Q-Lab Corporation SAe Cancels J1960 and J1885 Test Methods
Transcription
Q-Lab Corporation SAe Cancels J1960 and J1885 Test Methods
Q-Lab Corporation Issue 1 – 2008 INFORMATION ON Weathering, LIGHT STABILITY AND CORROSION Testing To receive LabNotes electronically, contact labnotes@q-lab.com SAE Cancels J1960 and J1885 Test Methods Two long-standing and widely-used standards for accelerated testing of automotive materials were cancelled by the Society of Automotive Engineers (SAE). Both documents have been superseded by newer, performance-based standards as of January 11, 2008. Chrysler has approved the Q-Sun for testing of interior and exterior automotive materials. Shown here is the 2008 Chrysler 300C. Chrysler Approves Q-Sun for Automotive Testing Chrysler has approved the company-wide use of Q-Sun Xenon Test Chambers to meet SAE J2527 and J2412 requirements for testing of automotive exterior and interior parts, components and materials, as part of the growing trend toward more cost-effective, performance-based weathering and light stability testing. The decision was the result of five years of research. In addition to the Q-Sun’s reliability, major factors driving the decision were cost savings and confirmed correlation to outdoor results. All Q-Sun models cost much less to purchase and operate than comparable rotating-rack style xenon testers. A technical paper documenting a portion of the Chrysler/ Q-Lab research that led to Chrysler’s accepting the use of Q-Suns in automotive testing, Automotive Xenon Arc Test Methods: A Correlation Study, is available from Q-Lab. J1960 – Accelerated Exposure of Automotive Exterior Materials Using a Controlled Irradiance Water Cooled XenonArc Apparatus, has been cancelled and replaced by J2527 – Performance Based Standard for Accelerated Exposure of Automotive Exterior Materials Using a Controlled Irradiance Xenon-Arc Apparatus (published February 2004). J1885 – Accelerated Exposure of Automotive Interior Trim Components Using a Controlled Irradiance Water Cooled Xenon Arc Apparatus, has been superseded by J2412 – Accelerated Exposure of Automotive Interior Trim Components Using a Controlled Irradiance Xenon-Arc Apparatus (published May 2004). According to the SAE Committee on Fade and Weathering, the rationale for cancelling the standards is that they were equipment-specific, applying only to certain models available from only one manufacturer. The change from standards specifically describing the type of hardware, to performance-based standards that describe test conditions, will reduce costs by allowing users to select from any type of equipment that meets the test parameters. Readers affected by these changes are reminded to update their scopes. For a copy of this technical paper, circle 735 New Q-Lab Training Center Opens in China Q-Lab China has opened its new training center in Shanghai. Serving both customers and sales representatives, the center provides training in accelerated weathering, light stability and corrosion testing. The first training session was held in January, under the supervision of Joe Carney, CET, Q-Lab Corporation’s Service & Repair Manager. Q-Lab China’s new office in Shanghai features a well-equipped training center. Shown above, instructor Mike Garrett explains the Q-Sun’s operation. 800 Canterbury Road, Cleveland, OH 44145 USA Telephone: 1-440-835-8700 Fax: 1-440-835-8738 www.q-lab.com ScientificViewpoint How Can I Tell If My Product Will Last Outdoors? The first of Warren D. Ketola’s two-part series in LabNotes will address outdoor testing. The next installment will cover how to relate outdoor testing with accelerated testing for reliable results. During my long career, I’ve been asked many questions by customers about which weathering tests they should use to evaluate their polymer or product. In most cases, the questions are about use of artificial accelerated weathering tests and how they relate to actual outdoor performance. Some typical questions are: • How many hours does it take in this accelerated test to equal a year in Florida? • I want to warranty this product for five years – how long do I need to test in a QUV running UVA340 lamps? • If my product looks OK after 2000 hours in SAE J2527, how long will it last in Arizona? The answer to all of these types of questions is, it depends. The answer will depend on how the polymer or product responds to the stresses produced by exposure to solar radiation, to temperature, and to moisture. There are many, many artificial accelerated tests that can be used, each producing a different combination of stress conditions. Selecting the optimum test condition can be a daunting task. However, there is one very simple answer to the question of how to tell if your product will last outdoors. That answer is, test your product outdoors. Outdoor testing needs to be the first test you start, before you begin any artificial accelerated weathering test. There are several critical reasons why starting outdoor exposures on your product must be done first. Outdoor Exposures Are Never Wrong While it seems trite, one must remember that the same cannot be said for artificial accelerated weathering tests. Some of these have been shown to be very good predictors of outdoor durability for some materials. However, there are also instances where results from artificial accelerated tests proved to be very poor predictors of outdoor The desert conditions at Q-Lab Arizona feature intense sunlight, high temperatures, and very low humidity. Test specimens may also experience large temperature fluctuations. This extreme climate has been proven useful for testing coatings, plastics and building materials. 