Improving the productivity of your chemistry

Transcription

Radleys Product Guide Vol5 V4:Hotplate & Overhead Update
10/6/09
11:44
Page 1
innovations for chemistry
Improving the
productivity
of your
chemistry
Innovative tools
for synthesis,
process development,
work-up, purification
and evaporation...
Summer 2009
Product Guide - Vol 5
www.radleys.com
www.radleys.co.uk www.lara-clr.com
NEW Carousel Stirring Hotplates
Carousel stirring hotplates feature 800 Watt heating power,
chemically resistant top plates and are available in three
models to suit your chemistry and budget.
Common Features...
• 800 Watt heating power.
• Hotplate temperature range: 20 - 300°C.
• Speed range: 100 - 1400rpm.
• Chemically resistant Kera-Disk top plate coating.
• 135mm Top plate diameter: 135mm.
Includes
3 YEAR
Warranty
Carousel
Standard
Carousel
Tech
Carousel Temperature
Controller
Carousel
Advanced
Carousel Standard
Speed, max (rpm)
Speed accuracy (%)
Display
Analogue/digital interface
Heating power (W)
Hotplate temperature (˚C)
Medium temperature, max. (˚C)
Accuracy temperature setting (K)
External temperature sensor
Temperature accuracy with external
temperature sensor (K)
Sensor breakage protection
Temperature control
Temperature accuracy hotplate (K)
Safety circuit hotplate (˚C)
Stirring capacity, max (H20)
Load, max (kg)
Power consumption (W)
Ambient temperature range (˚C)
Max. relative humidity (%)
Max. permitted operation (%)
Plate diameter (mm)
Plate material
Weight (kg)
Dimension l x w x h (mm)
Protection class
2
10/6/09
Supply voltage
11:44
Page 2
Carousel Standard Stirring Hotplate...
• Extra safety control circuit and hotplate cut-out by two independent temperature sensors.
• An independent safety circuit with separate circuit switches off
the heating if the set hotplate temperature is exceeded by 25°C.
• Illuminated switch for actual heating condition.
• Connector for electronic temperature control via optional
Carousel Temperature Controller.
• Accuracy temperature setting: ± 1 K with Temp. Controller.
• Solution control accuracy: ± 1 K with Temp. Controller.
• Triac guarantees long service life. Electronic current limiting to
protect the motor.
Carousel Tech Stirring Hotplate...
All of the above features, plus:
• Digital display for speed and temperature (set and actual).
Carousel Advanced Stirring Hotplate...
All of the above features, plus:
• RS232 interface for optional PC control.
• Speed range: 30 - 1400rpm (Superior speed accuracy: ± 1 %).
• Optional Pt 1000 temperature sensor: with ± 0.2 K accuracy.
• Optional Pt 1000 temperature sensor are available with
stainless steel or glass coated probe.
• External sensor control, if sensor is not being dipped in the
medium, heating is switched off.
• Independent safety circuit switches off the heating if a prefixed
temperature difference (∆T) above set temperature is reached.
• Accuracy temperature setting: ± 1 K.
• Hotplate residual heat indicator in the digital display lights when
unit is turned off and the hotplate temperature is >50 °C.
Carousel Temperature Controller...
• Fuzzy logic microprocessor control ensures fast heating with
no temperature overshoot.
• Digital display for set and actual temperature.
• Control range: ambient temperature to +300 °C.
• Displays every temperature between -50°C and +300°C
(Control accuracy: ± 1 K).
• Max. button displays the safety temperature at which the item
automatically is switched off.
• In case the temperature sensor has no contact with the
medium, heating is switched off.
• Alternatives with stainless steel or glass coated probe.
• Comes with 13mm x 340mm support rod (and support rod
hotplate adapter).
Carousel Tech
1400
±2
800 *
20 - 300
250
±5
Controller
1400
±2
Digital
800 *
20 - 300
250
±1
Controller
With Carousel
Temperature Controller
Electronic
±5
25˚C over hotplate
temperature
20
25
820
0 - 40
80
100
ø 135
Silumin with ceramic coating
2.9
173 x 277 x 94
IP 32
230 V/ 50 Hz
115 V/ 60 Hz
With Carousel
Temperature Controller
Electronic
±5
25˚C over hotplate
temperature
20
25
820
0 - 40
80
100
ø 135
2.6
173 x 277 x 94
IP 32
230 V/ 50 Hz
115 V/ 60 Hz
±1
±1
Radleys, Shire Hill, Saffron Walden, Essex CB11 3AZ. United Kingdom
Carousel Advanced
1400
±1
Digital
Yes
800 *
20 - 300
250
±1
Pt 1000
± 0.2
With Pt 1000
Microprocessor
±5
10˚C - 25˚C over nominal
temperature
20
25
825
0 - 40
80
100
ø 135
2.6
173 x 277 x 94
IP 32
230 V/ 50 Hz
115 V/ 60 Hz
10/6/09
11:45
Page 3
NEW Cool-It™ Insulated Bowls
The safe and efficient way of cooling and stirring round bottom flasks to -78˚C.
Cool-It replaces fragile glass dewars, unstable plastic bowls and keeps your chemistry
colder for longer.
The compact and virtually unbreakable Cool-It insulated bowls are designed to fit onto a standard
stirring hotplate to cool and stir round bottom flasks, beakers, test tubes etc.
Cool-It keeps it cooler for longer...
The excellent design and insulation qualities of the Cool-It bowls keep your sample cooler for longer.
• Compared to a standard non-insulated plastic bowl Cool-It will keep your sample below -70°C
for up to 5 times longer.
• Compared to a glass dewar Cool-It will keep your reactions below -70°C for twice as long.
Optional lid increases cooling time by 20%...
Cool-It bowls come with a unique two piece lid, which is easily fitted once
your flask is in place. Using the lid can keep your reaction cool for up to 20%
longer, minimises condensation and ice formation on your flask (maintaining
visibility of the contents) and prevents spitting from the cooling mixture.
Unbreakable...
Cool-It bowls are manufactured from a robust, chemically resistant HDPE casing encapsulating
a high quality insulated foam core. The combination of tough composite materials not only provides
excellent insulation but is also durable, and unlike fragile glass dewars, Cool-It is virtually unbreakable if dropped.
Easy pour spout and handle...
Cool-It’s unique non-drip spout and ergonomically designed handle makes the disposal of waste
solvents much safer and easier than with a standard dewar or bowl; avoiding accidental spillages
and creating a safer working environment.
Large and small bowl options...
Cool-It is available in two sizes of bowl. The small Cool-It bowl is suitable for flasks up to 400ml,
and large Cool-It bowl for flasks up to 2 Litres. Both sizes have their own dedicated lid.
Protects your stirrer and minimises spills...
As well as insulating your reaction, Cool-It minimises condensation on the outer surfaces, protecting
your stirrer from frost and moisture ingress. It is also designed to fit securely onto the top plate
minimising accidental spills and the risk of the bowl being knocked off the top plate.
Small Cool-It bowl for flasks up to 400ml
Cool-It fits on to all popular brands of stirring hotplate...
Cool-It bowls are suitable for use with all stirring hotplates with a circular top plate up to 145mm in
diameter (e.g. Heidolph, Radleys). For stirring hotplates with 135mm ø top plates (e.g. IKA, Eyela,
Radleys etc) an optional top plate adapter is available if required.
Cool-It accessories...
A useful range of accessories are available including, clamp, stand, stirring hotplate, digital
thermometer, scoop, protective gloves, apron and face shield.
Cool-It vs Glass Dewar
Large Cool-It bowl for flasks up to 2 litres
Cool-It accepts all
shapes and sizes
of round bottom
and florentine flask
up to 2 litres...
Flask Contents - Temp ˚C
Acetone & Dry Ice, 250ml flask, 100ml acetone
Time Minutes
Easy pour
design with spout
and handle
Tel: +44-1799-513320 Fax: +44-1799-513283 Email: sales@radleys.co.uk www.radleys.com
3
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Page 4
StarFish™ Multi-Experiment Work Station
StarFish
applications...
StarFish is a modular, general purpose heating and stirring work station.
• Stirring
Designed to fit on all leading brands of stirring hotplate and
accepts a wide range of standard glassware, including;
vials, test tubes, beakers and round-bottomed flasks.
• Heating
• Synthesis
Whether you just want to heat and stir, or perform more complex
experiments, StarFish really can make your life easier and improve
the productivity of your lab.
• Concentration
• Extraction
•
•
•
•
• Distillation
• Digestion
•
StarFish advantages...
• Increased Productivity...
Heat and stir experiments in parallel for
improved productivity.
• Safer, cleaner working...
Eliminates the need for oil baths, reducing
spills and accidents.
• Compact...
•
•
•
Set-up vessels individually or in parallel.
Powerful stirring and rapid heating of all positions equally.
Universal 3 and 5-way clamps will hold a variety of glassware.
Water Distribution Manifolds - distribute cooling water
to up to five separate condensers, simultaneously.
Gas/Vacuum Distribution Manifolds - allow gas or
a vacuum from a single source to be evenly distributed
to up to five positions or vessels.
MonoBlocks - single blocks with multiple wells of the same size.
PolyBlocks - 5 per system, mix‘n’match any combination of vessel.
Custom blocks - if you don’t see what you want we can make it for you.
Larger
test tubes
Vials of all
sizes
Small test
tubes
Uses less space than multiple heating
and stirring set-ups.
• Money saving...
Cheaper than using multiple stirrers,
hotplates, heating mantles or oil baths.
Also allows you to use your existing
stirring hotplate and glassware.
• True versatility...
Accommodates a wider range of vessel
types and accessory glassware than any
other system. Use it for one application
today and a different one tomorrow.
• Simple set-up...
Unique clamp and distribution manifolds
mean less tubing, clamping and easier
to set-up.
Universal 3 & 5-way clamps...
The StarFish clamps allow you to hold glassware of
virtually any size, and come with a choice
of Velcro or rubber straps. Using different straps
on separate clamps allows you to grip the
flask with rubber straps for
lifting, whilst the condenser
above slides through
the Velcro strap.
