114
370
115
100
98
108
89
75
99
101
82
93
76
99
85
104
78
79
110
83
102
95
86
93
90
114
101
84
105
92
103
84
91
88
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
71-126
72-128
63-130
73-124
72-132
73-130
71-127
71-125
61-134
59-150
73-135
46-150
72-130
54-146
41-150
50-150 L0
50-150
72-129
72-127
63-144
71-128
62-124
45-144
63-171
59-130
73-125
60-140
67-127
38-141
76-132
61-114
70-131
75-132
50-179
50-150
77-131
70-133
70-130
72-128
66-139
48-121
68-132
70-130
74-136
60-131
69-134
74-135
75-125
Page 76 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
LABORATORY CONTROL SAMPLE:
127311
Parameter
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
trans-1,4-Dichloro-2-butene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Xylene (Total)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Toluene-d8 (S)
Date: 02/11/2008 03:29 PM
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
Spike
Conc.
50
50
50
50
50
50
50
50
200
50
150
LCS
Result
38.7
42.7
47.9
51.0
38.8
41.7J
50.9
42.8
173
42.4
136
LCS
% Rec
% Rec
Limits
77
85
96
102
78
83
102
86
87
85
90
103
101
99
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
69-124
55-123
75-127
71-131
62-114
50-150
72-123
62-150
50-150
54-136
70-130
65-117
82-130
81-120
Page 77 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
QC Batch:
MSV/7194
Analysis Method:
EPA 8260
QC Batch Method:
EPA 8260
Analysis Description:
8260 MSV 5035A Volatile Organics
Associated Lab Samples:
METHOD BLANK:
5011474014
127312
Associated Lab Samples:
5011474014
Parameter
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Date: 02/11/2008 03:29 PM
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Blank
Result
Reporting
Limit
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Qualifiers
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
25.0
5.0
100
5.0
25.0
100
100
100
5.0
5.0
5.0
5.0
5.0
5.0
10.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 78 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
METHOD BLANK:
127312
Associated Lab Samples:
5011474014
Parameter
Units
Dibromomethane
Dichlorodifluoromethane
Ethyl methacrylate
Ethylbenzene
Hexachloro-1,3-butadiene
Iodomethane
Isopropylbenzene (Cumene)
Methyl-tert-butyl ether
Methylene chloride
n-Butylbenzene
n-Hexane
n-Propylbenzene
Naphthalene
p-Isopropyltoluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
trans-1,4-Dichloro-2-butene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Xylene (Total)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Toluene-d8 (S)
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
LABORATORY CONTROL SAMPLE:
127313
Parameter
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
Date: 02/11/2008 03:29 PM
Reporting
Limit
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
99
97
99
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Blank
Result
Spike
Conc.
50
50
50
50
50
50
50
50
50
50
50
Qualifiers
5.0
5.0
10.0
5.0
5.0
100
5.0
5.0
20.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
100
5.0
5.0
100
5.0
10.0
65-117
82-130
81-120
LCS
Result
LCS
% Rec
35.3
41.8
50.8
49.9
48.1
50.2
49.2
48.0
49.0
45.1
44.7
% Rec
Limits
71
84
102
100
96
100
98
96
98
90
89
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
69-124
67-129
68-130
72-129
68-128
65-138
71-126
63-130
52-131
59-132
72-129
Page 79 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
LABORATORY CONTROL SAMPLE:
127313
Parameter
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Ethyl methacrylate
Ethylbenzene
Hexachloro-1,3-butadiene
Iodomethane
Isopropylbenzene (Cumene)
Methyl-tert-butyl ether
Methylene chloride
n-Butylbenzene
n-Hexane
n-Propylbenzene
Naphthalene
p-Isopropyltoluene
sec-Butylbenzene
Styrene
Date: 02/11/2008 03:29 PM
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Spike
Conc.
50
50
50
50
50
50
50
50
50
250
50
250
50
250
250
1000
1000
50
50
50
50
50
50
100
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
100
50
50
50
50
50
50
50
50
LCS
Result
45.4
46.4
48.9
52.2
44.6
45.8
49.6
46.0
41.8
287
47.0
268
44.2
250
282
3440
1080
48.0
47.2
51.6
40.4
31.2
52.4
99.6
34.6
45.1
42.7
46.6
48.7
50.2
38.3
33.8
51.6
41.3
44.7
46.2
43.2
90.7J
44.8
103
45.5
43.2
50.4
48.0
48.4
43.1
45.9
43.5
LCS
% Rec
% Rec
Limits
91
93
98
104
89
92
99
92
84
115
94
107
88
100
113
344
108
96
94
103
81
62
105
100
69
90
85
93
97
100
77
68
103
83
89
92
86
91
90
103
91
86
101
96
97
86
92
87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
71-126
72-128
63-130
73-124
72-132
73-130
71-127
71-125
61-134
59-150
73-135
46-150
72-130
54-146
41-150
50-150 L0
50-150
72-129
72-127
63-144
71-128
62-124
45-144
63-171
59-130
73-125
60-140
67-127
38-141
76-132
61-114
70-131 L0
75-132
50-179
50-150
77-131
70-133
70-130
72-128
66-139
48-121
68-132
70-130
74-136
60-131
69-134
74-135
75-125
Page 80 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
LABORATORY CONTROL SAMPLE:
127313
Parameter
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
trans-1,4-Dichloro-2-butene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Xylene (Total)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Toluene-d8 (S)
Date: 02/11/2008 03:29 PM
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
Spike
Conc.
50
50
50
50
50
50
50
50
200
50
150
LCS
Result
41.5
41.7
46.1
49.0
37.9
44.8J
48.0
42.3
179
48.6
134
LCS
% Rec
% Rec
Limits
83
83
92
98
76
90
96
85
90
97
89
104
97
98
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
69-124
55-123
75-127
71-131
62-114
50-150
72-123
62-150
50-150
54-136
70-130
65-117
82-130
81-120
Page 81 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
QC Batch:
MPRP/2495
Analysis Method:
EPA 6010
QC Batch Method:
EPA 3050
Analysis Description:
6010 MET
Associated Lab Samples:
METHOD BLANK:
5011474001, 5011474002, 5011474003, 5011474004, 5011474005, 5011474006, 5011474007, 5011474008,
5011474009, 5011474010, 5011474011, 5011474012, 5011474013, 5011474014
127478
Associated Lab Samples:
Parameter
5011474001, 5011474002, 5011474003, 5011474004, 5011474005, 5011474006, 5011474007, 5011474008,
5011474009, 5011474010, 5011474011, 5011474012, 5011474013, 5011474014
Blank
Reporting
Units
Result
Limit
Qualifiers
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
LABORATORY CONTROL SAMPLE:
127479
Parameter
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
ND
ND
ND
ND
ND
ND
ND
Spike
Conc.
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
Parameter
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Date: 02/11/2008 03:29 PM
LCS
Result
50
50
50
50
50
50
25
4.8
33.6
ND
7.7
5.8
ND
ND
LCS
% Rec
52.9
50.1
49.7
49.4
49.8
50.5
25.3
127480
5011474001
Result
Units
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
2.0
2.0
2.0
2.0
2.0
2.0
2.0
% Rec
Limits
106
100
99
99
100
101
101
Qualifiers
80-120
80-120
80-120
80-120
80-120
80-120
80-120
127481
MS
Spike
Conc.
55.1
55.1
55.1
55.1
55.1
55.1
27.6
MSD
Spike
Conc.
51.7
51.7
51.7
51.7
51.7
51.7
25.8
MS
Result
54.7
93.0
45.6
58.4
53.5
48.3
26.5
MSD
Result
MS
% Rec
50.2
86.4
42.1
53.7
49.2
44.3
24.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
90
108
82
92
86
85
96
MSD
% Rec
88
102
81
89
84
83
95
% Rec
Limits
75-125
75-125
75-125
75-125
75-125
75-125
75-125
Max
RPD RPD
8
7
8
8
8
9
7
Qual
20
20
20
20
20
20
20
Page 82 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
QC Batch:
OEXT/5929
Analysis Method:
EPA 8082
QC Batch Method:
EPA 3546
Analysis Description:
8082 GCS PCB
Associated Lab Samples:
METHOD BLANK:
5011474001, 5011474002, 5011474003
127494
Associated Lab Samples:
Parameter
5011474001, 5011474002, 5011474003
Blank
Units
Result
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
LABORATORY CONTROL SAMPLE:
127495
Parameter
PCB-1016 (Aroclor 1016)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
ND
ND
ND
ND
ND
ND
ND
100
PCB-1016 (Aroclor 1016)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
Date: 02/11/2008 03:29 PM
Spike
Conc.