2 durability, to the point where the material performing best in the accelerated test actually performed the worst outdoors. You have many options to chose from when selecting an artificial accelerated test. Some might be good and some might be very bad. You don’t have to worry about making a wrong choice of tests when you test outdoors because the results from outdoor testing are never wrong. In fact, results from outdoor testing are now used to specify minimum durability performance for some materials. ASTM D 4956, Standard Specification for Retroreflective Sheeting Materials is an example, where three year exposures in hot/wet and hot/dry climates are required. Validity of Accelerated Weathering Tests As stated above, you have many options to choose from when selecting an artificial accelerated weathering test. Some might be good choices and some very bad. If you do not have results from outdoor exposures, you have absolutely no basis for assessing the validity of your artificial accelerated test. Let’s use an example to illustrate this point. Suppose you had five different options to use for a new product being introduced by your company. Your company wanted to warranty the outdoor durability of the product for three years. All the options met the performance and cost requirements and you used an accelerated test that had given you good information for other products to select the option that would be used for the new product. After the product had been on the market for 18-24 months, your company started to get quite a few warranty claims, because the product was failing outdoors. Everyone is asking about whether the other options could be substituted. Unfortunately, you only had weathering data from the one test. You didn’t think it would be necessary to do outdoor weathering because the test had given reliable results before. Any information you give about whether one of the other options could be used is only a guess. If you had started outdoor weathering on the product, you would have been able to see the marginal performance of the option that was selected and would have been able to make sound recommendations for an alternative. Are you willing to take the risk inherent with not starting your outdoor weathering exposures first? Subtropical conditions at Q-Lab Florida (located south of Miami) are generally hot and humid. Lots of sunshine and abundant rainfall create an environment that is ideal for testing exterior durability and moisture sensitivity. Q-Lab Corporation Outdoor Exposure Factors Now that you are convinced that outdoor testing is the first exposure test you will start, there are a few additional things to consider when setting up your outdoor testing. The first is using multiple locations for outdoor exposures. Your company is going to be making one version of the product you will be testing and it is going to be used in all kinds of climates. The effects of different types of climates can have a profound effect on the type and rate of degradation your product could experience. Q-Rack outdoor exposure rack kits allow you to supplement your current testing program with additional data from other locations. The direct exposure rack shown has additional panel flaps to expand its specimen capacity. Outdoor Testing Is Inexpensive Contrary to what people might think, outdoor weathering testing is very inexpensive when compared to the costs for artificial accelerated testing. Consider the following example. Suppose you need to choose between three formulation options for a new polymer that is critical to your company’s success. You have chosen to use an artificial accelerated test for which the cost is $0.20 per specimen per hour of exposure. You are testing two replicates of each of the three formulations and your test time is 2000 hours. The cost for the artificial accelerated test is $2400, assuming that the 2000 hour exposure is sufficient for you to choose between the materials. In many cases, longer exposures are needed. For your outdoor testing, let’s assume that you will send out separate sets of specimens for 12 months, 24 months and 36 months. Assuming the cost is $.25 per specimen per month, the total cost for the outdoor exposure is $108, which is likely to be spread out over the three years of exposure. It has been my experience that when conducting comprehensive programs of artificial accelerated and outdoor weathering exposures, about 90% of the total cost is for the artificial accelerated testing Some Polymers Degrade Faster in Arizona’s Hot Climate The chart shown in Figure 1 is one example of these differences. The x-axis is the amount of total solar radiation received by the test specimens. It is clear that the higher temperatures experienced in the hot desert exposures of Arizona produced much faster degradation. Moisture is another factor. Some polymers degrade much faster in Florida’s wet climate. For some materials, other effects