• More flexible...
Use as many/few positions as you want.
>>
• Easy to use....
Simple design means it is easy to use
and quick to assemble or disassemble.
Requires minimal training to operate.
>>
>>
Use the StarFish components to build the system you want...
Water and
Gas/Vacuum
Distribution Manifolds
Base Plate with optional handles
accepts both MonoBlocks
and PolyBlocks
Universal 3 and
5-way Clamps
4
Wide choice
of PolyBlocks
MonoBlocks for
3 or 5 round
bottom flasks
10/6/09
11:45
Page 5
Heat-On™ Block System
Simply the safest, fastest, most efficient way to heat and stir a round
bottom flask from 10ml to 5 litres.
Replace messy oil baths, heating mantles, avoid spills and make your chemistry safer,
cleaner and faster.
It is accepted that oil baths and heating mantles are no longer the preferred choice of chemists to heat
round bottom flasks. The risk of oil fires and injury from hot oil spills, plus the mess associated with the
use of oil means that oil baths no longer represent safe working practice in labs. Heating mantles are
expensive, difficult to clean, do not respond well to spills and often create hot spots when heating.
Therefore scientists are increasingly turning to specially designed aluminium blocks located on stirring
hotplates to heat standard round bottom flasks.
• All Heat-On blocks are manufactured from solid aluminium providing excellent, even heat transfer
to the entire block, preventing hot spots.
• Heat-On’s weight-saving design reduces the mass of the block to be heated, making the heat-up
times significantly faster. This weight-saving design also offers faster post synthesis cool down times.
• Heat-On blocks feature a proprietary well design that eliminates cracking of flasks. This unique
design allows the blocks to have deeper wells, maximising the heated surface area to improve
heat-up times and minimising the differential between the block and solution temperature.
• Heat-On blocks have two probe holes for insertion of temperature probe/s.
• Removable lifting handles ensure safe and rapid removal of the blocks from the heat source.
• Blocks can be used up to 200˚C and 260˚C for short periods.
Heat-On accepts 10ml, 25ml, 50ml,
100ml, 150ml, 250ml, 500ml,
1 litre, 2 litre, 3 litre and
5 litre round bottom
flasks...
Fluoropolymer coating gives
superb chemical resistance...
Heat-On blocks have an innovative
fluoropolymer coating that offers
outstanding chemical resistance
to most solvents, acids and alkalis.
The coating also extends the product
life, is easy-to-clean and reduces
heat-up times. Heat-On blocks are
also available as standard with a
lower cost anodised finish if
preferred.
Heat-On Multi-well Block
Holder with 50ml and 100ml
flask inserts
Not all blocks designs
are the same...
Test results show that
Heat-On heats up to 66%
faster and uses 30% less
energy than other leading
brands of block.
To see the test results, visit www.radleys.com
to download the Heat-On Application Bulletin
250ml Heat-On block
500ml Heat-On block
1 Litre Heat-On block
Heat-On for
Florentine
flasks
Blocks are
available to
accept 200ml,
300ml, 500ml,
1 litre and 2 litre
Florentine or
pear-shaped flasks.
For more information please
visit www.radleys.com
250ml Heat-On
block with hotplate
and temp. controller
500ml Heat-On
block with hotplate
and temp. controller
5 Litre Heat-On block
5
Simple & convenient, the Carousel
Work-Up Station will reduce post
synthesis bottle-necks...
10/6/09
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Page 6
NEW Carousel 12 Plus Reaction Station™
The unique patented Carousel simultaneously heats/cools, stirs and reflux’s
multiple samples under inert atmosphere.
The Carousel 12 Plus is an effective personal synthesis station for parallel solution phase
chemistry and solid supported reagent based synthesis.
The innovative Carousel 12 Plus is quick to set-up and easy to use; providing heating/cooling, stirring
and refluxing with inert gas control of 12 glass reactions tubes (1 to 20ml) simultaneously.
Whether using a single position or all 12, the Carousel is the neat and efficient way to perform your
chemistry in the most productive manner. Bringing all the benefits in productivity of parallel synthesis
to the individiual chemist at a fraction of the cost of expensive automated systems.
Use the Work-Up Station for parallel
or sequential work-up of 12 samples,
using filtration, phase separation,
liquid/liquid extraction or SPE.
• Visibility slots allow easier viewing of tube contents during experiments.
• Fluoropolymer coating for chemical resistance and easy cleaning.
• Unique removable PFA insulation plate helps insulate the heated base for faster heating and energy
savings of up to 36%.
• Chemically resistant PFA caps feature a ‘quick-thread’ for fast attachment to the glass tubes and
‘easy-on’ push connections to the stainless steel gas outlets.
• Removable reflux head allows reaction tubes to be transferred between heated base, cooled base
or stand without disconnecting the tubes.
The improved Carousel 12 Plus retains all of its popular features but with a host
of new innovations making it even better
NEW Central Quick Release inlet/outlet
er
Fluoropolym
ovides
pr
e
at
pl
insulation
g and
faster heatin
for vacuum and gas, combined with
a radial gas distribution system and
gas-tight fluoropolymer caps allow
reactions under an inert atmosphere.
gs
energy savin
of up to 36%
NEW Chemically resistant Easy-On
Heated directly by the stirring
hotplate; Digital temperature
control ±0.5˚C.
fluoropolymer caps feature a quickthread for fast attachment to the glass
tubes and push-on connections to the
stainless steel gas outlets.
Water cooled aluminium reflux head
provides efficient refluxing within
individual reaction tubes.
Quick release water couplings with cut-off
valves for ease of connection/removal of cooling
water supply to reflux/inerting head.
Provides 12 heated and stirred
glass reaction positions, with
a reaction volume of 5 to 20ml
(1ml with the reduced volume tubes).
Fluoropolymer coating for
heightened chemical resistance
and easy cleaning.
NEW Unique removable fluoropolymer
insulation plate helps insulate the heated
base for faster heating and energy
savings of up to 36%.
Easy to operate and set-up with
minimal training time. No electrical
or moving parts ensures
maintenance free operation.
NEW base design improves heat transfer
and provides energy savings. Maximum
operating temperature 180˚C
(220˚C for short periods).
NEW visibility slots allow
easier viewing of tube contents.
Easy to rotate round design gives
access to all tubes with no need
to lean into the fume cupboard.
6
Utilises the single rotating magnetic
field of the hotplate stirrer to stir all the
positions evenly and powerfully.
Carousel Stirring Hotplate offers
higher temperature, more powerful
stirring and digital control.
Rare earth cross shaped
stirring bars for more vigorous
stirring and a deeper vortex,
without jamming.
F
More
Eas
M
10/6/09
11:46
Page 7
NEW Cooled Carousel 12 Plus Reaction Station™
Upgrade your Carousel to
perform cooled chemistry...
Offering cost effective low temperature parallel synthesis from ambient
down to -78˚C.
The innovative Cooled Carousel 12 Plus reservoir is designed to accept the removable
reflux/inerting head from the Carousel 12 Plus; allowing for the reaction tubes to be easily
and rapidly transferred between heating and cooling bases.
• Simultaneously performs up to twelve cooled and stirred reactions to -78˚C, with a working volume
of 1ml to 20ml per tube.
• Fits directly on to a standard Carousel stirring hotplate and utilises the single rotating magnetic
field of the stirring hotplate to stir all the positions evenly and powerfully.
• Robust HDPE cooling reservoir is compatible with a wide range of cooling mixtures, including
dry-ice/acetone for manually controlled cooling from ambient down to -78˚C.
• Features a unique non-drip spout and ergonomically designed handle for disposal of waste solvents.
• Insulated foam core maintains low temperatures for long periods, whilst protecting the stirrer from
freezing. Also reduces condensation and ice formation on outer surfaces.
• HDPE lid keeps your reaction cooler for longer, minimises condensation and ice formation on your
tubes (maintaining visibility of the contents) and prevents spitting from the cooling mixture.
• The robust HDPE reservoir is virtually unbreakable.
Robust HDPE cooling
reservoir is compatible with
a wide range of freezing
mixtures including
dry-ice/acetone for
manually controlled cooling
from ambient to -78˚C.
Central inlet/outlet for vacuum and gas,
combined with a radial gas distribution
system and gas-tight PTFE caps, allows
Transfer the reflux/inerting head to the
Cooled Reservoir for cooling to -78˚C
PFA caps feature a ‘quick-thread’ for fast
attachment to the glass tubes and ‘easy-on’
push connections to the stainless
steel gas outlets.
Simultaneously performs up to
twelve cooled and stirred reactions
to -78˚C, with a working volume of
1ml to 20ml per tube.
Provides 12 cooled and stirred
a reaction volume of 5 to 20ml
(1ml with the reduced volume tubes)
Utilises single rotating
magnetic field of the stirrer
to stir all the positions
evenly and powerfully.
Features a unique non-drip spout
and ergonomically designed handle
for easy disposal of waste solvents.
Insulated foam core maintains low
temperatures for long periods, whilst
protecting the stirrer from freezing.
Also reduces condensation and ice
formation on outer surfaces.
Faster
nt
More efficie
se
Easier to u
Modular
The robust HDPE reservoir
is virtually unbreakable.
Carousel Stirring Hotplate offers
higher temperature, more powerful
NEW Carousel 12 Plus Stand...
The Carousel stand is designed to support
the reflux/inerting head either with
or without reaction tubes.
The heavy duty metal stand is fluoropolymer
coated for improved chemical resistance and ease
of cleaning. The integral drip tray catches any
dripping condensation from tubes and gives
excellent stability.
7
10/6/09
11:47
Page 8
Carousel 6 Reaction Station™
The Tornado IS6
facilitates powerful,
controlled mechanical
stirring of up to six
round bottomed
flasks with the
Carousel 6
Carousel 6 will increase the productivity of your chemistry. Choose from 5ml,
10ml, 25ml, 50ml, 100ml, 170ml or 250ml round bottom reaction flasks.