Units
ug/kg
ug/kg
%
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
Parameter
Units
ug/kg
ug/kg
%
Reporting
Limit
35.0
35.0
35.0
35.0
35.0
35.0
35.0
28-137
LCS
Result
167
167
ND
ND
% Rec
Limits
LCS
% Rec
173
172
127505
5011585002
Result
Qualifiers
104
103
99
Qualifiers
50-150
50-150
28-137
127506
MS
Spike
Conc.
189
189
MSD
Spike
Conc.
189
189
MS
Result
151
137
MSD
Result
MS
% Rec
131
122
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
80
73
74
MSD
% Rec
69
65
65
% Rec
Limits
50-150
50-150
28-137
Max
RPD RPD
14
11
Qual
20
20
20
Page 83 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
QC Batch:
PMST/2211
Analysis Method:
ASTM D2974-87
QC Batch Method:
ASTM D2974-87
Analysis Description:
Dry Weight/Percent Moisture
Associated Lab Samples:
SAMPLE DUPLICATE:
5011474001, 5011474002
127969
Parameter
Units
Percent Moisture
SAMPLE DUPLICATE:
5011626001
Result
Dup
Result
2.8
%
Max
RPD
RPD
2.9
4
Qualifiers
5
127970
Parameter
Percent Moisture
Date: 02/11/2008 03:29 PM
Units
%
5011623004
Result
14.0
Dup
Result
Max
RPD
RPD
14.3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
2
Qualifiers
5
Page 84 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
QC Batch:
PMST/2212
Analysis Method:
ASTM D2974-87
QC Batch Method:
ASTM D2974-87
Analysis Description:
Dry Weight/Percent Moisture
Associated Lab Samples:
SAMPLE DUPLICATE:
5011474003, 5011474004, 5011474005, 5011474006, 5011474007, 5011474008, 5011474009, 5011474010,
5011474011, 5011474012, 5011474013, 5011474014
127974
Parameter
Percent Moisture
Date: 02/11/2008 03:29 PM
Units
%
5011474003
Result
13.7
Dup
Result
Max
RPD
RPD
11.9
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
14
Qualifiers
5 R2
Page 85 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
QC Batch:
OEXT/5984
Analysis Method:
EPA 8270
QC Batch Method:
EPA 3546
Analysis Description:
8270 Solid MSSV Microwave Short Spike
Associated Lab Samples:
METHOD BLANK:
5011474014
128273
Associated Lab Samples:
5011474014
Parameter
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
2-Nitroaniline
2-Nitrophenol
3&4-Methylphenol(m&p Cresol)
3,3'-Dichlorobenzidine
3-Nitroaniline
4,6-Dinitro-2-methylphenol
4-Bromophenylphenyl ether
4-Chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenylphenyl ether
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
bis(2-Ethylhexyl)phthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenz(a,h)anthracene
Dibenzofuran
Diethylphthalate
Date: 02/11/2008 03:29 PM
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
Blank
Result
Reporting
Limit
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Qualifiers
330
330
330
330
1600
330
330
330
330
330
330
1600
330
660
660
1600
1600
330
660
660
330
1600
1600
330
330
330
330
330
330
330
330
660
330
330
330
330
330
330
330
330
330
330
330
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 86 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
METHOD BLANK:
128273
Associated Lab Samples:
5011474014
Parameter
Units
Dimethylphthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
LABORATORY CONTROL SAMPLE:
128274
Parameter
2,4-Dinitrotoluene
2-Chlorophenol
4-Chloro-3-methylphenol
4-Nitrophenol
Acenaphthene
N-Nitroso-di-n-propylamine
Pentachlorophenol
Phenol
Pyrene
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
Date: 02/11/2008 03:29 PM
Reporting
Limit
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
84
82
83
75
82
90
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
Blank
Result
Spike
Conc.
3330
3330
3330
3330
3330
3330
3330
3330
3330
Qualifiers
330
330
330
330
330
330
330
330
330
330
330
330
330
1600
300
330
330
34-122
56-118
35-117
50-117
41-124
55-118
LCS
Result
2290
2310
2190
2330
2420
2250
2090
2400
2330
% Rec
Limits
LCS
% Rec
69
69
66
70
72
68
63
72
70
87
83
83
76
83
87
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
54-124
56-111
61-115
42-122
57-113
52-128
24-132
54-117
51-119
34-122
56-118
35-117
50-117
41-124
55-118
Page 87 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
Parameter
2,4-Dinitrotoluene
2-Chlorophenol
4-Chloro-3-methylphenol
4-Nitrophenol
Acenaphthene
N-Nitroso-di-n-propylamine
Pentachlorophenol
Phenol
Pyrene
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
Date: 02/11/2008 03:29 PM
Units
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
%
%
%
%
%
128275
5011626001
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
128276
MS
Spike
Conc.
3420
3420
3420
3420
3420
3420
3420
3420
3420
MSD
Spike
Conc.
3420
3420
3420
3420
3420
3420
3420
3420
3420
MS
Result
2180
196J
823
ND
2190
1970
ND
1530
2330
MSD
Result
MS
% Rec
2200
175J
760
ND
2340
2300
ND
1400
2560
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
64
6
24
0
64
57
0
36
66
0
75
7
67
40
87
MSD
% Rec
64
5
22
0
68
67
0
32
73
0
79
5
71
38
92
% Rec
Limits
57-121
35-125
55-120
27-130
55-114
40-133
10-135
36-130
51-121
34-122
56-118
35-117
50-117
41-124
55-118
Max
RPD RPD
1
8
6
16
9
10
20
20
20
20
20
20
20
20
20
20
20
20
20
20
20
Qual
M0
M0
M0
M0
M0
S0
S0
S0
Page 88 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
QC Batch:
OEXT/6013
Analysis Method:
EPA 8082
QC Batch Method:
EPA 3546
Analysis Description:
8082 GCS PCB
Associated Lab Samples:
METHOD BLANK:
5011474004, 5011474005, 5011474006, 5011474007, 5011474008, 5011474009, 5011474010, 5011474011,
5011474012, 5011474013, 5011474014
128786
Associated Lab Samples:
Parameter
5011474004, 5011474005, 5011474006, 5011474007, 5011474008, 5011474009, 5011474010, 5011474011,
5011474012, 5011474013, 5011474014
Blank
Reporting
Units
Result
Limit
Qualifiers
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
ug/kg
%
LABORATORY CONTROL SAMPLE:
128787
Parameter
PCB-1016 (Aroclor 1016)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
ND
ND
ND
ND
ND
ND
ND
83
ug/kg
ug/kg
%
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
Parameter
PCB-1016 (Aroclor 1016)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
Date: 02/11/2008 03:29 PM
Spike
Conc.
Units
LCS
Result
167
167
ND
ND
LCS
% Rec
148
137
128788
5011662001
Units
Result
ug/kg
ug/kg
%
35.0
35.0
35.0
35.0
35.0
35.0
35.0
28-137
% Rec
Limits
89
82
84
Qualifiers
50-150
50-150
28-137
128789
MS
Spike
Conc.
175
175
MSD
Spike
Conc.
175
175
MS
Result
98.0
98.0
MSD
Result
MS
% Rec
88.1
110
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
56
56
48
MSD
% Rec
50
63
43
% Rec
Limits
50-150
50-150
28-137
Max
RPD RPD
11
12
Qual
20
20
20
Page 89 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALIFIERS
Project:
Beech Grove 6892.002
Pace Project No.:
5011474
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
ANALYTE QUALIFIERS
1d
The Sample was analyzed at dilution due to its physical characteristics. SAQ 02.08.08
2d
Due to the viscosity of the extract, it was run at 10x. KES 1-31-07
3d
The Sample was analyzed at dilution due to its physical charachteristics. SAQ 02.08.08
4d
Due to the viscosity of the extract, it was run at 10x. KES 1-31-08
J
Analyte detected below reporting limit, therefore result is an estimate.