such as thermal shock or cycling that would be experienced in a northern climate, could have significant effects. From these examples, you can see that you cannot predict durability in all locations using weathering results from only one location. Since you want your outdoor test results to be as “fast” as possible, you need to consider exposures in locations that will provide the most aggressive conditions, and where there is a considerable “history” of exposure information on a variety of materials. You also want to use locations where climate data such as solar radiation, temperature, and moisture for the exposure conditions you choose is readily available. These requirements are met by exposures conducted in the hot/wet climate of south Florida and the hot/desert climate near Phoenix, Arizona. Exposures in these types of climates are considered as international benchmarks for evaluating durability of materials. When setting up your outdoor exposure experiments for each type of climate, you also can choose the angle of exposure (vertical, 45 degrees, or 5 degrees to the horizontal), the type of backing for your test specimens, and whether your materials are exposed directly to the sun or behind window glass. You might also want to choose a solar concentrating exposure where you can accumulate five year’s worth of solar UV radiation in about one year of testing. Outdoor weathering experts can help you in making these choices that are best for your product. High Reliability, Low Cost In summary, the simple reason I recommend starting your product durability testing outdoors is this: Nothing else gives more accurate results, and nothing costs less – except for not testing at all, which can be a costly mistake. Warren Ketola is a noted authority on weathering and a leader in ASTM, ISO, and other standards organizations. He is currently principal of WK Weathering Consulting in St. Paul, Minnesota, after a 37-year career with 3M Commercial Tape and Traffic Safety Systems Divisions. Starting with this issue, he will be a frequent editorial contributor to LabNotes. Figure 1. Outdoor testing in multiple locations is important because there may be significant differences in environmental stresses. Shown here are Arizona and Florida exposures of a vinyl acrylic polymer. The Most Trusted Name in Weathering 3 DataPoint TOW in South Bend, Pennsylvania Why the QUV’s Condensation Cycle Is the Most Realistic Acceleration Possible Time of Wetness (TOW) research conducted in North America indicates materials exposed outdoors are wet a surprisingly high percentage of the time. Our data indicates that, on average, they are wet 30% of the time. This means that, on average, outdoor materials are wet 7.2 hours/day, or over 2,600 hours per year! But that is just an average. In places like Seattle, materials are frequently wet for 12 hours a day, or even more in some seasons. This startlingly high incidence of wetness is caused primarily by dew, not rain. Our data actually shows that, typically, the days with the higher TOW occurred in the absence of rain. In laboratory weathering, it is relatively easy to accelerate the damage caused by sunlight. Accelerating the effects of outdoor moisture is much more difficult. Because materials exposed outdoors are already wet for such a long time under natural conditions, it is effectively impossible to accelerate by increasing the hours of moisture exposure. The only effective way is to accelerate by increasing the temperature of the exposure. The QUV’s long, hot, condensation cycles are superior to methods of moisture simulation commonly used in other testers such as water spray, immersion and high humidity. Materials exposed outdoors are wet a remarkably high percentage of the time. Research indicates that dew (condensation), not rain, is the major source of wetness outdoors. The QUV produces condensation by heating water into a vapor and then recondensing it onto the surface of the test specimen. Because the water is purified in the process, this precludes water-spotting problems and, since there is no need for stills or deionizers, it simplifies QUV installation and operation. The QUV’s hot condensation mechanism brings highly oxygenated, liquid water into intimate contact with the test material for an extended period of time. A typical QUV condensation cycle lasts for 4 hours at 50˚C. Based on the ‘rule of thumb’ that a 10º increase in temperature can double the rate of the reaction, this provides significant acceleration. Consequently, the QUV both simulates and accelerates outdoor moisture attack. For more information on the QUV, circle 200 Look for the Q-Shaped Hole: Panels Are Available in Special Shapes, Sizes, Materials Among the millions of Q-Panel brand test substrates shipped out of Cleveland, Ohio each year are a growing number of special panels that don’t fit the traditional pattern of a rectangular metal panel with a Q-shaped hanging hole. Special shapes and sizes range from 1" (2.54 cm) circles to 15" x 24" (38 cm x 61 cm) formed automotive panels, used for testing, display, or training. Custom, 3-D fabricated assemblies are occasionally requested as a special order. Customers such as architectural firms specify aluminum panels in unusual sizes to coat and use as sales samples. Special order panels