The Carousel 6 utilises the same technology as the popular Carousel to simultaneously stir
and heat up to six round bottomed flasks.
The Carousel 6 is designed to be used by individual chemists in their own fume cupboard. The
affordability of the Carousel 6 brings all the benefits in productivity of multiple parallel synthesis to the
chemist at a fraction of the cost of any other comparable system.
Offering unrivalled
stirring for both
viscous samples
and for the dispersion
of delicate solids
in solution...
• Wide choice of reaction flask options including 250ml Azeotropic (Dean & Stark)
• Simultaneously performs up to six heated and stirred reactions
• Fits on a standard IKA or Carousel stirring hotplate
See Page 10
PTFE cap features an all
PTFE valve, which offers superior
solvent resistance, gas tight
sealing and easy operation.
Heated directly by the stirrers hotplate;
providing an operating temperature
range from ambient to +180°C. Digital
temperature control +/- 0.5˚C.
Carousel 6
with inserts and
selection of
smaller
reaction
flasks
Round design makes all reaction
flasks visible, with no need to lean
into the fume cupboard.
Water cooled aluminium reflux
head provides efficient refluxing
within individual glass reaction flasks.
Quick-release couplings prevent water
loss during set-up/breakdown.
Central inlet/outlet for vacuum
and gas, combined with a radial gas
distribution system and gas-tight PTFE
caps allow reactions under an inert
atmosphere.
Provides six heated and stirred
glass reaction positions. Expanded range
of glass vessels includes 5ml, 10ml,
25ml, 50ml, 100ml, 170ml & 250ml
round bottom flasks, as well as
vessels with one or two sidearms.
Aluminium inserts allow easy
removal of flasks and good temperature
transfer for refluxing.
Rare earth elliptical PTFE
stirring bar provides powerful
stirring and a deep vortex.
Utilises the single rotating magnetic field
of the hotplate stirrer to stir all the
positions evenly and powerfully.
PTFE heat protection ring
helps protect user from contact
with hot base.
Round aluminium base transmits
heating evenly to all positions.
Compact size has small bench-top
footprint - easy to store.
Expanded range of aluminium
inserts now includes 5ml,
10ml and 25ml round
bottomed flask
8
Aluminium Inserts for 5ml, 10ml,
25ml, 50ml, 100ml and 170ml Flasks
5ml Reaction Flask
Reflux Tube & PTFE Cap
10ml Reaction Flask
25ml Reaction Flask
50ml Reaction Flask
50ml Flask with Sidearm
Reflux Tube & PTFE Cap Reflux Tube & PTFE Cap
100ml Reaction Flask
10/6/09
11:47
Page 9
Cooled Carousel 6 Reaction Station™
The Cooled Carousel 6 will simultaneously stir and cool up to six
5ml, 10ml, 25ml, 50ml, 100ml, 170ml or 250ml round bottomed flasks.
The Cooled Carousel 6 is designed to be used by individual chemists in their own fume
cupboard to perform chilled reactions down to -78˚C.
• Robust HDPE cooling reservoir is compatible with a wide range of freezing mixtures including dry
ice/acetone for manually controlled cooling from ambient to -78˚C.
• Insulated foam core maintains low temperatures for long periods, whilst protecting the stirrer from
freezing. Also reduces condensation and ice formation on outer surfaces.
Visit www.radleys.com
to download a PDF on
the Cooled Carousel 6
• A stainless steel central inlet/outlet for vacuum and inert gas, combined with a radial gas
distribution system and gas-tight PTFE caps allow reactions under an inert atmosphere.
• Round design makes all reaction flasks visible and allows easy addition of reagents and solvents,
with no need to lean into the fumehood.
PTFE cap features an all
PTFE valve which offers superior
solvent resistance, gas tight sealing
and easy operation.
Central inlet/outlet for vacuum and gas,
combined with a radial gas distribution
system and gas-tight PTFE caps allow
Round design makes
all reaction flasks
visible; with no need
to lean into the fume
cupboard.
Insulated foam core maintains low
temperatures for long periods, whilst
protecting the stirrer from freezing.
Also reduces condensation and ice
formation on outer surfaces.
Rare earth elliptical PTFE
stirring bar provides powerful
stirring and a deep vortex.
Utilises the single rotating
magnetic field of the hotplate
stirrer to stir all the positions
evenly and powerfully.
No electrical or moving parts
ensures maintenance free
operation. Easy to set-up with
minimal training time.
Fits on a standard Carousel
or IKA hotplate stirrer, so
utilising existing and readily
available technology.
Improved Carousel Stirring
Hotplate offers more powerful
HDPE Cooled Carousel Stand
100ml Flask with Sidearm
Cooled Carousel Cover
Reduces frost formation, maintains
temperature of cooling mixture and
reduces the risk of solvents spitting.
Provides six cooled and stirred
a range of reaction vessels.
Robust HDPE cooling reservoir is
compatible with a wide range of
freezing mixtures including
dry-ice/acetone for manually
controlled cooling from ambient
to -78˚C.
250ml Long Neck
Reaction Flask & PTFE Cap
Compact size has a small
bench-top footprint
and is easy to store.
250ml Azeotropic Reaction
Flask with Dropping Funnel
with Dropping Funnel
250ml Flask with 2 Sidearms
with Dropping Funnel
9
10/6/09
11:48
Page 10
Tornado™ Overhead Stirring System
Increase your stirring productivity by up to 600%.
The Tornado facilitates powerful, controlled mechanical stirring of up to six round bottomed
flasks with the Carousel 6 Reaction Station; offering unrivalled stirring for both
viscous samples and for the dispersion of delicate solids in solution.
to watch the Tornado Movie
or download a PDF
Choice of Stirring Shafts...
A range of PTFE stirrer shafts have been designed
specifically for the Tornado. The centrifugal stirrer
shafts will fit into any one of the 50ml, 100ml and
250ml flasks. The anchor and propeller stirrer
shafts have been specifically designed to fit in the
new wide neck flasks (see below).
• Easy to set up and use.
• Integrates with Carousel 6 to provide up to six heated (max +180°C)
and stirred reaction positions.
• Uses a single overhead stirrer to agitate up to six 250ml flasks.
• Compatible with all leading brands of mechanical overhead stirrer.
• Evenly distributes high torque to all 6 positions, with 2-speed
drive (1:1 and 2:1) means that overhead stirrers with less
power/torque can be used for high viscosity liquids.
• Stir up to 1,000rpm in low viscosity solutions.
• Maximum viscosity 10,000cps at 500rpm.
Uses a single overhead stirrer
to agitate up to six 250ml flasks
Compatible with all leading
brands of overhead stirrer
Heated directly by the stirrers
hotplate; Digital temperature
control ±0.5˚C
Expanded range of glass vessels...
In addition to accepting a range of Carousel 6
glassware from 50ml to 250ml, the Tornado also
has a new range of dedicated vessels with baffles,
wide necks and azeotropic (Dean & Stark).
These wide neck vessels facilitate better mixing,
easier removal of viscous samples and the
accommodation of a variety of larger stirrer blades.
Baffles are popular with many chemists because
they improve stirring by disrupting the creation of
a vortex. Just some of these vessel options are
shown below.
Tool-free ‘Pinch-Grip’ mechanism
and sealed stirrer sealing system
allows easy stirrer shaft insertion
and operation under an inert
atmosphere
10
100ml with
sidearm
100ml with
sidearm & baffles
Provides up to six heated
(max +180˚C) and stirred
reaction positions
250ml with
sidearm
Easy to operate and set-up
with minimal training time
2-speed drive (1:1 and 2:1) means
lower rated mechanical stirrers can be
used for high viscosity liquids. Speeds
of up to 1,000rpm are achievable
in a low viscosity solutions
Integral polycarbonate
safety guard
Individual
vessels can be
removed easily
100ml vessels with two sidearms, baffles,
dropping funnel and stirrer seal
Fits
onto the
Carousel 6
without
the need
for tools
Integrates with
existing Carousel 6
without increasing
footprint
Accommodates 50ml, 100ml and
250ml round bottomed flasks
(with and without sidearms)
plus new baffled flasks
Fits on a standard Carousel or IKA
stirring hotplate, utilising powerful
600 Watt heating
Support stand gives
added stability
10/6/09
11:48
Page 11
Carousel Work-Up Station™
Simple and convenient, the Carousel Work-Up Station will reduce post
synthesis bottle-necks.
The Carousel Work-Up Station accepts up to 12 x 70ml columns loaded into one of two identical
stackable racks. The lower rack supports 12 corresponding Carousel Reaction Tubes or standard
1 inch boiling tubes for subsequent sample collection.
The Carousel Work-Up Station facilitates parallel or sequential
work-up of up to 12 samples, using filtration, phase separation,
liquid/liquid extraction or SPE techniques.
Use under gravity
or with the SpeediFlow
Booster, which allows
pressurisation of individual
columns to increase flow
rates and speed
up your work-ups.
to download a PDF on the
Carousel Work-Up Station
Aluminium racks are exceptionally
stable, with good access and
visibility of all columns and tubes.
Each position is numbered 1 to 12 for
ease of identification. The racks will
only locate in one orientation.
An optional 3rd rack can be
stacked above the 2nd rack for
sequential work-up.
Accepts 70ml columns;
including 20µm Filtration, Phase
Separation, Liquid/liquid
Extraction, Silica, SCX,
Aminopropyl and SAX Acetate.
Unique design uses no taps, valves
or drip needles, making assembly and
operation fast and simple. Minimising
cleaning time and consumable costs.
Identical racks lock together
for ease of operation or
transportation from location
to location.
Vacuum free operation makes
removal of collections tubes easy,
prevents drying of columns and
reduces the risk of bumping.
Accepts 12 x Carousel Reaction Tubes
or standard 1 inch boiling tubes.
Ergonomically designed,
lightweight aluminium racks
are easy to load with collection
tubes or work-up columns.
The unique Carousel Work-Up
Station is the perfect tool for
rapid parallel work-up
post synthesis
Removal of adapters
is simple...
Pull out the locking pin,
release the handle...