L0
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
M0
Matrix spike recovery was outside laboratory control limits.
R1
RPD value was outside control limits.
R2
RPD value was outside control limits due to matrix interference
S0
Surrogate recovery outside laboratory control limits.
S4
Surrogate recovery not evaluated against control limits due to sample dilution.
Date: 02/11/2008 03:29 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 90 of 90
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
LIMS USE: FR - DOUG PETROFF
LIMS OBJECT ID: 5011526
February 12, 2008
Mr. Doug Petroff
The Schneider Corporation
8901 Otis Ave
Indianapolis, IN 46216
RE: Project: Beech Grove Site 6892.002
Pace Project No.: 5011526
Dear Mr. Petroff:
Enclosed are the analytical results for sample(s) received by the laboratory on January 28, 2008.
The results relate only to the samples included in this report. Results reported herein conform to the
most current NELAC standards, where applicable, unless otherwise narrated in the body of the
report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Donna Spyker
dspyker@pacelabs.com
Project Manager
Illinois/NELAC Certification Number: 100418
Indiana Certification Number: C-49-06
Kansas Certification Number: E-10247
Kentucky Certification Number: 0042
Ohio VAP: CL0065
Pennsylvania: 68-00791
West Virginia Certification Number: 330
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
SAMPLE SUMMARY
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Lab ID
Sample ID
Matrix
Date Collected
Date Received
5011526001
GP-11
Water
01/25/08 10:30
01/28/08 11:48
5011526002
GP-10
Water
01/25/08 11:30
01/28/08 11:48
5011526003
GP-8
Water
01/25/08 13:30
01/28/08 11:48
5011526004
GP-12
Water
01/25/08 15:30
01/28/08 11:48
5011526005
GP-2
Water
01/25/08 17:00
01/28/08 11:48
5011526006
GP-4
Water
01/26/08 12:30
01/28/08 11:48
5011526007
GP-6
Water
01/26/08 14:00
01/28/08 11:48
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 2 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
SAMPLE ANALYTE COUNT
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Lab ID
5011526001
5011526002
5011526003
5011526004
5011526005
5011526006
5011526007
Sample ID
GP-11
GP-10
GP-8
GP-12
GP-2
GP-4
GP-6
Method
Analysts
Analytes
Reported
EPA 6010
FRW
7
EPA 7470
LLB
1
EPA 8082
SAQ
8
EPA 8260
SLB
72
EPA 8270
KES
66
EPA 6010
FRW
7
EPA 7470
LLB
1
EPA 8082
SAQ
8
EPA 8260
SLB
72
EPA 8270
KES
66
EPA 6010
FRW
7
EPA 7470
LLB
1
EPA 8082
SAQ
8
EPA 8260
SLB
72
EPA 8270
KES
66
EPA 6010
FRW
7
EPA 7470
LLB
1
EPA 8082
SAQ
8
EPA 8260
SLB
72
EPA 8270
KES
66
EPA 6010
FRW
7
EPA 7470
LLB
1
EPA 8082
SAQ
8
EPA 8260
SLB
72
EPA 8270
KES
66
EPA 6010
FRW
7
EPA 7470
LLB
1
EPA 8082
SAQ
8
EPA 8260
SLB
72
EPA 8270
KES
66
EPA 6010
FRW
7
EPA 7470
LLB
1
EPA 8082
SAQ
8
EPA 8260
SLB
72
EPA 8270
KES
66
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 3 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-11
Parameters
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mercury
Mercury
8270 MSSV Semivolatile Organic
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Date: 02/12/2008 03:16 PM
Lab ID: 5011526001
Results
Units
Collected: 01/25/08 10:30
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8082 Preparation Method: EPA 3510
ND
ND
ND
ND
ND
ND
ND
94
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
0.68
0.68
0.68
0.68
0.68
0.68
0.68
10-143
1
1
1
1
1
1
1
1
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/31/08 15:23
01/31/08 15:23
01/31/08 15:23
01/31/08 15:23
01/31/08 15:23
01/31/08 15:23
01/31/08 15:23
01/31/08 15:23
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
877-09-8
01/31/08 03:20
01/31/08 03:20
01/31/08 03:20
01/31/08 03:20
01/31/08 03:20
01/31/08 03:20
01/31/08 03:20
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
Analytical Method: EPA 6010 Preparation Method: EPA 3010
141
1080
7.3
269
168
60.0
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
10.0
100
5.0
10.0
10.0
10.0
50.0
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
Analytical Method: EPA 7470 Preparation Method: EPA 7470
ND ug/L
6.0
1
01/29/08 00:00 01/30/08 15:45 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3510
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
12.2
12.2
12.2
12.2
12.2
12.2
12.2
12.2
24.4
12.2
12.2
24.4
24.4
12.2
12.2
6.1
12.2
12.2
12.2
12.2
12.2
12.2
24.4
12.2
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
91-94-1
120-83-2
Page 4 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-11
Parameters
8270 MSSV Semivolatile Organic
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260 MSV
Acetone
Acrolein
Acrylonitrile
Date: 02/12/2008 03:16 PM
Lab ID: 5011526001
Results
Collected: 01/25/08 10:30
Units
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3510
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
76
72
71
38
59
73
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
%
%
12.2
12.2
12.2
12.2
61.0
61.0
12.2
12.2
12.2
6.1
12.2
12.2
6.1
12.2
24.4
12.2
12.2
12.2
12.2
12.2
24.4
6.1
61.0
61.0
61.0
12.2
12.2
61.0
12.2
12.2
61.0
12.2
12.2
12.2
12.2
12.2
40-112
31-114
10-116
10-100
13-100
26-125
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
100
100
100
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
01/30/08 18:51
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
367-12-4
118-79-6
Analytical Method: EPA 8260
ND ug/L
ND ug/L
ND ug/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 10:54 67-64-1
01/31/08 10:54 107-02-8
01/31/08 10:54 107-13-1
Page 5 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-11
Parameters
8260 MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
2-Hexanone
Iodomethane
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Date: 02/12/2008 03:16 PM
Lab ID: 5011526001
Results
Collected: 01/25/08 10:30
Units
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
5.0
5.0
5.0
5.0
5.0
5.0
25.0
5.0
5.0
5.0
10.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
100
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
100
5.0
25.0
10.0
5.0
5.0
5.0
25.0
4.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
110-57-6
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
97-63-2
87-68-3
591-78-6
74-88-4
98-82-8
99-87-6
75-09-2
108-10-1
1634-04-4
Page 6 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-11
Parameters
8260 MSV
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Dibromofluoromethane (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 02/12/2008 03:16 PM
Lab ID: 5011526001
Results
Collected: 01/25/08 10:30
Units
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
106
101
98
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10.0
2.0
10.0
82-122
73-120
80-120
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
01/31/08 10:54
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
1868-53-7
460-00-4
2037-26-5
Page 7 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-10
Parameters
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mercury
Mercury
8270 MSSV Semivolatile Organic
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Date: 02/12/2008 03:16 PM
Lab ID: 5011526002
Results
Units
Collected: 01/25/08 11:30
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8082 Preparation Method: EPA 3510
ND
ND
ND
ND
ND
3.5
ND
66
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
1.1
1.1
1.1
1.1
1.1
1.1
1.1
10-143
1
1
1
1
1
1
1
1
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
02/07/08 16:41
02/07/08 16:41
02/07/08 16:41
02/07/08 16:41
02/07/08 16:41
02/07/08 16:41
02/07/08 16:41
02/07/08 16:41
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
877-09-8
01/31/08 03:26
01/31/08 03:26
01/31/08 03:26
01/31/08 03:26
01/31/08 03:26
01/31/08 03:26
01/31/08 03:26
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
Analytical Method: EPA 6010 Preparation Method: EPA 3010
640
8460
51.5
1790
9600
215
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
50.0
500
25.0
50.0
50.0
50.0
250
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
Analytical Method: EPA 7470 Preparation Method: EPA 7470
ND ug/L
20.0
1
01/29/08 00:00 01/30/08 15:47 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3510
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
13.7
13.7
13.7
13.7
13.7
13.7
13.7
13.7
27.4
13.7
13.7
27.4
27.4
13.7
13.7
6.8
13.7
13.7
13.7