offer clean, consistent material quality and finishes at an affordable price. Materials and Surface Treatments Steel panels are made from standard lowcarbon, cold-rolled steel complying with ASTM standards. Types include smooth finish, matte finish, ground (polished) finish, thin/flexible, tinplate, adhesion and abrasion panels, and stainless steel. Panel Trends Robert Little, Q-Lab’s Panel Product Engineer, says that the impact of quality and environmental regulations is being felt in the panel markets. For example, U.K. orders for aluminum panels (including extruded aluminum) are specifying Qualicoat standards. “As regulations get tougher, it will be more important than ever for panel users to be able to rely on the high quality materials and production standards that the Q-Panel brand provides,” he concluded. For more information on panels, circle 502 Aluminum panels are lighter and corrosion resistant. They are available in bare or chromated types, adhesion, automotive styling, or large display panels. Steel panels are packaged with corrosion inhibiting materials and have a shelf life of up to 10 years. Panels receive minimal handling. 4 Iron phosphated panels are made from the same premium steel as our standard panels Large automotive panels can be used for training and are available in two finishes. or display. Q-Lab Corporation Meet the Q-Sun Xenon Family When Q-Lab introduced the Q-Sun Xenon Test Chamber in 1998, its flat array design was considered a major change from the rotating rack technology that was widely used at the time. Less than a decade later, the Q-Sun family has grown to include several flat array models, as well as the new Q-Sun B02 – which updates the traditional rotating rack design to create a more affordable textile lightfastness tester for the 21st century. Model B02 is a new design rotating rack tester specifically designed to meet the requirements of ISO 105 B02 for lightfastness testing of textiles. Thanks to the simple, practical design of this tester, xenon testing now is more affordable for textile labs around the world. Q-Sun Model B02 Simple and Cost-Effective The design of every Q-Sun xenon tester is as simple as possible, making it easy to install, operate and maintain. This reduces both the initial purchase price and operating costs for the life of the equipment. Large Specimen Capacity Q-Sun Xe-1 and Xe-3 models feature a slideout specimen tray that can hold unusual shapes and sizes, even large 3-D parts. The Model B02’s specimen capacity is 48% to 92% larger than comparable models. Efficient Lamps & Filters The Q-Sun’s air-cooled xenon arc lamps reproduce the full spectrum of sunlight. They cost much less than competitive lamps, are easier to install, and have a long service life. Optical filters are used to realistically reproduce sunlight, sunlight through window glass, or other spectra required by test methods. Superior Control Systems Solar Eye TM Irradiance Control ensures maximum repeatability and reproducibility. Calibration is quick and easy with the patented AutoCal system. All Q-Sun models control specimen temperature, and many models feature chamber air temperature and relative humidity control. The Most Trusted Name in Weathering Q-Sun Xenon Test Chambers are used for accelerated weathering and light stability testing of products used indoors or outdoors. Model Xe-1 is an economical, table top tester with one lamp. It is designed for labs with smaller budgets, tight space, or where less testing is performed. Its specimen tray is 9.88" x 18" (251 mm x 457 mm). Options include water spray and a chiller. Q-Suns are used worldwide for accelerated weathering and light stability testing of products used indoors or outdoors. The testers meet a wide range of ISO, ASTM, AATCC, SAE, DIN and other standards. Each Q-Sun model has special features that make it the right choice for specific tests, product applications, or budgets. But all Q-Suns share some common “family” characteristics. Q-Sun Models Xe-1 (left) and Xe-3 Mounting textile specimens on the rotating rack of the Model B02’s large capacity chamber (367 in2/2.362 cm2). For Q-Sun B02 information, circle 733 Model Xe-3 is a full-size unit with three lamps and a 17.75" x 28.26" (451 mm x 718 mm) specimen tray. Options include water spray, dual spray for acid etch, chiller, chamber air temperature and relative humidity controls. Even with its multiple capabilities, the Xe-3 costs much less to purchase and operate than comparable xenon testers. For Q-Sun Xe-1/Xe-3 information, circle 700 PersonnelProfile Melissa Precise, Order Department Supervisor If the job involves orders coming in, or products shipping out from Q-Lab’s Instruments Division, the person in charge is Melissa Precise, Order Department supervisor since mid-2006. A real success story, Melissa joined Q-Lab in 1997 as the receptionist and now supervises a department of five. She is accustomed to comments about her surname being such a good fit with the nature of her work, which demands “precise” accuracy. Q-Lab’s Order Department is responsible for shipping and billing. All outgoing deliveries and freight shipments are handled by the department. This includes everything from container shipments to Europe to trade show display materials. To keep up with the complex demands of global logistics, Melissa currently is taking courses in preparation for her Customs Broker licensing examination. She cited major growth in Q-Lab’s international customer base, as well as the company’s expansion of product categories with customers in India and the Far East, as trends that keep her job interesting every day and make the extra time she spends studying for the exam worthwhile. 