To locate a second rack on top
of the first, pull out the spring
loaded knob and rotate 90˚.
...and the adapter can
be easily pulled out.
SpeediFlow Adapters
The SpeediFlow now includes
an expanded range of optional
adapters to fit a wide range
of standard column sizes...
150ml
Whatman
AutoCup®
70ml
25ml
15ml
Removable adapters are now
available for use with 15ml, 25ml
70ml and 150ml columns plus the
Whatman AutoCup®. Bringing added
versatility to the SpeediFlow.
11
Storm Vs Breeze:
What’s the difference?
Storm and Breeze are both
heating and cooling work
stations, but have different
features and are therefore
suitable for different reactions and applications.
10/6/09
Page 12
NEW Storm™ & Breeze™ Heating/Cooling Work Stations
Storm & Breeze are compatible with the Carousel 6/Tornado and Heat-On as
well as any other reactors, blocks or even glass vessels that would normally
locate on to the top plate of a stirring hotplate with a diameter of 135mm.
Combined with a suitable circulator or thermoregulator these innovative work
stations can provide controlled heating and cooling from -65°C to +200°C.
Powerful heating and cooling using an external thermoregulator...
The Storm and Breeze are designed to work with all leading thermoregulators or circulators, with
thermofluids operating in the range of -85˚C to +235˚C. Use a thermoregulator with control software
to program precise heating/cooling gradients and ramps.
Storm features M24 and Breeze features M16 hose fittings. Radleys offer a full range of thermoregulators, insulated hoses, hose adapters, valves and thermofluids, as well as advice on selecting a suitable thermoregulator for your application. Fig 1 and Fig 2 below show typical heating and cooling
profiles of a Storm and Carousel 6 using a Huber 705 thermoregulator.
Storm
The larger of the two work stations
features a sophisticated internal
fluid path that combines with a high
performance insulated case to
maximise thermal transfer. These
features create a temperature
control module that has a wide
operating range with excellent heat
transfer, making Storm ideal for
steady state reactions from -65˚C
to +200˚C that require stable
temperatures for extended periods,
with minimal variation across the
heated surface.
Breeze
More compact, with a small
bench-top footprint, featuring a
removable stand for stability and
easy clamping. Breeze has no
insulation resulting in a smaller
operating range of -30°C to +165°C
but has a much faster response
time to required changes in
temperature. This makes Breeze
more suitable for applications that
require solution control such as
crystallisation studies.
Fig 1: Storm/Carousel 6 Cooling Profile using a Huber 705
Perform single reactions with Heat-On...
Storm and Breeze can also be used with the full range of Heat-On
blocks, making them ideal for controlling the temperature of individual
reactions in round bottom flasks (10ml to 5 litres). Add an overhead
stirrer and you have a controlled lab reactor.
Technical Specifications
Description
Storm
Solution Temperature Range
-65˚C to +200˚C
Thermofluid Operating Limits
-85˚C to +235˚C
Control by Solution Temperature
No
Typical Applications
Hose Fittings
Insulated
Huber Unistat 705 (-75˚C/+250˚C)
Huber Unistat 825 (-85˚C/+250˚C)
1.5
3.0
Yes
135 x 80mm
M16 (16mm)
No
Without stand 1.6kg
(With stand 3.2kg)
13kg
2.0
-85˚C to +235˚C
367 x 143.5mm
Weight
Huber Ministat 230 (-33˚C/+200˚C)
Breeze
-30˚C to +165˚C
Variable temp reactions
such as crystallisation
Yes
Heating
Power
(kW)
Contro
ooling
heating/c
to
from -65˚C
+200˚C
Steady state temp reactions
such as parallel chemistry
M24 (24mm)
Dimensions (mm)
Description
Fig 3: Breeze Stepped Temperature Profile
using a Huber Ministat 230
Fig 2: Storm/Carousel 6 Heating Profile using a Huber 705
Create a ‘Parallel Process Reactor’ with the Carousel 6 and Tornado...
Storm and Breeze were designed as add-on modules for the Carousel 6 and Tornado combination
creating a powerful Parallel Process Reactor that heats and cools, mechanically stirs up to 6 round
bottom flasks (50ml to 250ml), making it the ideal process optimisation and
development tool. See pages 8, 9 and 10 for full information on the
Carousel 6 and Tornado.
lled
Performance Data
12
11:48
Cooling
Storm
Breeze
Power
at 0˚C (kW) Cooling to -30˚C Heating to 100˚C Cooling to -30˚C Heating to 100˚C
0.35
0.65
2.2
n/a
44 mins
27 mins
34 mins
56 mins
27 mins
n/a
30 mins
85 mins
n/a
60 mins
44 mins
10/6/09
11:48
Page 13
NEW Storm™ Heating/Cooling Work Station
Combined with a suitable circulator or thermoregulator the powerful Storm
can provide controlled steady state heating and cooling from -65°C to +200°C.
Storm is designed to accommodate the Carousel 6/Tornado or Heat-On as well as any other
reactors, blocks and glass vessels that locate on to the top plate of a stirring hotplate with
a diameter of 135mm or larger.
Powerful, even heating...
Storm was created using computer modelling techniques to develop a unique thermofluid path design
which maximises heat transfer and minimises surface temperature variation. This, combined with the
high performance external insulation, ensures a small Delta-T between the thermofluid temperature
and the solution temperature of the reactor(s), making Storm ideal for steady state reactions.
High performance insulation...
Storm is packed with thermal insulation which minimises heat-loss, protects the user and provides
Storm with a thermofluid operating range of -85°C to +235°C, providing a reaction solution temperature
range of -65°C to +200°C.
PTFE insulating plate improves performance and energy efficiency...
A removable PTFE insulating plate has been designed to fit over the surface of the Carousel 6.
The plate not only provides a thermal barrier that improves heating/cooling performance, but it also
increases energy efficiency and reduces condensation and ice formation on the block and flasks
when cooling. The insulating plate also acts as an effective safety barrier protecting the user from
extreme surface temperatures.
Integral safety...
The insulated aluminium outer case of the Storm prevents the user from coming into contact with the
extreme temperatures of the internal thermofluid.
Fluoropolymer splash guard is
chemically resistant and prevents
heat transfer from block to
insulated outer case.
Contoured inner
accepts Carousel 6 base
and Heat-On blocks.
Highly insulated outer
case ensures efficient operation
with minimum heat loss and
maximum safety.
24mm hose fittings
(adapters available).
NEW Breeze™ Heating/Cooling Work Station
Storm with Carousel 6, Tornado,
overhead stirrer and PTFE insulating plate
PTFE insulating plate improves performance
and energy efficiency
The compact Breeze provides rapid heating and/or cooling from -30°C to +165°C,
making it ideal for applications requiring control by solution temperature.
Suitable for solution control...
Breeze has a small internal volume and no insulation which means it is quick to respond to changes
in thermofluid temperature and ideal for experiments that require solution control. When controlling
by solution temperature a thermoregulator with an external temperature probe will be required.
Includes removable stand and drip tray...
Breeze comes with a removable aluminium stand and stainless steel support rods that ensure the
set-up is sturdy and safe. The stand also acts as a drip-tray for any condensation
that may form when using sub-ambient temperatures.
Anodised aluminium
block heats and
cools rapidly.
Affordable,
lightweight and
compact.
16mm hose fittings
(adapters available).
Storm &
hnical
Breeze Tec
Data Sheet
n
Available o
t
Reques
Includes removable
stand/drip tray combination
with integral support rods.
Breeze with 250ml Heat-On, stand
and overhead stirrer
13
GreenHouse Work-Up
Rapid sequential and parallel
purification in a 24 well micro titer
plate footprint using standard
filtration, phase separation and
SPE columns.
The GreenHouse Work-Up Station
is designed to make your parallel
and combinatorial chemistry workup and purification
quick and easy.
11:48
Page 14
GreenHouse Plus Parallel Synthesiser™
The GreenHouse Plus offers all the features of the original GreenHouse Classic
but with increased volume and a single combined reflux and additions head.
The GreenHouse Plus provides 24 heated and stirred glass reaction positions able to
accommodate reaction volumes from 0.5ml to 7ml. A new combined reflux and additions
head allows for convenient additions or withdrawals whilst maintaining an inert atmosphere
and efficiency.
The patented GreenHouse Plus brings all the benefits in productivity of parallel synthesis at a fraction
of the cost of automated systems. Holding 24 glass reaction tubes in a removable reaction block with
the same footprint as a standard micro titer plate the GreenHouse Plus facilitates rapid transfer
of samples by multi-channel pipettor or robotic systems.
Stirs & Cools...
The GreenHouse features an optional cooling
reservoir for chilled reactions to -70˚C
using dry ice and acetone
Water cooled aluminium reflux head
with nickel condensing fingers
provides efficient refluxing within
individual glass reaction tubes.
Heated directly by the stirrer hotplate;
providing an operating temperature
range from ambient to +150˚C.
Digital temperature control +/- 0.5˚C.
Combined reflux and additions head
allowing for convenient additions
or withdrawals whilst refluxing.
is to Evaporation in a sin
Synthes
From
A choice of septum mats
are available.
Cylindrical glass gas enclosure
provides visibility of all 24 reaction
tubes, with no need to lean into
the fume cupboard.
Provides 24 heated and stirred
a reaction volume of 0.5 to 7ml.
No electrical or moving parts
ensures maintenance free operation.
Easy to operate and set-up,
with minimal training time.
“V-Mag” technology uses a
vertically positioned stirring bar
to maximise the uniformity of the
stirring within each reaction tube.
Round aluminium base transmits
heating evenly to all positions.
Compact size has small bench-top
footprint - easy to store.
to download a PDF on
the GreenHouse Plus
14
10/6/09
or IKA hotplate stirrer, so
utilising existing and readily
available technology.
Utilises single rotating magnetic
field of the hotplate stirrer
to stir all 24 positions.