13.7
13.7
13.7
27.4
13.7
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
91-94-1
120-83-2
Page 8 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-10
Parameters
8270 MSSV Semivolatile Organic
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260 MSV
Acetone
Acrolein
Acrylonitrile
Date: 02/12/2008 03:16 PM
Lab ID: 5011526002
Results
Collected: 01/25/08 11:30
Units
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3510
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
81
79
78
41
57
77
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
%
%
13.7
13.7
13.7
13.7
68.5
68.5
13.7
13.7
13.7
6.8
13.7
13.7
6.8
13.7
27.4
13.7
13.7
13.7
13.7
13.7
27.4
6.8
68.5
68.5
68.5
13.7
13.7
68.5
13.7
13.7
68.5
13.7
13.7
13.7
13.7
13.7
40-112
31-114
10-116
10-100
13-100
26-125
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
100
100
100
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
01/31/08 01:11
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
367-12-4
118-79-6
Analytical Method: EPA 8260
ND ug/L
ND ug/L
ND ug/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 11:24 67-64-1
01/31/08 11:24 107-02-8
01/31/08 11:24 107-13-1
Page 9 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-10
Parameters
8260 MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
2-Hexanone
Iodomethane
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Date: 02/12/2008 03:16 PM
Lab ID: 5011526002
Results
Collected: 01/25/08 11:30
Units
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
5.0
5.0
5.0
5.0
5.0
5.0
25.0
5.0
5.0
5.0
10.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
100
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
100
5.0
25.0
10.0
5.0
5.0
5.0
25.0
4.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
110-57-6
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
97-63-2
87-68-3
591-78-6
74-88-4
98-82-8
99-87-6
75-09-2
108-10-1
1634-04-4
Page 10 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-10
Parameters
8260 MSV
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Dibromofluoromethane (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 02/12/2008 03:16 PM
Lab ID: 5011526002
Results
Collected: 01/25/08 11:30
Units
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
106
101
96
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10.0
2.0
10.0
82-122
73-120
80-120
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
01/31/08 11:24
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
1868-53-7
460-00-4
2037-26-5
Page 11 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-8
Parameters
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mercury
Mercury
8270 MSSV Semivolatile Organic
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Date: 02/12/2008 03:16 PM
Lab ID: 5011526003
Results
Units
Collected: 01/25/08 13:30
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8082 Preparation Method: EPA 3510
ND
ND
ND
ND
ND
ND
ND
90
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
0.64
0.64
0.64
0.64
0.64
0.64
0.64
10-143
1
1
1
1
1
1
1
1
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/31/08 15:40
01/31/08 15:40
01/31/08 15:40
01/31/08 15:40
01/31/08 15:40
01/31/08 15:40
01/31/08 15:40
01/31/08 15:40
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
877-09-8
01/31/08 03:31
01/31/08 03:31
01/31/08 03:31
01/31/08 03:31
01/31/08 03:31
01/31/08 03:31
01/31/08 03:31
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
Analytical Method: EPA 6010 Preparation Method: EPA 3010
519
3260
29.5
802
699
161
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
50.0
500
25.0
50.0
50.0
50.0
250
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
Analytical Method: EPA 7470 Preparation Method: EPA 7470
ND ug/L
20.0
1
01/29/08 00:00 01/30/08 15:48 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3510
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
13.5
13.5
13.5
13.5
13.5
13.5
13.5
13.5
27.0
13.5
13.5
27.0
27.0
13.5
13.5
6.8
13.5
13.5
13.5
13.5
13.5
13.5
27.0
13.5
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
91-94-1
120-83-2
Page 12 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-8
Parameters
8270 MSSV Semivolatile Organic
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260 MSV
Acetone
Acrolein
Acrylonitrile
Date: 02/12/2008 03:16 PM
Lab ID: 5011526003
Results
Collected: 01/25/08 13:30
Units
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3510
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
88
79
74
44
59
74
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
%
%
13.5
13.5
13.5
13.5
67.6
67.6
13.5
13.5
13.5
6.8
13.5
13.5
6.8
13.5
27.0
13.5
13.5
13.5
13.5
13.5
27.0
6.8
67.6
67.6
67.6
13.5
13.5
67.6
13.5
13.5
67.6
13.5
13.5
13.5
13.5
13.5
40-112
31-114
10-116
10-100
13-100
26-125
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
100
100
100
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
01/31/08 01:32
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
367-12-4
118-79-6
Analytical Method: EPA 8260
ND ug/L
ND ug/L
ND ug/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 11:54 67-64-1
01/31/08 11:54 107-02-8
01/31/08 11:54 107-13-1
Page 13 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-8
Parameters
8260 MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
2-Hexanone
Iodomethane
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Date: 02/12/2008 03:16 PM
Lab ID: 5011526003
Results
Collected: 01/25/08 13:30
Units
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
5.0
5.0
5.0
5.0
5.0
5.0
25.0
5.0
5.0
5.0
10.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
100
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
100
5.0
25.0
10.0
5.0
5.0
5.0
25.0
4.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
110-57-6
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
97-63-2
87-68-3
591-78-6
74-88-4
98-82-8
99-87-6
75-09-2
108-10-1
1634-04-4
Page 14 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-8
Parameters
8260 MSV
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Dibromofluoromethane (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 02/12/2008 03:16 PM
Lab ID: 5011526003
Results
Collected: 01/25/08 13:30
Units
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
105
101
96
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10.0
2.0
10.0
82-122
73-120
80-120
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
01/31/08 11:54
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
1868-53-7
460-00-4
2037-26-5
Page 15 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-12
Parameters
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mercury
Mercury
8270 MSSV Semivolatile Organic
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Date: 02/12/2008 03:16 PM
Lab ID: 5011526004
Results
Units
Collected: 01/25/08 15:30
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8082 Preparation Method: EPA 3510
ND
ND
ND
ND
ND
ND
ND
92
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
0.60
0.60
0.60
0.60
0.60
0.60
0.60
10-143
1
1
1
1
1
1
1
1
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/31/08 15:48
01/31/08 15:48
01/31/08 15:48
01/31/08 15:48
01/31/08 15:48
01/31/08 15:48
01/31/08 15:48
01/31/08 15:48
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
877-09-8
01/31/08 03:37
01/31/08 03:37
01/31/08 03:37
01/31/08 03:37
01/31/08 03:37
01/31/08 03:37
01/31/08 03:37
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
Analytical Method: EPA 6010 Preparation Method: EPA 3010
166
2110
10.1
343
820
41.1
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
10.0
100
5.0
10.0
10.0
10.0
50.0
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
Analytical Method: EPA 7470 Preparation Method: EPA 7470
ND ug/L
20.0
1
01/29/08 00:00 01/30/08 16:44 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3510
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
12.0
12.0
12.0
12.0
12.0
12.0
12.0
12.0
24.1
12.0
12.0
24.1
24.1
12.0
12.0
6.0
12.0
12.0
12.0
12.0
12.0
12.0
24.1
12.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
91-94-1
120-83-2
Page 16 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-12
Parameters
8270 MSSV Semivolatile Organic
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260 MSV
Acetone
Acrolein
Acrylonitrile
Date: 02/12/2008 03:16 PM
Lab ID: 5011526004
Results