5 RepresentativeProfile Will Your Products Last? South African Firm Gains Success Through Teamwork and Local Investment Apollo Scientific’s sales staff at the 2007 Lab Africa trade show. The firm is known for its dynamic sales and marketing efforts, as well as its strong support for the South African business community. ASTM D5894 Weathering & Corrosion Improve correlation to outdoor results by using the QUV Accelerated Weathering Tester and Q-Fog Cyclic Corrosion Tester as specified in ASTM D5894 Like the ancient Greek god Apollo, Q-Lab’s South African representative, Apollo Scientific, is multi-talented. The firm’s leadership in business, investment, training and marketing – in a part of the world where positive change is urgently needed – consistently earns recognition at home and abroad. Apollo Scientific was founded in 1998 by Craig and Nicki Blignaut and Dion Keet, who currently hold the positions of Sales/Marketing Director, Administrative Director and Technical Director, respectively. Their aim was to supply quality laboratory instrumentation coupled with unequalled service and after-sales support in southern Africa. The firm represents 10 different product lines (including familiar companies such as Instron, Binder, and Erweka). Apollo became a Q-Lab representative in 2002. Offices in the four major cities of South Africa include new headquarters in Johannesburg and branches in Port Elizabeth, Cape Town, and Durban. continuous learning and teambuilding activities, staff members work together to provide customers with the highest quality products and services. Their slogan states this objective: “As Precise As It Gets”. Apollo’s focus on increasing the region’s scientific knowledge, and investing in infrastructure and trained personnel, has created an impact extending beyond its four offices and 40 employees. They regularly participate in South African business events, use local services to create highly visible marketing campaigns, maintain memberships in regional business associations, and regularly advertise in the country’s publications. The firm is especially proud of its Broad-Based Black Economic Empowerment rating. Apollo has an ISO 17025 accredited laboratory and is certified by the South African National Accreditation System to calibrate instruments dealing with force, speed, displacement, and temperature. The Most Trusted Name in Weathering www.q-lab.com For QUV information, circle 200 For Q-Fog information, circle 401 6 Q-Lab Corporation’s Sales Director Ron Roberts cited Apollo’s strong commitment to marketing, training, and community as the basis for its excellent customer service and respected position in the marketplace. Through Sales/Marketing Director Craig Blignaut “South Africa is entering its 13th year of democracy,” said Craig Blignaut. “There are many challenges, but many more opportunities. We are uniquely positioned to capitalize on the growth of industry throughout South Africa. We have the geographical coverage and top-notch people and skills. As South Africa’s industry grows, so does Apollo.” To learn more, visit www.apollosci.co.za. Q-Lab Corporation ASTM D7356 Upcoming Weathering Education Events After five years of correlation research, the BASF and Q-Lab accelerated acid etch test method was recognized by the ASTM in 2007 as ASTM D7356, Test Method for Accelerated Acid Etch Weathering of Automotive Clearcoats Using a Xenon Arc Exposure Device. Q-Lab announces two dates and locations for its Weathering 101 – The Basics of Weathering & Light Stability seminar. The one-day educational events will be held Thursday, March 13 at Q-Lab’s headquarters facility near Cleveland, Ohio, and Wednesday, April 23 in Los Angeles, California. For more information, circle 732 Weathering 101 provides general information and instruction on using natural and laboratory exposure techniques. The seminar is useful for those involved in research and development, quality control, or with responsibilities for analyzing test results. Societies&Standards John Boisseau of BASF spoke about accelerated acid etch test research and ASTM D7356 at Q-Lab’s Automotive Weathering Symposium last October in Detroit. ISO TC 38/SCI Textiles Several Q-Lab representatives participated with representatives from 10 countries in the ISO TC 38/SCI Textiles meeting in Las Vegas last July. The WG1 Light & Weathering Working Group discussed standards affecting the textile industry, hearing arguments for changing ISO 105 B02 from a hardware based to a performance based method. Raymond Ramrajkar (left), representing the Bureau of Indian Standards, shares a moment between meetings of the ISO textile group in Las Vegas with Patrick Brennan, a U.S. delegate from Q-Lab Corporation. For registration information, contact Marilee Husband or Linda Turney at 440-835-8700, or email info@q-lab.com. Patrick Brennan from Q-Lab will lead a six-country group performing