Combined Reflux and
Additions head with nickel
condensing fingers
GreenHouse Plus allows
additions & withdrawals
through sealing mats
Reaction block fits
directly into Genevac
vacuum centrifuges
10/6/09
11:49
Page 15
GreenHouse Blowdown Evaporator™
High performance
personal evaporation
at an affordable price...
Personal parallel evaporation of chemistry samples and HPLC fractions.
Turn your existing GreenHouse Plus Parallel Synthesiser (opposite page) into a parallel
evaporator, or simply use this system as your own personal benchtop evaporator.
Compatible with:
The GreenHouse Blowdown uses a precisely controlled flow of inert gas combined with digitally
controlled heating to carefully evaporate your samples. Interchangeable plates with either 8 or 24
hollow pins deliver an equal flow of gas to each tube, vial or well. The absence of any vacuum
avoids bumping, further protecting your sample during evaporation.
Tests show that the Greenhouse Blowdown can evaporate 8 vials, each containing 5ml of methanol
in only 22 minutes
• GreenHouse Reaction Block
• 8 or 24 position Vials Racks
• 8 or 24 well Micro Titer Plates
Visit www.radleys.com to download
a PDF on the GreenHouse Blowdown
By inserting the Adaptor into
the GreenHouse Plus Base the system
is quickly adapted to accept vial racks
or standard micro titer plates.
Environmentally friendly enclosed design
contains evaporating solvent, allowing subsequent
trapping and collection of solvent via a high
performance glass condenser.
This precise heat control and the
absence of a vacuum also protects
your sample and avoids bumping.
Select the appropriate Blowdown Pin Plate.
Interchangeable plates with either 8 or 24
hollow pins deliver an equal flow of gas
to each tube, vial or well.
Removable head features quick-release
handles for rapid changing of blowdown
pins plates and safety relief valve on inlet to
prevent over-pressure during evaporation.
a singl
e com
pact
syst
em.
..
The GreenHouse Blowdown can be used
with standard 8 or 24 well Micro Titer Plates,
GreenHouse Reaction Tubes or choose
from 6 different vial racks.
Digitally controlled
heating from the hotplate
gently adds energy to the
sample to speed the
evaporation process.
Blowdown Head with 24
Pin Plate, Standard
GreenHouse Base
and GreenHouse
Reaction Block
Blowdown Head,
Standard GreenHouse
Base, Base Adapter and
24 Position Vial Rack
or IKA hotplate stirrer, so utilising existing
and readily available technology.
GreenHouse with
Blowdown Head, low
profile Stand Alone Base
and 24 Position Vial Rack
Blowdown Head,
Standard GreenHouse
8 Position Vial Rack
Blowdown Head,
low profile Stand Alone
Base and 8 Position
Vial Rack
Blowdown Head,
Standard GreenHouse
24 Position MTP
GreenHouse with
Blowdown Head, low
profile Stand Alone Base
and 24 Position MTP
15
GreenHouse Work-Up
Rapid sequential and parallel
purification in a 24 well micro titer
plate footprint using standard
filtration, phase separation and
SPE columns.
The GreenHouse Work-Up Station
is designed to make your parallel
and combinatorial chemistry workup and purification
quick and easy.
11:49
Page 16
GreenHouse Work-Up Station™
Rapid sequential and parallel purification in a 24 well micro titer plate
footprint using standard filtration, phase separation and SPE columns.
The GreenHouse Work-Up Station is designed to make your parallel and combinatorial
chemistry work-ups and purification quick and easy.
The principle of the GreenHouse Work-Up Station allows efficient purification of samples from any
standard 24 well format micro titer plate, as well as the GreenHouse Plus reaction blocks and other
24 position synthesisers.
The GreenHouse Work-Up Station allows two levels of filtration, phase separation and/or SPE (Solid
Phase Extraction) columns to be stacked, one above the other. This enables parallel and sequential
filtration, phase separation and/or SPE in 24 samples.
GreenHouse Work-Up Station
Clear gas cover allows slight positive
pressure to be applied to increase
flow rate of difficult samples.
Easily removable upper
support plate allows unit
to be used for single or
sequential parallel purification.
Stacked column design
allows sequential purification
e.g. phase separation and
SPE or filtration and SPE.
Robust anodised
aluminium construction.
Radleys offers a wide range of
SPE columns, including Silica,
SAX Acetate, Aminopropyl, SCX,
plus Phase Separation and
Filtration columns.
Design accommodates
all standard 3ml and 6ml
tabbed or tabless SPE
or filtration columns.
Unique recessed design
of support plates allows
positioning of standard format
columns within micro titer plate
footprint without column tabs
obstructing each other.
Silicone sponge gasket on upper
and lower support plates seals
with clear acrylic gas cover.
16
10/6/09
Accepts all standard 24 well
micro titer plates, as well as
GreenHouse Plus Reaction
Blocks for fraction collection.
Easily removable upper support plate allows unit to be used
for single or sequential parallel purification. Clear gas cover
allows slight positive pressure to be applied to increase flow
rate of difficult samples.
Accommodates
all standard 3ml
and 6ml tabbed
or tabless SPE
or filtration
columns.
10/6/09
11:50
Page 17
Titan™ 24 & 96 Well Resin Loaders
Load ten 24 or 96 well
micro titer plates or tube
arrays in less than 50 mins
Rapidly load resins or solid supported reagents into any standard
24 or 96 well array.
The Titan Resin Loader is designed for the efficient parallel dispensing of resins into a variety
of 24 & 96 well formats. Developed by chemists at GlaxoSmithKline the Titan Resin Loader
greatly speeds up the process of loading small amounts of resin into 24 or 96 arrays and
avoids the use of toxic solvents.
Compatible with:
•
•
•
•
•
•
Resins that can be dispensed include:
• Solid phase resins e.g. Wang, Merrifield.
• Solid supported reagents such as PS-carbodiimide.
• Scavengers, such as PS-isocyanate and ion-exchange resins.
Different amounts of resin can be dispensed by selecting the appropriate Filler Plate. The 24 well
system includes three sizes of Filler Plate and the 96 well six sizes of Filler Plate - which can
be used individually or in combination to provide a wide range of filling volumes.
Titan Resin Loaders
24 or 96 Well Micro Titer Plates
24 or 96 Position Tube Systems
GreenHouse Reaction Block
Mettler MiniBlock
Irori MicroKans & Minikans
Robbins FlexChem Synthesiser
Titan 96 Well Resin Loader
Excess resins
collected in troughs
to avoid waste
Precision engineered
filler plates allow a
wide range of volumes
to be dispensed
Universal locating
plates locate on top of
any standard well array
Titan
24 Well
Resin Loader
Special bar locks filler
plates into position ensuring
accurate charging of wells
d
c
b
e
The Titan 24 Well Resin
Loader includes:
a
b
c
Locating Plate
100mm3 Filler Plate
150mm3 Filler Plate
f
a
d
e
f
The Titan 24 Well
Resin Loader is
compatible with the
24 tube GreenHouse
Plus Reaction Block
c
a
c
c
b
b
f
e
d
g
Titan 96 Well Resin Loader includes:
a Locating Plate
b Three Shallow Filler Plates
c Three Deep Filler Plates
d Shallow Calibrator Block
e Deep Calibrator Block
f Spacing Bar
g Acrylic Resin Spreader
b
250mm3 Filler Plate
Loader Spacing Bar
Acrylic Resin Spreader
17
10/6/09
11:51
Page 18
Metz Syn10 Reaction Station™
Software Features...
Simultaneously carry out 10 reactions at the same time - but each with
a different temperature, from -30˚C to +150˚C.
• Change-on-the-fly function
for pausing, stopping & modifying
profiles in progress
Features include...
• Multi-user function
up to 10 users can use the
software, and collate their profile
& data irrespective of other users
• Individual well control via PC Computer Interface of heating, cooling and stirring.
• Individual temperature control of each position with a range of -30˚C to +150˚C, with temperature
stability -/+ 0.5˚C.
• Controlled heating and cooling ramp rates from 0.01 to 5.0˚C per minute. Optional crash
heating/cooling at much faster rates.
• Variable data sampling
at selected frequency from once
every 5 secs to 1 hour
• Individual stirring control of each position from 250rpm to 1200rpm, with a magnetic stirrer
for each position.
• Control by solution temperature
• Optional, removable water cooled Reflux Head ensures even and efficient refluxing.
• A single inlet/outlet for vacuum and inert gas, combined with gas-tight PTFE caps, allows
reactions under inert atmosphere.
• Log reaction parameters at selected frequency from once every 5 seconds to 1 hour.
• Change-on-the-fly function for pausing, stopping and modifying profiles in progress.
Extend the working volume of your
Metz Syn10 down to 1ml...
• Using multi-user function, up to 10 users can enter the Metz Syn10 software, create, run, modify
and collate their profile and data irrespective and independent of other users.
Optional Reduced Volume Glass Reaction Tubes
with a working volume of 1ml to 10ml are available
for use with the Metz Syn10. These tubes require
the use of an Aluminium Reduced
Volume Insert.
• Record solution temperature of each individual well with Thermocouple Module and probes.
• Using the Thermocouple Module and probes, users can control by solution temperature.
• System utilises reliable Peltier technology for heating and cooling of wells. Therefore a separate
cooled water source or circulator is required to dissipate heat from the Peltier cells.
A central inlet/outlet manifold for
vacuum and inert gas, combined with
gas-tight PTFE caps, allows reactions
under an inert atmosphere.
Thermocouple Module and probes,
allow control by solution temperature
(Advanced Software Only). Individual
users can select which cells are
controlled by solution temperature
or well temperature irrespective of
other experiments already running.
PTFE caps feature an all PTFE valve, which offers
superior solvent resistance, gas tight sealing and
easy operation. The cap also has a ‘barbed’
stainless steel inlet for easier removal of tubing.
Maximum temperature
differential between any
two positions is 180˚C.
Optional, removable water cooled
reflux head ensures even and
efficient refluxing, minimising solvent
evaporation during synthesis for even
the most volatile solvents e.g. ether.
Adjustable stirring rates for
individual wells. Also features
stirring soft start to ensure
stirrer bar coupling.