Collected: 01/25/08 15:30
Units
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3510
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
81
77
80
38
56
77
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
%
%
12.0
12.0
12.0
12.0
60.2
60.2
12.0
12.0
12.0
6.0
12.0
12.0
6.0
12.0
24.1
12.0
12.0
12.0
12.0
12.0
24.1
6.0
60.2
60.2
60.2
12.0
12.0
60.2
12.0
12.0
60.2
12.0
12.0
12.0
12.0
12.0
40-112
31-114
10-116
10-100
13-100
26-125
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
100
100
100
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
01/30/08 19:38
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
367-12-4
118-79-6
Analytical Method: EPA 8260
ND ug/L
ND ug/L
ND ug/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 12:29 67-64-1
01/31/08 12:29 107-02-8
01/31/08 12:29 107-13-1
Page 17 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-12
Parameters
8260 MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
2-Hexanone
Iodomethane
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Date: 02/12/2008 03:16 PM
Lab ID: 5011526004
Results
Collected: 01/25/08 15:30
Units
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
5.0
5.0
5.0
5.0
5.0
5.0
25.0
5.0
5.0
5.0
10.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
100
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
100
5.0
25.0
10.0
5.0
5.0
5.0
25.0
4.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
110-57-6
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
97-63-2
87-68-3
591-78-6
74-88-4
98-82-8
99-87-6
75-09-2
108-10-1
1634-04-4
Page 18 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-12
Parameters
8260 MSV
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Dibromofluoromethane (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 02/12/2008 03:16 PM
Lab ID: 5011526004
Results
Collected: 01/25/08 15:30
Units
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
102
99
97
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10.0
2.0
10.0
82-122
73-120
80-120
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
01/31/08 12:29
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
1868-53-7
460-00-4
2037-26-5
Page 19 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-2
Parameters
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mercury
Mercury
8270 MSSV Semivolatile Organic
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Date: 02/12/2008 03:16 PM
Lab ID: 5011526005
Results
Units
Collected: 01/25/08 17:00
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8082 Preparation Method: EPA 3510
ND
ND
ND
ND
ND
ND
ND
93
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
0.63
0.63
0.63
0.63
0.63
0.63
0.63
10-143
1
1
1
1
1
1
1
1
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/31/08 15:57
01/31/08 15:57
01/31/08 15:57
01/31/08 15:57
01/31/08 15:57
01/31/08 15:57
01/31/08 15:57
01/31/08 15:57
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
877-09-8
01/31/08 03:43
01/31/08 03:43
01/31/08 03:43
01/31/08 03:43
01/31/08 03:43
01/31/08 03:43
01/31/08 03:43
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
Analytical Method: EPA 6010 Preparation Method: EPA 3010
160
1240
13.2
371
213
49.7
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
10.0
100
5.0
10.0
10.0
10.0
50.0
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
Analytical Method: EPA 7470 Preparation Method: EPA 7470
ND ug/L
20.0
1
01/29/08 00:00 01/30/08 16:45 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3510
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
11.8
11.8
11.8
11.8
11.8
11.8
11.8
11.8
23.5
11.8
11.8
23.5
23.5
11.8
11.8
5.9
11.8
11.8
11.8
11.8
11.8
11.8
23.5
11.8
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
91-94-1
120-83-2
Page 20 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-2
Parameters
8270 MSSV Semivolatile Organic
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260 MSV
Acetone
Acrolein
Acrylonitrile
Date: 02/12/2008 03:16 PM
Lab ID: 5011526005
Results
Collected: 01/25/08 17:00
Units
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3510
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
86
77
75
38
58
86
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
%
%
11.8
11.8
11.8
11.8
58.8
58.8
11.8
11.8
11.8
5.9
11.8
11.8
5.9
11.8
23.5
11.8
11.8
11.8
11.8
11.8
23.5
5.9
58.8
58.8
58.8
11.8
11.8
58.8
11.8
11.8
58.8
11.8
11.8
11.8
11.8
11.8
40-112
31-114
10-116
10-100
13-100
26-125
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
100
100
100
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
01/30/08 19:59
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
367-12-4
118-79-6
Analytical Method: EPA 8260
ND ug/L
ND ug/L
ND ug/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 13:33 67-64-1
01/31/08 13:33 107-02-8
01/31/08 13:33 107-13-1
Page 21 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-2
Parameters
8260 MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
2-Hexanone
Iodomethane
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Date: 02/12/2008 03:16 PM
Lab ID: 5011526005
Results
Collected: 01/25/08 17:00
Units
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
5.0
5.0
5.0
5.0
5.0
5.0
25.0
5.0
5.0
5.0
10.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
100
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
100
5.0
25.0
10.0
5.0
5.0
5.0
25.0
4.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
110-57-6
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
97-63-2
87-68-3
591-78-6
74-88-4
98-82-8
99-87-6
75-09-2
108-10-1
1634-04-4
Page 22 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-2
Parameters
8260 MSV
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Dibromofluoromethane (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 02/12/2008 03:16 PM
Lab ID: 5011526005
Results
Collected: 01/25/08 17:00
Units
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
104
102
97
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10.0
2.0
10.0
82-122
73-120
80-120
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
01/31/08 13:33
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
1868-53-7
460-00-4
2037-26-5
Page 23 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-4
Parameters
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mercury
Mercury
8270 MSSV Semivolatile Organic
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Date: 02/12/2008 03:16 PM
Lab ID: 5011526006
Results
Units
Collected: 01/26/08 12:30
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8082 Preparation Method: EPA 3510
ND
ND
ND
ND
ND
ND
ND
97
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
0.62
0.62
0.62
0.62
0.62
0.62
0.62
10-143
1
1
1
1
1
1
1
1
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/31/08 16:05
01/31/08 16:05
01/31/08 16:05
01/31/08 16:05
01/31/08 16:05
01/31/08 16:05
01/31/08 16:05
01/31/08 16:05
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
877-09-8
01/31/08 03:48
01/31/08 03:48
01/31/08 03:48
01/31/08 03:48
01/31/08 03:48
01/31/08 03:48
01/31/08 03:48
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
Analytical Method: EPA 6010 Preparation Method: EPA 3010
78.0
860
5.0
249
114
31.4
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
10.0
100
5.0
10.0
10.0
10.0
50.0
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
Analytical Method: EPA 7470 Preparation Method: EPA 7470
ND ug/L
6.0
1
01/29/08 00:00 01/30/08 16:47 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3510
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
14.1
14.1
14.1
14.1
14.1
14.1
14.1
14.1
28.2
14.1
14.1
28.2
28.2
14.1
14.1
7.0
14.1
14.1
14.1
14.1
14.1
14.1
28.2
14.1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
91-94-1
120-83-2
Page 24 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-4
Parameters
8270 MSSV Semivolatile Organic
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260 MSV
Acetone
Acrolein
Acrylonitrile
Date: 02/12/2008 03:16 PM
Lab ID: 5011526006
Results
Collected: 01/26/08 12:30
Units
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3510
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
86
77
54
43
59
80
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
%
%
14.1
14.1
14.1
14.1
70.4
70.4
14.1
14.1
14.1
7.0
14.1
14.1
7.0
14.1
28.2
14.1
14.1
14.1
14.1
14.1
28.2
7.0
70.4
70.4
70.4
14.1
14.1
70.4
14.1
14.1
70.4
14.1