additional testing and standard drafting for possible revisions in ISO/DIS-B10. JustAsk Q-Lab Translates into “Quality” in Any Language LabNotes is published electronically in Chinese, Spanish and Portuguese, as well as English. Contact labnotes@q-lab.com to subscribe. Shown below are two examples of literature recently printed in multiple languages. Use the Free Information Form on page 8, or email your request to info@q-lab.com. Sonnenlicht, Bewitterung & Lichtechtheit UV Region Visible Region Summer Sunlight Das Sonnenlicht ändert sich jedoch im Laufe des Tages. Außerdem variiert es je nach Jahreszeit. Das Diagramm auf der rechten Seite zeigt die spektrale Energieverteilung (SEV) am Mittag im Vergleich von Sommersonnenlicht zu Wintersonnenlicht. Wie zu erkennen ist, gibt es signifikante Unterschiede hinsichtlich Intensität und Spektrum des Sonnenlichts. Am deutlichsten ist der Rückgang der kurzwelligen UV-Strahlung in den Wintermonaten. UV-A UV-C Equinox UV-B Irradiance (W/m2/nm) 1.5 Die spektrale Empfindlichkeit variiert von Material zu Material. Für haltbare Materialien wie die meisten Beschichtungen und Kunststoffe ist kurzwellige UV-Strahlung die Hauptursache für den Abbau von Polymeren. Für weniger beständige Materialien (zum Beispiel viele Farbstoffe und Pigmente) kann hingegen auch längerwellige UV-Strahlung und sogar kurzwelliges sichtbares Licht zu erheblichen Schäden führen. Justin Kowallek Joins U.S. Sales Justin Kowallek has joined Q-Lab as a Sales Representative serving the U.S. and Canadian markets. He is based at the company’s headquarters in Cleveland, Ohio. Il Nuovo Standard per Test di Solidità alla Luce 2.0 Sonnenlicht ist die Hauptursache für Schäden an vielen Kunststoffen, Textilien, Beschichtungen und sonstigen organischen Materialien. Temperatur und Feuchtigkeit sind zwar wichtige Faktoren für die Degeneration einiger unter Wettereinfluss stehender Produkte, doch im Mittelpunkt dieser Präsentation steht Sonnenstrahlung. Q-Lab’s educational seminars are held in many locations around the world. In addition to these group seminars, on-site training is offered at customers’ own facilities. 1.0 Winter Sunlight 0.5 Schnellbewitterung Für schnelle und reproduzierbare Tests werden seit Jahren Kurzbewitterungs- und Lichtechtheits-Prüfgeräte in Forschung, Qualitätssicherung und Materialfreigabe eingesetzt. Kurzbewitterungsgeräte verwenden unterschiedliche Strahlungsquellen um die realen Umweltbedingungen von Materialen beschleunigt zu simulieren. Fluoreszierende UV- und Xenonbogen-Lampen sind dafür heutzutage in der Industrie üblich. Eine ausführliche Diskussion über Strahlungsquellen in Kurzbewitterungsgeräten finden Sie in den Technischen Mitteilungen von Q-Lab LU-8160, A Choice of Lamps, und LX-5060, A Choice of Filters. 0.0 250 300 350 400 450 500 550 600 650 Xenon Tester per Solidità alla Luce 700 Wavelength (nm) Modello B02 Natürliche Sonnenlichtspektren QUV-Spektren Spektren des Q-Sun-Xenonbogens Das Sonnenlicht lässt sich in UV-Strahlung (UV), sichtbares Licht (VIS) und InfrarotStrahlung (IR) einteilen. UV ist Strahlung mit Wellenlängen kürzer als 400 Nanometer (nm). Das sichtbare Licht setzt sich aus Wellenlängen zwischen 400 und 760 nm zusammen. Mit IR bezeichnet man Strahlung jenseits des sichtbaren roten Lichts im Wellenlängenbereich von etwa 760 nm bis 1 mm. Das QUV-Schnellbewitterungsgerät simuliert den UV-Anteil des natürlichen Sonnenlichts. Diese Methode ist sehr wirksam, da kurzwelliges UV für fast alle wetterbedingten Schäden an beständigen Materialien verantwortlich ist. Es stehen unterschiedliche Lampen zur Verfügung. Die Wahl des Lampentyps richtet sich nach dem Anwendungszweck. Der Vollspektrum-Xenonbogen reproduziert das gesamte Sonnenlichtspektrum einschließlich Ultraviolett-Strahlung (UV), sichtbarem Licht (VIS) und Infrarot-Strahlung (IR). Mit seiner Hilfe können sowohl durch kurzwellige UV-Strahlen verursachte Schäden als auch solche bei höheren Wellenlängen, wie Ausbleichen und Farbänderungen, simuliert werden. Die Kombination von Xenonbogen und speziellen optischen Filtern ermöglicht, unerwünschte UV-Bereiche herauszufiltern und das gewünschte Spektrum zu erzielen. Es gibt drei allgemeine Filterkategorien. Die Wahl des optischen Filters hängt vom geprüften Material und von der Endanwendung ab. Sonnenlicht im Laufe des Tages QUV UVA-340 und Sonnenstrahlung Q-Sun Tageslicht und Filter vom Typ Extended UV 300 325 Wavelength 350 (nm) 375 400 Die Lampen des Typs UVB-313 nutzen kurzwellige UV-Strahlen zur maximalen Beschleunigung und sind besonders geeignet zum Testen extrem haltbarer Materialien oder für Anwendungen in Qualitätskontrolle, Entwicklung und Forschung. Allerdings kann die Emission kurzwelliger Strahlung unterhalb der Grenzwellenlänge terrestrischer solarer Strahlung insbesondere hinsichtlich der Farbechtheit zu anomalen Ergebnissen führen. Irradiance (W/m2/nm) Kitt Peak Cleveland 1.0 Miami 0.5 Miami, Florida: Altitude- 4 m, Latitude- 25˚ 47'N Cleveland, Ohio: Altitude- 241 m, Latitude- 41˚ 30'N Kitt Peak, Arizona: Altitude- 2096 m, Latitude- 31˚ 58'N 0.0 250 300 350 400 450 500 550 Wavelength (nm) 600 650 700 Solar-Eye sorgt für eine konstante Bestrahlungsstärke auf den Proben. Eine Bestrahlungsstärke von 0,68 W/m2/nm bei 340 nm entspricht z.B. der Intensität von Mittagssonnenlicht im Sommer. Darüber hinaus sind auch höhere Bestrahlungsstärken zur weiteren Beschleunigung der Ergebnisse einstellbar. Direct Sunlight 0.8 Sunlight Through Window Glass 275 300 325 350 Wavelength (nm) 375 400 0.6 QUV und Xenonbogen basieren auf unterschiedlichen Ansätzen. Mit Hilfe der XenonbogenStrahlung wird im Wesentlichen versucht, das gesamte Sonnenspektrum (einschließlich UV, VIS und IR) zu reproduzieren. Unerwünschte Nebeneffekte sind höherer elektrischer Verbrauch und überhöhte Wärme(IR)-Strahlung. 