18
Individual stirring control of each
position from 250 - 1200rpm,
with a magnetic stirrer for each
position. Provides excellent
magnetic coupling for stirring
even viscous samples.
Individual temperature
control of each position with
a range of -30˚C to +150˚C, with
temperature stability -/+ 0.5˚C.
Integral Peltier cells cool
and heat individual wells.
Individual well control, via PC
Control Software of heating,
cooling and stirring.
Email sales@radleys.co.uk
for technical or pricing info on
the Metz Reaction Stations
10/6/09
11:51
Page 19
Metz Syn10 - for faster process development
and reaction optimisation
The Metz Syn10 allows you to do chemistry at a level
more advanced than ever before. Quickly discover
the optimal conditions for your chemistry.
Metz Syn10 Software Options...
Standard Software
• Individual programming and profiling of
each cell via dedicated Control Software.
• Controlled heating/cooling ramps from
0.01 to 5.0˚C per minute.
• Crash function for rapid temperature changes.
• Individual stirring profiling from 250 to 1200rpm.
• Automatic detection & recapture of magnetic stirrer bars in the event of uncoupling.
• Soft start stirrer start-up to prevent sample damage and maintain coupling.
• Select and observe key reaction parameters in real time graphical display.
• Record solution temperatures with Metz Syn10 Thermocouple Module.
• Variable data sampling - log reaction parameters at from once every 5 seconds to 1 hour.
• Change-on-the-fly function for pausing, stopping and modifying profiles in progress.
Gas Tight PTFE Caps with PTFE Valve
Innovative PTFE magnetic stirring bars
Advanced Software
Advanced software offers all the features of the 'Standard' software plus ‘Multi-user’ and ‘Control by
Solution Temperature’, providing the chemist with maximum flexibility from their Metz Syn10.
Software Upgrade Options for existing Metz Syn10 Users
A variety of upgrade options are available to existing Metz Syn10 users to allow them to take
advantage of these many new features. For full information contact sales@radleys.co.uk
Metz Syn10 Software Features in Detail...
Well programming and logging
via user friendly control software
• Variable Data Sampling - Log reaction parameters at selected frequency from once every 5 seconds
to 1 hour. Offers the chemist the versatility of high frequency data collection for monitoring small
fluctuations accurately or low frequency collection to eliminate the creation of large data files.
• Change-on-the-fly - function for pausing, stopping and modifying profiles in progress. Once the
profile is started further changes can be made to any owners cell for the remainder of their profile;
truly user friendly software.
• Multi-user function - up to 10 users can enter the Metz Syn10 software, create, run, modify and
collate their profile and data irrespective and independent of other users (Advanced Software
Only), creating a reaction station truly capable of multiple independent reactions.
• Control by Solution Temperature - Using the Thermocouple Module and probes, users can
control by solution temperature (Advanced Software Only). Individual users can select which cells
are controlled via solution temperature or well temperature irrespective of other experiments
already running.
One and Two Zone Metz Economy Versions...
The new Metz Syn1 and Metz Syn2 provide all the features of the existing Metz Syn10 but with less
zones. The Metz Syn1 controls all 10 tubes as a
single temperature zone, whereas the Metz Syn2
is controlled as 2 independent zones of 5 cells.
Number of positions
Controlled zones
Reaction volume
Maximum temp difference between adjacent zones
Independent stirring between zones
Multi-user function
Monitor solution temp
Control by solution temp
Current software version
Syn1
10
1 x 10 cells
1ml to 20ml
No
No
Yes
No
V3.11.3
Syn2
10
2 x 5 cells
1ml to 20ml
180˚C
Yes
Yes
Yes
No
V3.11.3
PFA probe inserted
through a port in the
PTFE probe cap
Syn10
10
10 x 1 cells
1ml to 20ml
180˚C
Yes
Yes
Yes
Yes
V3.11.3
Flexible wire probe
inserted via a glass
pocket in the tube
Syn48
48
12 x 4 cells
0.25ml to 2ml
130˚C (60˚C sub ambient)
No
Yes
No
No
V3.11.3
19
11:51
Page 20
Metz Syn48 Reaction Station™
Simultaneously carry out 48 reactions at the same time with 12 different
temperature zones from -30˚C to +150˚C, with magnetic stirring to 1200rpm.
Perfect for high throughput synthesis or small scale optimisation. The Metz Syn48 Reaction
Station builds on the proven Metz technology offering differential temperatures in all 12 zones
of 4 cells, comprising 48 cells in total.
Features include...
Easy to use control
and logging software is
compatible with other
Metz Reaction Stations...
Compatible with:
• Individual zone control via PC Computer Interface of heating, cooling and stirring.
• The system accepts 48 glass reaction vessels configured in 12 independent temperature zones.
• Each cell accepts a single glass reaction vessels with a reaction volume of 0.25ml to 2ml.
• Individual temperature control of each of the 12 zones (4 cells per zone) with a range of -30˚C
to +150˚C, with temperature stability -/+ 0.5˚C.
• Controlled heating and cooling ramp rates from 0.01 to 5.0˚C per minute. Optional crash
heating/cooling at much faster rates.
• Stirring control from 250rpm to 1200rpm - all cells stir at the same speed.
• Metz Syn1
• Metz Syn2
• Metz Syn10
• Removable water cooled Reflux Head ensures even and efficient refluxing. Reflux Head
is available with Viton or Chemraz® seals to provide an inert, gas tight seal of each reaction vessel.
• The Reflux Head also features a single inlet/outlet for vacuum and inert gas for performing
Software Features include...
• Individual programming and
profiling of each of the 12 zones.
• Controlled heating/cooling ramps
with crash cooling option.
• Stirring control 250 to 1200rpm.
• Soft start stirring prevents
sample damage and maintains
coupling.
• System utilises reliable Peltier technology for heating and cooling of zones. Therefore a separate
cooled water source or circulator is required to dissipate heat from the Peltier cells.
Reflux Head is available with
Viton or Chemraz o-rings to provide
an inert, gas tight seal of each
of the 48 glass reaction vessels.
A single inlet/outlet in the Reflux Head
combined with gas-tight inert seals allows
• Select and observe key reaction
parameters in real time graphical
display.
• Variable Data Sampling - Log
reaction parameters at selected
frequency from once every 5
seconds to 1 hour. Offers the
chemist the versatility of high
frequency data collection for
monitoring small fluctuations
accurately or low frequency
collection to eliminate the creation
of large data files for longer
duration experiments.
• Change-on-the-fly - function for
pausing, stopping and modifying
profiles in progress.
• Multi-user function - up to 12
users can enter the Metz Syn48
software (each controlling one
of the 12 zones), create, run,
modify and collate their profile
and data irrespective and
independent of other users,
creating a reaction station
capable of multiple independent
reactions.
20
10/6/09
Removable water cooled
reflux head ensures even and
efficient refluxing, minimising solvent
evaporation during synthesis for even
the most volatile solvents.
Individual programming and
logging of each of the 12
zones via user friendly
control software.
Each of the 48
cells accepts a
glass reaction
vessel with a
reaction volume
of 0.25ml to 2ml.
Maximum temperature
differential between any
two positions is 130˚C.
(60˚C sub ambient)
Adjustable stirring rates from
250 to 1200rpm powered by
energising magnetic coils.
Temperature control of each
zone with a range of -30˚C
to +150˚C, with temperature
stability -/+ 0.5˚C.
RS232/RS485 interface
at rear of unit.
Integral Peltier cells cool and heat
each of the 12 zones of 4 cells.
Soft start stirring
feature ensures good stirrer
bar coupling.
Email sales@radleys.co.uk
for technical or pricing info on
the Metz Reaction Stations
10/6/09
11:51
Page 21
Metz Heater-Shaker Reaction Station™
Multiple position heating and shaking with removable blocks for reaction
tubes or micro titer plates.
The Metz Heater-Shaker is ideal for parallel synthesis, combinatorial chemistry, process
optimisation and development as well as biological incubations. The Heater-Shaker is
particularly suited to solid phase chemistries where conventional stirring with a stirring bar
would damage the delicate resin.
Features include...
• Precise heating control from ambient +5˚C to +150˚C (temp uniformity ±0.5˚C between wells).
Standard and custom
reaction blocks available
Standard Reaction Block Modules
•
•
•
•
•
•
96 position block for 16mmø tubes
40 position block for 24mmø tubes
4 position block for standard MTPs
4 position block for PTFE MTPs
2 x Charybdis Calypso systems
90 position block for 1.5ml tubes
• Microprocessor controlled shaking from 100 to 600rpm. Orbital motion has a 19mm diameter.
• Easy to use touch panel control of heating and shaking with back lit LCD display of values.
• Compact, low profile design (235mm wide x 165mm high x 508mm deep).
• Choice of easily removable reaction blocks for tubes and micro titer plates. Custom reaction blocks
are available on request to accept vessels of your specification.
• Soft start or ramping feature to allow slow build-up to set speed (from 0-59 mins), minimising
splashing or sample damage.
• Auto-Park feature ensures the block always returns to the same X-Y position for accurate alignment with robotic systems.
• RS232/RS485 interface allows setting of individually timed heating and agitation profiles via
external PC control. System can also be integrated with robotic systems for automated operation.
Precision engineered aluminium blocks
efficiently heat reaction tubes to +150˚C
• An over temperature thermal cut-off switch eliminates runaway heating conditions.
• When the reaction block temperature raises above 50°C, a hot warning symbol will flash - warning
of high temperature, even if the unit is then disconnected from the mains supply.
• Safety Interlock facility ensures the agitation will stop when the block door is opened.
• Agitation Watch Dog constantly monitors speed to prevent a run-away speed condition.
Robust internal plate mechanism allows
heavy workloads and 24 hour continuous
operation. Eccentric drive provides
strong uniform agitation.
Auto-Park feature ensures platform always
stops/starts in the same x-y position.
Choice of easily removable
reaction blocks for tubes
and micro titer plates.
Easy to use touch panel control of heating and
shaking with back lit LCD display of values
Soft start protects
delicate samples.