14.1
14.1
14.1
14.1
40-112
31-114
10-116
10-100
13-100
26-125
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
100
100
100
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
01/31/08 00:50
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
367-12-4
118-79-6
Analytical Method: EPA 8260
ND ug/L
ND ug/L
ND ug/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 14:08 67-64-1
01/31/08 14:08 107-02-8
01/31/08 14:08 107-13-1
Page 25 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-4
Parameters
8260 MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
2-Hexanone
Iodomethane
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Date: 02/12/2008 03:16 PM
Lab ID: 5011526006
Results
Collected: 01/26/08 12:30
Units
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
5.0
5.0
5.0
5.0
5.0
5.0
25.0
5.0
5.0
5.0
10.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
100
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
100
5.0
25.0
10.0
5.0
5.0
5.0
25.0
4.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
110-57-6
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
97-63-2
87-68-3
591-78-6
74-88-4
98-82-8
99-87-6
75-09-2
108-10-1
1634-04-4
Page 26 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-4
Parameters
8260 MSV
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Dibromofluoromethane (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 02/12/2008 03:16 PM
Lab ID: 5011526006
Results
Collected: 01/26/08 12:30
Units
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
106
99
98
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10.0
2.0
10.0
82-122
73-120
80-120
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
01/31/08 14:08
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
1868-53-7
460-00-4
2037-26-5
Page 27 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-6
Parameters
8082 GCS PCB
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
6010 MET ICP
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
7470 Mercury
Mercury
8270 MSSV Semivolatile Organic
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
4-Bromophenylphenyl ether
Butylbenzylphthalate
4-Chloro-3-methylphenol
4-Chloroaniline
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
2-Chloronaphthalene
2-Chlorophenol
4-Chlorophenylphenyl ether
Chrysene
Dibenz(a,h)anthracene
Dibenzofuran
3,3'-Dichlorobenzidine
2,4-Dichlorophenol
Date: 02/12/2008 03:16 PM
Lab ID: 5011526007
Results
Units
Collected: 01/26/08 14:00
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8082 Preparation Method: EPA 3510
ND
ND
ND
ND
ND
ND
ND
89
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
0.68
0.68
0.68
0.68
0.68
0.68
0.68
10-143
1
1
1
1
1
1
1
1
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/30/08 00:00
01/31/08 16:14
01/31/08 16:14
01/31/08 16:14
01/31/08 16:14
01/31/08 16:14
01/31/08 16:14
01/31/08 16:14
01/31/08 16:14
12674-11-2
11104-28-2
11141-16-5
53469-21-9
12672-29-6
11097-69-1
11096-82-5
877-09-8
01/31/08 03:54
01/31/08 03:54
01/31/08 03:54
01/31/08 03:54
01/31/08 03:54
01/31/08 03:54
01/31/08 03:54
7440-38-2
7440-39-3
7440-43-9
7440-47-3
7439-92-1
7782-49-2
7440-22-4
Analytical Method: EPA 6010 Preparation Method: EPA 3010
82.1
976
6.6
258
112
31.2
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
10.0
100
5.0
10.0
10.0
10.0
50.0
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
Analytical Method: EPA 7470 Preparation Method: EPA 7470
ND ug/L
2.0
1
01/29/08 00:00 01/30/08 16:48 7439-97-6
Analytical Method: EPA 8270 Preparation Method: EPA 3510
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
14.7
14.7
14.7
14.7
14.7
14.7
14.7
14.7
29.4
14.7
14.7
29.4
29.4
14.7
14.7
7.4
14.7
14.7
14.7
14.7
14.7
14.7
29.4
14.7
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
83-32-9
208-96-8
120-12-7
56-55-3
50-32-8
205-99-2
191-24-2
207-08-9
100-51-6
101-55-3
85-68-7
59-50-7
106-47-8
111-91-1
111-44-4
108-60-1
91-58-7
95-57-8
7005-72-3
218-01-9
53-70-3
132-64-9
91-94-1
120-83-2
Page 28 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-6
Parameters
8270 MSSV Semivolatile Organic
Diethylphthalate
2,4-Dimethylphenol
Dimethylphthalate
Di-n-butylphthalate
4,6-Dinitro-2-methylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
Di-n-octylphthalate
bis(2-Ethylhexyl)phthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p Cresol)
Naphthalene
2-Nitroaniline
3-Nitroaniline
4-Nitroaniline
Nitrobenzene
2-Nitrophenol
4-Nitrophenol
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d6 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
8260 MSV
Acetone
Acrolein
Acrylonitrile
Date: 02/12/2008 03:16 PM
Lab ID: 5011526007
Results
Collected: 01/26/08 14:00
Units
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8270 Preparation Method: EPA 3510
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
158
147
146
91
134
151
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
%
%
14.7
14.7
14.7
14.7
73.5
73.5
14.7
14.7
14.7
7.4
14.7
14.7
7.4
14.7
29.4
14.7
14.7
14.7
14.7
14.7
29.4
7.4
73.5
73.5
73.5
14.7
14.7
73.5
14.7
14.7
73.5
14.7
14.7
14.7
14.7
14.7
40-112
31-114
10-116
10-100
13-100
26-125
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
100
100
100
1
1
1
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/29/08 00:00
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
01/30/08 19:22
84-66-2
105-67-9
131-11-3
84-74-2
534-52-1
51-28-5
121-14-2
606-20-2
117-84-0
117-81-7
206-44-0
86-73-7
87-68-3
118-74-1
77-47-4
67-72-1
193-39-5
78-59-1
91-57-6
95-48-7
91-20-3
88-74-4
99-09-2
100-01-6
98-95-3
88-75-5
100-02-7
621-64-7
86-30-6
87-86-5
85-01-8
108-95-2
129-00-0
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
13127-88-3
367-12-4
118-79-6
S3
S3
S3
S3
S3
Analytical Method: EPA 8260
ND ug/L
ND ug/L
ND ug/L
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 15:17 67-64-1
01/31/08 15:17 107-02-8
01/31/08 15:17 107-13-1
Page 29 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-6
Parameters
8260 MSV
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
2-Butanone (MEK)
n-Butylbenzene
sec-Butylbenzene
tert-Butylbenzene
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
2-Chlorotoluene
4-Chlorotoluene
Dibromochloromethane
1,2-Dibromoethane (EDB)
Dibromomethane
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
trans-1,4-Dichloro-2-butene
Dichlorodifluoromethane
1,1-Dichloroethane
1,2-Dichloroethane
1,1-Dichloroethene
cis-1,2-Dichloroethene
trans-1,2-Dichloroethene
1,2-Dichloropropane
1,3-Dichloropropane
2,2-Dichloropropane
1,1-Dichloropropene
cis-1,3-Dichloropropene
trans-1,3-Dichloropropene
Ethylbenzene
Ethyl methacrylate
Hexachloro-1,3-butadiene
2-Hexanone
Iodomethane
Isopropylbenzene (Cumene)
p-Isopropyltoluene
Methylene chloride
4-Methyl-2-pentanone (MIBK)
Methyl-tert-butyl ether
Date: 02/12/2008 03:16 PM
Lab ID: 5011526007
Results
Collected: 01/26/08 14:00
Units
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
5.0
5.0
5.0
5.0
5.0
5.0
25.0
5.0
5.0
5.0
10.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
100
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
100
5.0
25.0
10.0
5.0
5.0
5.0
25.0
4.0
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
71-43-2
108-86-1
74-97-5
75-27-4
75-25-2
74-83-9
78-93-3
104-51-8
135-98-8
98-06-6
75-15-0
56-23-5
108-90-7
75-00-3
67-66-3
74-87-3
95-49-8
106-43-4
124-48-1
106-93-4
74-95-3
95-50-1
541-73-1
106-46-7
110-57-6
75-71-8
75-34-3
107-06-2
75-35-4
156-59-2
156-60-5
78-87-5
142-28-9
594-20-7
563-58-6
10061-01-5
10061-02-6
100-41-4
97-63-2
87-68-3
591-78-6
74-88-4
98-82-8
99-87-6
75-09-2
108-10-1
1634-04-4
Page 30 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
ANALYTICAL RESULTS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
Sample: GP-6
Parameters
8260 MSV
Naphthalene
n-Propylbenzene
Styrene
1,1,1,2-Tetrachloroethane
1,1,2,2-Tetrachloroethane
Tetrachloroethene
Toluene
1,2,3-Trichlorobenzene
1,2,4-Trichlorobenzene
1,1,1-Trichloroethane
1,1,2-Trichloroethane
Trichloroethene
Trichlorofluoromethane
1,2,3-Trichloropropane
1,2,4-Trimethylbenzene
1,3,5-Trimethylbenzene
Vinyl acetate
Vinyl chloride
Xylene (Total)
Dibromofluoromethane (S)
4-Bromofluorobenzene (S)
Toluene-d8 (S)
Date: 02/12/2008 03:16 PM
Lab ID: 5011526007
Results
Collected: 01/26/08 14:00
Units
Report Limit
Received: 01/28/08 11:48
DF
Prepared
Matrix: Water
Analyzed
CAS No.