3.0 1.6 1.4 300 325 350 Wavelength (nm) 375 UVA-340 at Maximum Irradiance Direct Sunlight 350 400 450 500 550 Wavelength (nm) 600 650 700 Italian, circle 733-I German, circle 733-G 1.4 1.2 0.6 1.0 Daylight - B/B 0.8 0.6 0.4 Extended UV - Q/B Direct Sunlight 300 325 350 Wavelength (nm) 375 Fensterglasfilter im UV-Bereich Dieses Diagramm zeigt die Wirkung der Fensterglasfilter im UV-Bereich. Kleine Unterschiede in der spektralen Grenzwellenlänge können große Unterschiede Im Polymerabbau hervorrufen. Auf Farbänderungen von Farbstoffen und Pigmenten sollten sich diese Unterschiede jedoch nicht auswirken. 2.0 1.5 QUV with UVA-340 1.0 400 Window - Q Window - B/SL Sunlight Through Window Glass 300 350 Window - IR 400 450 500 550 Wavelength (nm) 600 650 700 1.4 1.2 1.0 Direct Sunlight 0.8 Window - Q 0.6 0.4 0.2 0.0 250 275 300 325 350 Wavelength (nm) Sunlight Through Window Glass Window - IR 375 400 Sunlight, Weathering & Light Stability (SPD) wall poster www.q-lab.com Q-Lab Europe Ltd. Express Trading Estate Farnworth Bolton BL4 9TP England Tel: +44 (0) 1204 861616 Fax: +44 (0) 1204 861617 Q-Lab China 美国Q-Lab公司中国代表处 中国上海浦东新区商城路618号 良友大厦1809室 200120 电话: +86-21-5879-7970 传真: +86-21-5879-7960 Q-Lab Florida 1005 SW 18th Ave. Homestead, FL 33034 U.S.A. Tel: +1-305-245-5600 Fax: +1-305-245-5656 Q-Lab Arizona 24742 W. Durango St. Buckeye, AZ 85326 U.S.A. Tel: +1-623-386-5140 Fax: +1-623-386-5143 Basierend auf LU-0822, Sunlight, Weathering and Light Stability (Sonnenlicht, Bewitterung und Lichtbeständigkeit) von Q-Lab Corporation. Q-Panel, QUV, Q-Lab, Q-Sun, Q-Trac and Solar Eye sind Handelsmarken der Q-Lab Corporation. LW-6016-GR © 2007 Q-Lab Corporation Technische Änderungen vorbehalten. Chinese, contact Q-Lab China English, circle 733 Direct Sunlight Window - B/SL Das QUV dagegen reproduDirect Sunlight ziert lediglich den UV-Anteil 0.0 des Sonnenspektrums und 250 335 420 505 590 675 760 845 930 1015 1100 demzufolge nur dessen phoWavelength (nm) tochemische Effekte. Diese Methode ist sehr wirksam, da die kurzwellige UV-Strahlung für fast alle witterungsbedingten Schäden an beständigen Materialien verantwortlich ist. Allerdings liefert sie aufgrund des begrenzten Spektrums nicht immer zutreffende Resultate in Bezug auf die Farbechtheit. Eine ausführliche Behandlung dieses Themas finden Sie im Q-Lab Technical Bulletin LU-8009. 375 3.0 2.0 0.0 250 400 Xenon Arc with Daylight Filters 300 325 350 Wavelength (nm) 1.5 0.5 UVA-340 at Normal Irradiance 275 Daylight - Q 275 2.5 0.4 0.5 300 0.0 250 Die Kombination Xenonbogen mit Fensterglasfilter erzeugt ein Spektrum, das dem Sonnenlicht hinter Fensterglas entspricht. Diese Strahlung wird zum Prüfen der meisten Innenmaterialien empfohlen. Direct Sunlight 1.2 1.0 1.0 Extended UV - Q/B 0.0 250 Q-SunFensterglasfilter 1.0 2.5 2.0 1.5 0.5 400 0.8 3.0 Q-Sun Model B02 brochure Daylight - B/B Daylight - Q 2.5 0.2 275 1.8 QUV, Xenonbogen und Sonnenlicht Irradiance (W/m2/nm) Das Diagramm zeigt den UV-Bereich dieser Filter. Man sieht den Unterschied in der kurzwelligen Flanke. Auf Grund der hohen Photonen-Energie können kleine Unterschiede in der Grenzwellenlänge große Unterschiede im Polymerabbau hervorrufen. 0.4 0.0 250 12.0 Die Spektren von Tageslichtfiltern entsprechen der direkten Einstrahlung von Mittagssonnenlicht im Sommer und weisen eine gute Annäherung an die Grenzwellenlänge der Sonne auf. Sie werden zum Testen von Außenmaterialien empfohlen. Extended UV-Filter sind dagegen durchlässig für kurzwellige UV-Strahlen unterhalb der terrestrischen solaren Grenzwellenlänge. Sie werden für einige Prüfverfahren in der Automobilindustrie vorgeschrieben. Tageslicht und Extended UV-Filter im UV-Bereich 1.0 0.2 Q-Lab Corporation Q-Lab Headquarters & Instruments Division 800 Canterbury Road Cleveland, Ohio 44145 U.S.A. Tel: +1-440-835-8700 Fax: +1-440-835-8738 375 0.2 400 Der Q-Trac Natural Sun10.0 light Concentrator ist ein Q-Trac Gerät zur beschleunigten Freibewitterung, das als 8.0 Strahlungsquelle natürliches Sonnenlicht verwendet. Mit Hilfe von zehn 6.0 Spiegeln reflektiert Q-Trac das vollständige Spektrum 4.0 natürlichen Sonnenlichts in konzentrierter Form auf die Direct Sunlight Prüflinge. Darüber hinaus 2.0 folgt er von morgens bis abends automatisch dem 0.0 Lauf der Sonne. Dieses 250 300 350 400 450 500 550 600 650 700 System zur Konzentration Wavelength (nm) des Sonnenlichts maximiert die Menge des auf den Prüfling gestrahlten Sonnenlichts und kann im Jahr durchschnittlich die fünffache Menge der gesamten UV-Bestrahlung (295-385 nm) eines typischen Jahrs in Florida produzieren. Einzelheiten hierzu finden Sie im Q-Lab Technical Bulletin LL-9031. LW_6016_GR_B.indd 1 300 325 350 Wavelength (nm) 0.8 0.0 250 Sunlight Through Automotive Glass 0.2 0.0 250 UVA-340 275 1.2 Irradiance (W/m2/nm) Irradiance (W/m2/nm) 1.2 