Hot block warning when
the block is over 50˚C.
Easy integration with
leading robotic and auto
sampler systems.
96 position reaction block holds 16mm Ø tubes
(12 x 8) gripped by internal ‘O’ rings
Safety door locking ensures
the platform stops if the
door is opened.
Titan 100% solid PTFE plates
are available in a wide range
of well formats and volumes
Reaction block accepts 4 Titan PTFE
Micro Titer Plates
21
22
10/6/09
11:51
Page 22
Jacketed Reaction System Quick Guide
Reaction Systems
Reactor-Ready™
Lab Reactor
Controlled Lab Reactor
Custom designed
reaction systems from
100ml to 50 litres
Innovative, reactor work
station for vessels from
250ml to 5 litre
Lab reactor platform with
integrated digital control for
vessels from 100ml to 10 litres
Chemists requiring a custom
reaction system to meet specific
requirements or applications
Chemists requiring an
off-the-shelf, pre-configured,
easy to use glass lab reactor
Chemists and process engineers
who require a versatile reactor
platform to accommodate a wide
variety of vessel volumes
and designs
Chemists and process engineers
who require an automated reactor
platform with datalogging & software
control to accommodate a wide variety of vessel volumes & designs
Custom
Reaction Systems
Lara Lite™
User Profile
Key Features
Lara™
Automated
Controlled Lab Reactor
Fully automated lab reactor
platform for vessels from
100ml to 10 litres
Custom design service
- with over 40 years experience
and technical expertise
Accepts reactors from
250ml to 5 litre
100ml to 10 litre
100ml to 10 litre
Incorporate a full range of reactor
features and integrate a wide
range of 3rd party devices
Convenient and quick reactor
exchange and stirrer alignment
Innovative reactor clamp
allows rapid reactor exchange
leaving lid in place
Innovative reactor clamp
allows rapid reactor exchange
leaving lid in place
Wide choice of reactor materials
including glass, hastelloy,
stainless steel, PTFE etc
Off-the-shelf, quick to set up
and easy to use
Integrated self aligning overhead
stirring with digital speed and
torque display
Integrated self aligning overhead
stirring with software control
In-house manufacturing to ISO
approved standards
Cost effective
Upgradeable to Lara
or generic control software
Intuitive software for control
and datalogging with full
integration of 3rd party devices
100ml to 50 litre
250ml to 5 litre
-90˚C to +250˚C
-60˚C to + 190˚C
Specifications
Flexible recipe design
incorporating multiple steps,
control loops & safety feedbacks
100ml to 10 litre
100ml to 10 litre
-70˚C to +200˚C
-70˚C to + 200˚C
10/6/09
11:52
Page 23
Custom design glass reaction systems
from 100ml to 50 litres
Reaction systems to your specifications.
Drawing upon 40 years experience Radleys has established an international
reputation for manufacturing the highest quality glass reaction systems.
Indeed, all of the reaction systems we manufacture are designed in close
co-operation with our customers to ensure optimum performance.
Whether you require a large multi-vessel process system, a single 100ml benchtop
reactor or a complex parallel reaction system, Radleys’ team of highly skilled
product specialists, chemical engineers and scientific glassblowers will be pleased
to assist in all aspects of your project.
Our range of services include:
•
•
•
•
•
•
Single and double jacketed vessels.
Frameworks and supports.
Thermoregulators, chillers and circulators.
Overhead stirrers, sensors and probes.
Data logging and software control.
Full installation and training.
To discuss your requirements please email
sales@radleys.co.uk or contact your local Radleys distributor.
Scope of our services...
•
•
•
•
•
•
•
•
•
•
•
•
•
•
Single jacketed reaction vessels to 50 litre.
Vacuum jacketed reaction vessels to 10 litre.
Cylindrical, spherical, dish shaped, tall or squat vessels.
Glass or PTFE lids with any number or style of ports.
Multi-reactor systems for parallel synthesis.
Solid phase reactors with sinters.
Fermenters and bioreactors.
Photochemical and UV reactors.
Software and semi-automated control.
Benchtop and floor stands/supports/frameworks.
Scrubbers, condensers and distillation assemblies.
Overhead stirrers: electrical, air powered and ATEX.
Thermoregulators: supply, servicing and support.
Steel and PTFE vessels.
Simply tell us what you want...
The combination of different features and design variations for vessel systems is almost limitless. Therefore
please contact our specialists on sales@radleys.co.uk
for FREE technical advice and design service.
Need a vessel modification or repair?
If you have an existing piece of glassware you want
modified or repaired we can help.
Tel: +44-1799-513320 Fax: +44-1799-513283 Email: sales@radleys.co.uk www.radleys.co.uk www.lara-clr.com
23
11:53
Page 24
NEW Reactor-Ready™ Lab Reactor
Innovative, patented, low cost, reactor work station for glass vessels
from 250ml to 5 litres.
Features include...
•
•
•
•
•
•
•
•
•
•
Quick-release vessel clamp allows rapid vessel exchange.
Range of single and double jacketed glass vessels including 250ml, 500ml, 1 litre, 2 litre and 5 litre.
Support system accepts all leading brands of overhead stirrer and allows easy, tool free adjustment.
Triple support stand features heavy duty stainless steel support rods for maximum strength,
stability and to minimise vibration.
Glassware accessories include condensers, dropping funnels etc.
Self aligning stirrer coupling engages without the need for tools.
Quick release hose coupling allows rapid exchange of vessels.
Hose manifolds allow easy thermofluid drain down.
Temperature range: -60ºC to +190ºC (subject to thermoregulator).
Thermofluid Connections: M24.
Support system accepts
all leading brands of overhead
stirrer and allows easy, tool
free adjustment
Stirrer support I-beam
allows the stirrer drive to be easily
lowered and raised without needing
to reposition the stirrer drive.
Vessel clamp support beam allows
easy vertical repositioning of the vessel whilst
maintaining the stirrer coupling alignment.
Precision ground lid and vessel flanges combine
with PTFE collar and FEP encapsulated o-ring
to offer superior sealing performance.
Vessel-to-manifold hoses
are supported by the manifolds and frame,
eliminating stress on the vessel.
Venting stopcock on the return manifold
allows quick and easy venting of the heat
transfer fluid during vessel changeover.
Heat transfer fluid may be drained back to the
circulator or decanted via a fluid drain
tap on the supply manifold.
24
10/6/09
Wide range of accessory glassware
including condensers, dropping funnels, adapters,
powder addition funnels, gas purge and liquid
inlet adapters etc.
Patented drop-in
stirrer coupling engages easily
without the need for tools.
PTFE stirrer guide provides excellent stirring
and sealing performance. An extended stirrer
shaft support ensures whip-free agitation.
Reaction vessels are held by a novel
quick-release clamp. No tools are required
to exchange vessels.
Accepts jacketed and vacuum
jacketed vessels including 250ml, 500ml,
1 litre, 2 litre and 5 litre.
Chemically resistant PTFE
stirrer shafts in a wide
range of styles.
Quick release coupling allows rapid exchange
of vessels without the use of tools. Operates
over the temperature range -60˚C to +190˚C.
Innovative triple support stand features heavy duty
stainless steel support rods for maximum strength,
stability and to minimise vibration.
Heavy duty base plate with levelling feet
ensures that the Reactor-Ready support
stand is secure and stable.
10/6/09
11:53
Page 25
Lara Lite™Controlled Lab Reactor
This versatile lab reactor platform replaces the
need for multiple reactor set-ups, saving space,
money & making your synthesis more productive.
Features include...
•
•
•
•
The Lara Lite benefits...
• Remote LCD stirrer control panel
can be mounted in any location
and allows control of stirring
speed with torque display.
• Fixed overhead stirring ensures
perfect stirrer alignment every
time.
• Unique vessel clamping and
quick-release sidearms allows
you to swap vessels in minutes
without the use of tools
• Clamping mechanism automatically centralises the reaction
vessel and lid, and provides a
vacuum tight compression on
the sealing interface.
• Vessel remains supported even
when clamp is unlocked
• Unique self gripping, chemically
resistant, vacuum tight stirrer
design allows shafts to be
gripped or released in seconds
without the need for tools.
• Wide choice of standard/custom
stirrer designs facilitates agitation
studies.
• Semi-automated oil drain down
provides a quick, safe and clean
method of removing thermofluid
when changing vessels.
• Easy connecting side arm
couplings are leak free and can
be removed and reconnected in
seconds without tools.
• Choice of single, double (vacuum) and split jacketed vessels;
offered in a variety of geometries
allow you to mimic plant.
• Options for liquid and solid
additions, gas, vacuum, reflux,
distillation and post reaction
work up.
•
•
•
•
•
•
•
•
•
Manual stirrer control from 70 to 1000rpm with LCD display.
Torque Reading in Ncm (with zero feature).
RS232 interface for optional PC control.
Quick-release vessel clamp for ‘tool free’ reactor change
in under 5 minutes.
Accepts reaction vessels from 100ml to 10 litres.
Wide range of standard and custom vessel designs.
Glassware accessories include condensers, dropping funnels etc.
Integrated self aligning stirrer, with self gripping stirrer guide.
Quick connect sidearm couplings.
Semi-automated thermofluid drain down.
Integral, sturdy support framework.
Temperature range: -70ºC to +200ºC (subject to thermoregulator).
Thermofluid Connections: M16.
Correct stirrer alignment is
assured every time, with
no requirement to align
the stirrer motor between
procedures.
Self gripping stirrer guide design
allows stirrer shafts to be gripped
or released in seconds without
the need for tools.
Reaction vessels are held by a
quick-release clamp. No tools are
required to exchange vessels.
The integral hinged stirrer design
ensures the quick and easy removal
of the lid and stirrer guide.
Remote
control wit
h LCD
display of
speed
and torque
Low profile stirrer reduces the
overall height of the unit.
250ml
1 litre
5 litre
10 litre
Accepts glass reaction vessels
from 100ml to 10 litre, with split
jacket, vacuum jacket, conical,
dished etc. Custom designs to
mimic your plant.