Qual
Analytical Method: EPA 8260
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
105
97
95
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
10.0
2.0
10.0
82-122
73-120
80-120
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
01/31/08 15:17
91-20-3
103-65-1
100-42-5
630-20-6
79-34-5
127-18-4
108-88-3
87-61-6
120-82-1
71-55-6
79-00-5
79-01-6
75-69-4
96-18-4
95-63-6
108-67-8
108-05-4
75-01-4
1330-20-7
1868-53-7
460-00-4
2037-26-5
Page 31 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
QC Batch:
OEXT/5892
Analysis Method:
EPA 8270
QC Batch Method:
EPA 3510
Analysis Description:
8270 Water MSSV
Associated Lab Samples:
METHOD BLANK:
5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007
126776
Associated Lab Samples:
Parameter
5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007
Blank
Reporting
Units
Result
Limit
Qualifiers
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophenol
2,4-Dimethylphenol
2,4-Dinitrophenol
2,4-Dinitrotoluene
2,6-Dinitrotoluene
2-Chloronaphthalene
2-Chlorophenol
2-Methylnaphthalene
2-Methylphenol(o-Cresol)
2-Nitroaniline
2-Nitrophenol
3&4-Methylphenol(m&p Cresol)
3,3'-Dichlorobenzidine
3-Nitroaniline
4,6-Dinitro-2-methylphenol
4-Bromophenylphenyl ether
4-Chloro-3-methylphenol
4-Chloroaniline
4-Chlorophenylphenyl ether
4-Nitroaniline
4-Nitrophenol
Acenaphthene
Acenaphthylene
Anthracene
Benzo(a)anthracene
Benzo(a)pyrene
Benzo(b)fluoranthene
Benzo(g,h,i)perylene
Benzo(k)fluoranthene
Benzyl alcohol
bis(2-Chloroethoxy)methane
bis(2-Chloroethyl) ether
bis(2-Chloroisopropyl) ether
bis(2-Ethylhexyl)phthalate
Butylbenzylphthalate
Chrysene
Di-n-butylphthalate
Di-n-octylphthalate
Dibenz(a,h)anthracene
Dibenzofuran
Diethylphthalate
Date: 02/12/2008 03:16 PM
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
10.0
10.0
10.0
10.0
50.0
10.0
10.0
10.0
10.0
10.0
10.0
50.0
10.0
20.0
20.0
50.0
50.0
10.0
20.0
20.0
10.0
50.0
50.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
20.0
10.0
10.0
5.0
5.0
10.0
10.0
10.0
10.0
10.0
10.0
10.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 32 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
METHOD BLANK:
126776
Associated Lab Samples:
Parameter
5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007
Blank
Reporting
Units
Result
Limit
Qualifiers
Dimethylphthalate
Fluoranthene
Fluorene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachlorocyclopentadiene
Hexachloroethane
Indeno(1,2,3-cd)pyrene
Isophorone
N-Nitroso-di-n-propylamine
N-Nitrosodiphenylamine
Naphthalene
Nitrobenzene
Pentachlorophenol
Phenanthrene
Phenol
Pyrene
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
%
%
LABORATORY CONTROL SAMPLE:
126777
Parameter
2,4-Dinitrotoluene
2-Chlorophenol
4-Chloro-3-methylphenol
4-Nitrophenol
Acenaphthene
N-Nitroso-di-n-propylamine
Pentachlorophenol
Phenol
Pyrene
2,4,6-Tribromophenol (S)
2-Fluorobiphenyl (S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-d14 (S)
Date: 02/12/2008 03:16 PM
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
82
75
52
81
34
89
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
%
%
%
Spike
Conc.
100
100
100
100
100
100
100
100
100
10.0
10.0
10.0
5.0
10.0
20.0
10.0
10.0
10.0
10.0
10.0
5.0
10.0
50.0
10.0
10.0
10.0
26-125
31-114
13-100
40-112
10-100
10-116
LCS
Result
93.1
80.5
82.6
44.8J
86.9
89.8
81.8
36.6
93.1
% Rec
Limits
LCS
% Rec
93
81
83
45
87
90
82
37
93
89
79
57
85
36
95
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
39-129
39-105
44-115
10-80
40-116
35-129
16-133
12-120
44-126
26-125
31-114
13-100
40-112
10-100
10-116
Page 33 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
QC Batch:
MPRP/2490
Analysis Method:
EPA 6010
QC Batch Method:
EPA 3010
Analysis Description:
6010 MET
Associated Lab Samples:
METHOD BLANK:
5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007
126785
Associated Lab Samples:
Parameter
5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007
Blank
Reporting
Units
Result
Limit
Qualifiers
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
LABORATORY CONTROL SAMPLE:
126786
Parameter
ND
ND
ND
ND
ND
ND
ND
Spike
Conc.
Units
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
Parameter
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Date: 02/12/2008 03:16 PM
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
10.0
100
5.0
10.0
10.0
10.0
50.0
LCS
Result
1000
1000
1000
1000
1000
1000
500
993
944
962
937
958
964
501
126787
5011471008
Result
1730
9700
14.2
268
791
114
ND
LCS
% Rec
% Rec
Limits
99
94
96
94
96
96
100
Qualifiers
80-120
80-120
80-120
80-120
80-120
80-120
80-120
126788
MS
Spike
Conc.
1000
1000
1000
1000
1000
1000
500
MSD
Spike
Conc.
1000
1000
1000
1000
1000
1000
500
MS
Result
2540
10500
802
1090
1580
892
462
MSD
Result
MS
% Rec
2500
10000
812
1080
1580
882
455
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
80
78
79
82
79
78
92
MSD
% Rec
77
35
80
81
79
77
90
% Rec
Limits
75-125
75-125
75-125
75-125
75-125
75-125
75-125
Max
RPD RPD
1
4
1
1
0
1
2
Qual
20
20 P6
20
20
20
20
20
Page 34 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
QC Batch:
MERP/1511
Analysis Method:
EPA 7470
QC Batch Method:
EPA 7470
Analysis Description:
7470 Mercury
Associated Lab Samples:
METHOD BLANK:
5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007
126811
Associated Lab Samples:
Parameter
5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007
Blank
Reporting
Units
Result
Limit
Qualifiers
Mercury
ug/L
LABORATORY CONTROL SAMPLE:
126812
Parameter
ND
Spike
Conc.
Units
Mercury
ug/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
Parameter
Mercury
Date: 02/12/2008 03:16 PM
Units
ug/L
2.0
LCS
Result
5
4.2
126813
5011471008
Result
ND
LCS
% Rec
% Rec
Limits
83
Qualifiers
80-120
126814
MS
Spike
Conc.
50
MSD
Spike
Conc.
50
MS
Result
41.8
MSD
Result
MS
% Rec
39.4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
83
MSD
% Rec
78
% Rec
Limits
75-125
Max
RPD RPD
6
Qual
20
Page 35 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
QC Batch:
OEXT/5911
Analysis Method:
EPA 8082
QC Batch Method:
EPA 3510
Analysis Description:
8082 GCS PCB Mod
Associated Lab Samples:
METHOD BLANK:
5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007
127169
Associated Lab Samples:
Parameter
5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007
Blank
Reporting
Units
Result
Limit
Qualifiers
PCB-1016 (Aroclor 1016)
PCB-1221 (Aroclor 1221)
PCB-1232 (Aroclor 1232)
PCB-1242 (Aroclor 1242)
PCB-1248 (Aroclor 1248)
PCB-1254 (Aroclor 1254)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
LABORATORY CONTROL SAMPLE:
127170
Parameter
PCB-1016 (Aroclor 1016)
PCB-1260 (Aroclor 1260)
Tetrachloro-m-xylene (S)
Date: 02/12/2008 03:16 PM
ND
ND
ND
ND
ND
ND
ND
84
Units
ug/L
ug/L
%
0.50
0.50
0.50
0.50
0.50
0.50
0.50
10-143
LCS
Result
Spike
Conc.
5
5
% Rec
Limits
LCS
% Rec
5.0
4.8
101
96
85
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
40-160
40-160
10-143
Page 36 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
QC Batch:
MSV/7225
Analysis Method:
EPA 8260
QC Batch Method:
EPA 8260
Analysis Description:
8260 MSV
Associated Lab Samples:
METHOD BLANK:
5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007
127884
Associated Lab Samples:
Parameter
5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007
Blank
Reporting
Units
Result
Limit
Qualifiers
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Date: 02/12/2008 03:16 PM
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
25.0
5.0
25.0
5.0
25.0
100
100
100
5.0
5.0
5.0
5.0
5.0
5.0
10.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 37 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
METHOD BLANK:
127884
Associated Lab Samples:
Parameter
5011526001, 5011526002, 5011526003, 5011526004, 5011526005, 5011526006, 5011526007
Blank
Reporting
Units
Result
Limit
Qualifiers
Dibromomethane
Dichlorodifluoromethane
Ethyl methacrylate
Ethylbenzene
Hexachloro-1,3-butadiene
Iodomethane
Isopropylbenzene (Cumene)
Methyl-tert-butyl ether
Methylene chloride
n-Butylbenzene
n-Propylbenzene
Naphthalene
p-Isopropyltoluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
trans-1,4-Dichloro-2-butene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Xylene (Total)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Toluene-d8 (S)
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
LABORATORY CONTROL SAMPLE:
127885
Parameter
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
Date: 02/12/2008 03:16 PM
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
99
106
98
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Spike
Conc.