1.0 0.4 0.4 0.0 250 Bestrahlungsregelsystem Solar Eye 0.6 Direct Sunlight 0.8 0.6 0.2 Irradiance (W/m2/nm) Q-Trac & Sonnenlicht 1.2 1.0 QUV UVB-313 und Sonnenstrahlung 2.0 1.5 Fensterglas Glas ist durchlässig für sichtbares Licht, filtert aber einen Großteil der UV-Strahlung heraus. Je kürzer die Wellenlänge, desto größer der Filtereffekt. UV-Strahlen unterhalb von 310 nm werden durch normales Fensterglas vollständig gefiltert. Die Durchlässigkeit variiert je nach Dicke, Farbe, chemischer Zusammensetzung usw. Das bedeutet, dickeres, getöntes oder beschichtetes Glas absorbiert den größten Anteil des kurzwelligen UV. Lampentyp UVA-340 liefert die beste verfügbare Simulation von natürlichem Sonnenlicht, da sein Licht im Bereich von 365 nm bis hinab zur Grenzwellenlänge terrestrischer solarer Strahlung dem Mittagssonnenlicht im Sommer entspricht. Die Fluoreszenzlampe UVA-340 wurde entwickelt, um die Korrelation in den entsprechenden Prüfgeräten zu verbessern, und wird für Untersuchungen empfohlen, bei denen die Korrelation ein entscheidender Faktor ist. Irradiance (W/m2/nm) Sonnenlicht an verschiedenen Orten 6:00 PM (cloudy) 275 Irradiance (W/m2/nm) 5:00 PM 5:00 AM 0.1 Irradiance (W/m2/nm) 6:00 AM 0.4 0.2 Irradiance (W/m2/nm) 0.6 0.5 0.0 250 Trotz der immanenten Variabilität der solaren UV-Strahlung zeigen Messungen zum Zeitpunkt der Sommersonnenwende erstaunlich geringe Abweichungen an verschiedenen Orten und sind demnach unabhängig von geographischer Länge und Breite. 7:00 AM 0.7 Irradiance (W/m2/nm) 0.9 0.3 Irradiance (W/m2/nm) 1.0 0.8 Irradiance (W/m2/nm) Aufgrund des Filtereffekts der Erdatmosphäre variieren Quantität und Qualität des Sonnenlichts vom Sonnenaufgang bis -untergang deutlich. Dieses Diagramm zeigt, wie sich der UV-Anteil des Sonnenlichts im Laufe des Tages ändert. Die Daten wurden zur Sommersonnenwende in Ohio, USA, gemessen. Solar Noon 11:00 AM 1:00 PM 10:00 AM 2:00 PM The Most Trusted Name in Weathering 10/9/07 12:30:31 PM German, circle 108-G English, circle 108 Contact Q-Lab China at info@q-lab.com.cn for all Q-Lab publications available in Chinese, including LabNotes. See page 8 for additional contact information. The Most Trusted Name in Weathering Justin previously worked for CEC Combustion Services Group, where he was responsible for client relationship management, sales training and support, parts management, as well as various marketing functions. He is a graduate of Baldwin-Wallace College. 7 Issue 1 – 2008 Q-Lab Corporation INFORMATION ON Weathering, LIGHT STABILITY AND CORROSION Testing In this Issue: • SAE Cancels J1960 and J1885 • Chrysler Approves Q-Sun for Automotive Testing • How Can I Tell If My Product Will Last Outdoors? News and Information from Q-Lab Q-Lab Corporation Q-Lab Headquarters & Instruments Division 800 Canterbury Road Westlake, OH USA Tel. +1-440-835-8700 Fax +1-440-835-8738 FREE INFORMATION Issue 1 - 2008 Email your request, or circle the number(s) below and fax or mail this form to our headquarters office (USA) or Q-Lab Europe. Contact Q-Lab China for information in Chinese. Q-Lab (USA): info@q-lab.com Fax +1-440-835-8738 Q-Lab Europe: info.eu@q-lab.com Fax +44 (0) 1204-861617 502 Q-Panel Brand Test Substrates Weathering Research Service 108 108-G SPD Wall Poster (German) 700 Q-Sun Xenon Test Chamber Q-Lab Florida 1005 SW 18th Avenue Homestead, FL USA Tel. +1-305-245-5600 Fax +1-305-245-5656 200 QUV Weathering Tester 732 Q-Lab/BASF Accelerated Acid Etch 301 Q-Lab Weathering Research Service 733 Q-Sun B02 Lightfastness Tester 319 Q-Rack Outdoor Exposure Kits 733-G Q-Sun B02 (German) 401 Q-Fog Corrosion Tester 733-I Q-Sun B02 (Italian) 735 Q-Lab/Chrysler Technical Paper Q-Lab Arizona 24742 W. Durango Street Buckeye, AZ USA Tel. +1-623-386-5140 Fax +1-623-386-5143 SPD Wall Poster Please print: Q-Lab Europe, Ltd. Express Trading Estate Stone Hill Road, Farnworth Bolton BL4 9TP England Tel. +44 (0) 1204-861616 Fax +44 (0) 1204-861617 Name ________________________________________________________________________________________ Company _____________________________________________________________________________________ Address ______________________________________________________________________________________ City___________________________________________________________________________________________ State/Province_________________________________________________________________________________ Country _______________________________________________________________________________________ 美国Q-Lab公司中国代表处 传 中国上海市共和新路3388号永鼎大厦1001室 邮编:200436 电话:+86-21-58797970, +86-21-56030380 传真:+86-21-58797960 Zip or Postal Code _____________________________________________________________________________ Telephone _____________________________________________________________________________________ Fax ___________________________________________________________________________________________ Email _________________________________________________________________________________________ Industry _______________________________________________________________________________________ www.q-lab.com Product _______________________________________________________________________________________ Q-Panel, QUV, Q-Lab, Q-Sun, Q-Fog, and Solar Eye are trademarks of Q-Lab Corporation. © 2008 Q-Lab Corporation