Compatible with PTFE,
glass and steel stirrer designs.
Custom stirrer designs available.
Quick release coupling
allows rapid exchange
of vessels without the
use of tools. Operate
over the temperature
range -70˚C to +200˚C.
Remote LCD stirrer control
panel can be mounted in any
location and allows digital
control of stirring speed.
Semi-automated thermofluid drain down,
provides a quick and safe method of removing
the thermofluid from the vessel jacket.
25
Lara benefits...
•
•
•
•
•
Enhanced productivity
Process reproducibility
Time-saving user features
Fits into a standard fumehood
Custom glass vessels to mimic
your plant
10/6/09
11:53
Page 26
Lara™Controlled Lab Reactor
A fully automated lab reactor platform for reaction
vessels from 100ml to 10 litres.
Lara allows the user to replace multiple reaction set-ups in
several fumehoods with a single automated system; saving
money, space, increasing your productivity and making
process automation much more accessible.
Lara accepts reaction vessels from 100ml to 10 litres, with vessel exchange and draindown taking
less than 2 minutes. Lara is designed to remove all the hassle of setting up and adjusting vessels,
lids, stirrers etc that is associated with conventional reaction systems. Lara also includes an integral
stirrer, datalogging and intuitive software that allows you to write recipes, store data and control 3rd
party equipment like thermoregulators, peristaltic pumps, balances, pH meters, syringe pumps,
turbidity meters, flow meters etc to create an integrated and automated reaction system.
Optical Windows...
Lara split jacket vessels are available
incorporating a flat, optically clear
window for use with video microscopy.
The new innovation opens the way
to accurate and sensitive particle
characterisation enabling early stage
evaluation and resolution of process
issues, reducing process costs and
avoiding the need for repeat batches.
Correct stirrer alignment is
assured every time, with no
requirement to align the stirrer
motor between procedures.
The integral hinged stirrer design
ensures the quick and easy removal
of the lid and stirrer guide.
250ml
Self gripping stirrer guide design
allows stirrer shafts to be gripped
or released in seconds without
the need for tools.
The Lara Expansion Hub offers unlimited
system expansion and development
opportunities through the control of
existing or future third party laboratory
equipment such as pumps, balances,
thermoregulators, temperature probes
etc. The Expansion Hub simply connects
to the Lara core system providing a complete integrated, yet expandable solution.
1 litre
5 litre
10 litre
Accepts glass reaction vessels
from 100ml to 10 litre, with split
jacket, vacuum jacket, conical,
dished etc. Custom designs to
mimic your plant.
Reaction vessels are held by a
quick-release clamp. No tools are
required to exchange vessels.
Connect more devices...
Low profile stirrer reduces the
overall height of the unit.
Integrate and control 3rd
party RS232, analogue
or digital devices such as
balances, pumps, syringe
pumps, pH meters etc
Compatible with PTFE,
glass and steel stirrer designs.
Custom stirrer designs available.
In-built scaffolding
allows the attachment of glassware
and third party
devices.
Quick release coupling
allows rapid exchange
of vessels without the
use of tools. Operate
over the temperature
range (-70 to +200˚C).
Semi-automated thermofluid drain down,
provides a quick and safe method of removing
the thermofluid from the vessel jacket.
26
Self aligning integral stirrer drive
Low profile drive
mechanism
Self gripping
stirrer guide
Quick-release
vessel clamp
Easy to
change lids
Easy to change
glass vessels
Accepts a wide
range of sensors
10/6/09
11:53
Page 27
Lara™Control & Logging Software
The Lara software is presented in a clear and simple format so
that even unfamiliar users can quickly learn to program complex
recipes.
Using familiar Windows® shortcuts and visually intuitive prompts, users of the
Lara software quickly gain confidence in writing simple and complex recipes,
minimising learning time associated with the control software. This makes Lara
much more accessible than many other instruments and reduces the training
requirements for new users.
Intuitive Software...
• Intuitive drag and drop interface allows the easy set-up of new hardware and recipes.
• Automatic pre-run verification ensures correct communication with required devices.
• User defined graphs allow real time data to be presented in a variety of formats.
Apparatus View
Flexible Recipe Design...
• Create new recipes via a logical flowchart interface.
• Incorporate any number of steps, involving any combination of sequential or parallel
operations.
• Complete data logging of experimental parameters.
• Archive, recall and transfer recipes to ensure exact experimental reproducibility.
• Double Click allows full on-the-fly editing of the recipe during the running experiment.
Safety Control Loops...
• Includes alarms and fail-safe conditions for each device that has been configured.
• Each item of hardware has it’s own independent warning alarm and safety shutdown.
• Safe unattended operation increases productivity and throughput.
Temperature Controlled Dosing...
• Software includes automated additions recipe steps which allow the chemist to
predetermine linear or non linear addition rates.
• Allows the user to predetermine a maximum reactor temperature where the addition
should halt until a safe working temperature has been recovered.
Recipe Design View
Sensor Feedback...
• Includes automated recipe control steps for pH, temperature, agitation and addition.
• Allows the user to predetermine any sensor reading to trigger any recipe step to start,
hold or finish.
• The architecture of Lara software has been designed so that it can integrate and
control almost any third party RS232, analogue or digital device.
• Create ‘control loops’ to provide unlimited flexibility in designing and setting up new
experiments.
Annotated Pause Function...
• Designed so that at any stage the recipe will hold stirring and temperature control
conditions and display a message prompt for the user. The recipe continues when the
chemist has acknowledged the message and this event is time stamped.
On the Fly Control...
• Allows responses to be continuously monitored and graphed on screen.
• Experiments can be modified “on-the-fly” and all reaction data is continuously logged
to CSV data files making analysis easy.
• If changes to a recipe need to be made, the chemist has complete control at all times
to intervene quickly and simply.
Run View - with Log
User Notebook...
• Includes a Comment Log, which allows the user the opportunity to record comments.
• Time references are useful for the write up and later optimisation of the recipe.
Graphical Displays...
• Displays user defined graphs of whichever sensor readings and instrument set points
the user wishes to view.
• Enables post experimental viewing of the data, graphically and numerically, along side
the reaction log containing user notes and time recorded events.
Run View - with Mimic
27
Product Guide Vol5 Back Pg:Distributor Update
11/5/10
16:26
Page 1
Improving the productivity of your chemistry...
Radleys have been manufacturing scientific glassware and supplying laboratory instruments for over 40 years. Our customers include leading
industrial and academic research facilities around the world. In an ever changing commercial environment we work hard to respond to the needs
of our customers by investing in new product development that will allow them to remain at the forefront of chemistry research. Our specific areas
of expertise are focused on equipment for chemistry synthesis, process development, work-up, purification and evaporation.
International Distributors
Pakistan
Diagnostic Systems
Sweden
Pretech Instruments KB
Ireland
Labplan Ltd
Poland
Witko Sp z o.o.
Switzerland
IG Instrumenten-Gesellschaft AG
Israel
Labotal Scientific Equipment Ltd
Portugal
Antonio M.S Cruz - Material de
Labotorio, LDA
Taiwan
Pantech Instruments Co., Ltd
Australia & New Zealand
Pacific Laboratory Products
Croatia
BIA
India
INKARP Instruments Private Ltd
Belgium & Luxembourg
Analis Scientific Instruments
Denmark
Biolab A/S
t 3 9845 0300
f 3 9845 0350
e elinork@pacificlab.com.au
www.pacificlab.com.au
Contact: Elinor Kamachu
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f 09 220 08 48
e htn@analis.be
www.analis.com
Contact: Herman Theunissen
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Contact: Martina Vitanc
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Polimate
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Contact: Regiani Ronqui
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Contact: Serge Preseault
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Tegent Technology Ltd
Hong Kong Office
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Quantum Eesti AS
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PLD Finland Oy
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Contact: Vesa Rauhala
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Interchim
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Contact: Athina Mathioudaki
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Contact: John Post
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Kvalitex Kft
t 1340 4700
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e info@kvalitex.hu
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Contact: Dr Pal Tetenyi Jr
Italy
Stepbio srl
t 051 6343340
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Contact: Dr Stefano Giovanninetti
Japan
LMS Co. Ltd
t 03 5842 4301
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e kasuga@lms.co.jp
www.lms.co.jp
Contact: Yoshio Kasuga
Korea
Young Jin Biochrom Co., Ltd.
t 02 575 1494
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Contact: Mr J H Lim
Latvia
SIA Quantum Latvia
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Contact: Andres Siiman
Malaysia
Bio-Focus Saintifik Sdn Bhd
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Contact: Shamsul Bharin Hassan
Norway
Bergman AS
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Contact: Marianne Ager Ryen
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BIA
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Contact: Jes Lim
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BIA
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Separations Pty Ltd
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e nicolas@separations.co.za
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Contact: Nicolas Queisser
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Contact: Jörg Heerklotz
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f 02-2741-5583
e sales@pantech.com.tw
www.pantech.com.tw
Contact: Cindy kuang
Thailand
Scientific Promotion Co Ltd
t 0 2185 4333 ext 2701
f 0 2185 4426
e sorraton.sr@spcgroup.co.th
www.spcgroup.co.th
Contact: Sorraton Ramangkur
Turkey
Info Kimya
t 216 325 6747
f 216 325 6566
e bulentelma@infokimya.com
www.infokimya.com
Contact: Bulent Elma
United Kingdom
Radleys
t 01799 513320
f 01799 513283
e peter.savic@radleys.co.uk
www.radleys.com
Contact: Peter Savic
USA
Heidolph Brinkmann, LLC
t 224 265 9600 ext 107
f 224 265 9611
e koconnor@heidolph.com
www.heidolphbrinkmann.com
Contact: Kristof O’Connor
For full contact details of our
distributors please visit...
www.radleys.com
Spain
Scharlab S.L.
t 093 7456426
f 093 7152765
e cromato@scharlab.com
www.scharlab.com
Contact: Anna Maria Pastor
© Radleys 2009.

Improving the productivity of your chemistry

Transcription

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