50
50
50
50
50
50
50
50
50
50
50
50
5.0
5.0
100
5.0
5.0
10.0
5.0
4.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
5.0
100
5.0
5.0
10.0
2.0
10.0
73-120
82-122
80-120
LCS
Result
LCS
% Rec
53.9
54.2
47.0
49.9
50.1
53.6
52.6
50.2
48.0
49.4
46.9
48.3
% Rec
Limits
108
108
94
100
100
107
105
100
96
99
94
97
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
70-126
70-128
66-134
71-131
72-125
66-140
72-125
63-130
50-139
61-129
72-128
70-130
Page 38 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
LABORATORY CONTROL SAMPLE:
127885
Parameter
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Ethyl methacrylate
Ethylbenzene
Hexachloro-1,3-butadiene
Iodomethane
Isopropylbenzene (Cumene)
Methyl-tert-butyl ether
Methylene chloride
n-Butylbenzene
n-Propylbenzene
Naphthalene
p-Isopropyltoluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Date: 02/12/2008 03:16 PM
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Spike
Conc.
50
50
50
50
50
50
50
50
250
50
250
50
250
250
1000
1000
50
50
50
50
50
50
100
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
100
50
50
50
50
50
50
50
50
50
LCS
Result
47.8
53.2
50.7
46.1
47.4
48.7
47.5
57.3
237
44.7
263
45.2
241
307
219
948
46.8
47.1
48.6
55.0
45.1
39.6
107
59.5
45.0
63.3
49.8
39.4
49.6
45.7
53.8
51.8
40.8
48.8J
47.0
53.1
86.1
48.8
106
49.7
51.9
48.6
50.9
48.2
48.4
47.0
40.2
40.9
LCS
% Rec
% Rec
Limits
96
106
101
92
95
97
95
115
95
89
105
90
96
123
22
95
94
94
97
110
90
79
107
119
90
127
100
79
99
91
108
104
82
98
94
106
86
98
106
99
104
97
102
96
97
94
80
82
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
72-129
66-131
72-125
72-130
74-128
70-130
72-124
62-134
44-150
74-133
38-150
73-129
55-142
29-150
50-150 L0
50-150
75-126
72-129
67-139
70-130
63-127
43-146
52-172
65-125
74-123
61-141
68-127
42-138
77-132
60-119
72-133
76-133
50-179
70-130
70-129
71-132
70-130
74-126
68-139
50-119
70-130
74-135
56-134
70-133
75-133
75-125
69-121
55-121
Page 39 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
LABORATORY CONTROL SAMPLE:
127885
Parameter
Units
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
trans-1,4-Dichloro-2-butene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Xylene (Total)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Toluene-d8 (S)
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
MATRIX SPIKE SAMPLE:
127886
Parameter
1,1,1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Butanone (MEK)
2-Chlorotoluene
2-Hexanone
4-Chlorotoluene
4-Methyl-2-pentanone (MIBK)
Acetone
Acrolein
Acrylonitrile
Benzene
Bromobenzene
Bromochloromethane
Date: 02/12/2008 03:16 PM
LCS
% Rec
LCS
Result
50
50
50
50
50
50
200
50
150
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
Spike
Conc.
46.1
55.7
47.4
51.5J
49.6
48.6
199
39.2
143
5011524001
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Spike
Conc.
% Rec
Limits
92
111
95
103
99
97
100
78
95
104
105
97
MS
Result
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
250
50
250
50
250
250
1000
1000
50
50
50
50.6
55.6
45.6
48.3
50.1
57.5
54.2
46.2
45.7
45.3
45.6
45.7
46.6
52.1
49.8
45.8
45.3
47.5
45.5
57.9
231
45.3
251
44.8
233
256
2040
924
47.5
46.1
47.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qualifiers
72-126
73-131
59-119
50-150
73-123
65-145
50-150
54-139
72-127
73-120
82-122
80-120
MS
% Rec
% Rec
Limits
101
111
91
97
100
115
108
92
91
91
91
91
93
104
100
92
91
95
91
116
92
91
100
90
93
103
204
92
95
92
95
Qualifiers
54-134
63-130
59-139
64-136
67-129
59-150
68-127
39-136
41-137
34-137
36-143
64-132
52-136
62-134
67-128
33-145
47-139
63-134
46-135
51-136
54-148
43-147
60-140
46-139
56-147
27-163
50-150 M0
50-150
66-135
57-135
61-142
Page 40 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALITY CONTROL DATA
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
MATRIX SPIKE SAMPLE:
127886
Parameter
Bromodichloromethane
Bromoform
Bromomethane
Carbon disulfide
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1,2-Dichloroethene
cis-1,3-Dichloropropene
Dibromochloromethane
Dibromomethane
Dichlorodifluoromethane
Ethyl methacrylate
Ethylbenzene
Hexachloro-1,3-butadiene
Iodomethane
Isopropylbenzene (Cumene)
Methyl-tert-butyl ether
Methylene chloride
n-Butylbenzene
n-Propylbenzene
Naphthalene
p-Isopropyltoluene
sec-Butylbenzene
Styrene
tert-Butylbenzene
Tetrachloroethene
Toluene
trans-1,2-Dichloroethene
trans-1,3-Dichloropropene
trans-1,4-Dichloro-2-butene
Trichloroethene
Trichlorofluoromethane
Vinyl acetate
Vinyl chloride
Xylene (Total)
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
Toluene-d8 (S)
Date: 02/12/2008 03:16 PM
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
%
%
%
5011524001
Result
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
Spike
Conc.
50
50
50
100
50
50
50
50
50
50
50
50
50
50
50
50
50
100
50
100
50
50
50
50
50
50
50
50
50
50
50
50
50
50
50
200
50
150
MS
Result
51.9
43.3
41.4
111
59.7
43.9
64.8
49.6
40.8
49.5
44.1
50.2
50.5
46.5
47.2J
46.5
50.7
84.1
49.2
104
50.0
50.4
48.2
47.2
47.7
48.6
46.5
38.7
41.8
45.7
57.0
44.5
46.8J
50.3
53.3
180
43.5
144
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
MS
% Rec
% Rec
Limits
104
87
83
111
119
88
130
99
82
99
88
100
101
93
94
93
101
84
98
104
100
101
96
94
95
97
93
77
84
91
114
89
94
101
107
90
87
96
103
104
97
Qualifiers
60-135
50-127
32-148
46-173
51-130
59-135
58-153
61-133
44-135
75-133
51-121
56-139
70-136
25-175
50-150
59-143
50-155
70-130
48-139
62-147
46-119
50-156
33-153
40-136
38-143
35-151
53-133
37-136
40-127
63-137
70-134
49-121
50-150
61-131
64-146
50-150
54-140
54-140
73-120
82-122
80-120
Page 41 of 42
Pace Analytical Services, Inc.
7726 Moller Road
Indianapolis, IN 46268
(317)875-5894
QUALIFIERS
Project:
Beech Grove Site 6892.002
Pace Project No.:
5011526
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL - Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.
BATCH QUALIFIERS
Batch: MSSV/2236
[1]
A matrix spike/matrix spike duplicate was not performed for this batch due to insufficient sample volume.
Batch: GCSV/2315
[1]
A matrix spike/matrix spike duplicate was not performed for this batch due to insufficient sample volume.
ANALYTE QUALIFIERS
L0
Analyte recovery in the laboratory control sample (LCS) was outside QC limits.
M0
Matrix spike recovery was outside laboratory control limits.
Matrix spike recovery was outside laboratory control limits due to a parent sample concentration notably higher than the
spike level.
Surrogate recovery exceeded laboratory control limits. Analyte presence below reporting limits in associated samples.
Results unaffected by high bias.
P6
S3
Date: 02/12/2008 03:16 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 42 of 42