IJFTR 31(3) 387
Transcription
IJFTR 31(3) 387
I ndian Journal of Fibre & Textile Research Vol. 3 1 , September 2006, pp. 387-393 Structural and functional characteristics of yarns manufactured by different pneumatic spinning systems A R i va L Coli & M Kasem ", I nstituto de I nvestigaci6n Textil de Terrassa CINTEXTER), U n iversidad Poli tecnica de Catalufia, Spain Revised received 2 J April 2005; accepted R lillie 2005 The structural and functional properties of yarns manufactured by two pneumatic spinning systems, namely pneumatic wrapping spinning by false twist and pneumatic spinning by real wrapping twist, have been studied and compared to those of the yarns manufactured by conventional ring spinning. These properties are assessed by determining apparent diameter. yarn deformation, yarn evenness, hairiness, neps, average apparent twist, tenacity, elongation, twist vivacity, elongation due to untwist-backtwisting and residual shrinkage. The real wrapping twist pneumatic spinning system produces yarns that have a less pronounced corkscrew structure than those produced by false twist pneumatic spinning. However, the yarns produced by real twist spi nning show some characteristics of i rregularity and dynamometric characteristics that situate them in an inferior position to yarns produced by conventional ring spinning. Keywords: Cotton, Corkscrew structure, Pneumatic spinning, Polyester, Ring spi nning, Wrapping fibre. Yarn IPC Code: I nl. C I . 8 00 1 H i l l i S 1 Introduction Of the various spinning systems utilized to manufacture yarns, pneumatic spinning allows one of the quickest speeds of production. Nevertheless, the yarns manufactured by pneumatic spinning are characterised by a particular structure, i n which a core of parallel fibres is bound by wrapping fibres. This structure is peculiar and responsible for the difference between the physical properties of these yarns and those of the yarns manufactured by conventional ring spinning or open-end spinning (rotor) systems. The yarns manufactured by pneumatic spi nning have a corkscrew type structure that is more or less pronounced depending on the quantity of wrapping fibres and on their tension around the core fibres. The regularity and other structural characteristics of the pneumatic yarns depend on a n umber of variables i n the spinning process . I n this paper, the structural and functional properties of yarns manufactured by two pneumatic spinning systems (pneumatic wrapping spi nning by false twist and pneumatic spinning by real wrapping twist) have been studied and compared to those of the yarns manufactured by the conventional ring spinning. I - 1 2 These properties are assessed by "To whom all the correspondence should be addressed. E-mail: ariva@intexter.upc.edu determining the parameters, such as apparent diameter, yarn deformation, yarn evenness, hairiness, neps, average apparent twist, tenacity, elongation, twist vivacity, elongation due to untwist-backtwisting and residual shrinkage. 2 Materials and Methods 2.1 Materials The yarns used in the study were of three types. Two types of yarns were manufactured using two different pneumatic spinning systems and the third type was obtained using the conventional ring spmnmg. The two pneumatic spinning systems used were as follows: (i) (ii) Pneumatic wrapping spinning by false twist, hereafter refened to as HZNtf. Pneumatic spinning by real wrapping twist, hereafter refened to as HZNtrz. The fundamental difference between the two systems is the manner in which they twist the wrapping fibres. The pneumatic wrapping spinning system (HZNtf) (Fig. I ) consists of a tandem twist detwist air jet. The types of air j ets which are now used to impart transient (false) twist in the pneumatic wrapping-spinning system have the disadvantage that the spun yarn takes the characteristical form of a I N D I A N J. F I B R E TEXT. RES., SEPTEMB E R 2006 388 1 2 Table I �Average fibre l e ngth a n d evenness of t h e s l ivers Composi t ion % CO 1 00 75 50 25 Fig. I�Murata MJS technique ( I -draft i ng roller, 2-delivcry roller, 3-suction nozzle, 4-false t w i st nozzle, 5-compressed air, 6-fibre and 7-yarn) R 2 3 4 Fig. 2�New technique ( I -draft roller, 2-dc l i very roller, 3-tw isting nozzle, 4-false twist m i n i-spindle, 5-comprcssed a i r, 6-fibre, 7yarn and 8-dust and free fibres suction) corkscrew and shows a rough touch which negatively influences the properties of the end product. Thi s effect i s particularly felt i n t h e case o f high quality woven and knitted fabrics. On trying to weigh out the low twisting power of the spinning air jets by air overpressure, the excess of flows degradates the quality of the yarns . Thi s fact, together with high hairiness more considerable in 1 00% cotton spun yarns, negatively influences the properties of the end product and thus the appl ication of these yarns is Ii mited. 1 3 - 1 9 A Murata MJS 802 spinning frame was utilized to implement this spinning system. The HZNtrz system (Fig. 2) i s able to produce real twist yarns ; it is basically composed of a false twist miniature spindle and a special air jet, responsible for the aspiration of slivers from the drafting roller (R), for releasing the ends of fibres corresponding to the group of fibres transient twisted by the false twist mini-spindle (4) and for twisti ng them (real twist) on the nucleus. When the yarn loses the false twi st, after goi ng through the false twist mini-spindle, the twisting of fibres wrapping the nucleus is reinforced. All along the spinning zone, the fibres and the yarn are guided by special ducts connected to a vacuum Average fibre length, m m Evenness Uster C Y % Neps neps/g 27.5 28 . 5 30.0 3 1 .7 34.8 3 . 84 4.46 4.49 3.57 2.95 II 9 9 7 ' PES 25 50 75 1 00 4 pump to prevent the contamination of dust and fluff in the working envi ronment. The yarns produced with this system have a structure almost like that of a conventional yarns, where the fibres covering the nucleus have real twist and only the fibres i nside 2 2 remain without torsion, as described earlier. 0. 1 A prototype studied at the I nsti tute of Textile Research of Terrassa ( INTEXTER) was utilized to i mplement this spinning system. The yarn obtained using conventional ring spinning are referred to as RS. Cotton/polyester blend yarns ( 1 5 tex) were spun on each of the spinning systems i n the ratios 1 00:0, 75:25, 50:50, 25:75 and 0: 1 00. The raw materials used were extra-long Egyptian cotton (CO) and 1 .3/38 Br polyester (PES) . The spi nning was done in a n INTEXTER pilot plant. The slivers of all the composi tions were made by three passes through a modified Ingolstadt (Shubert-Salzer) drawi ng frame. From the resulting slivers, the evenness of the sliver and the average fibre length were determined . The average fibre length was determined as per the DIN Standard 53808 (ref. 22) using Afis (Uster) equipment. 23 The evenness of the slivers was obtained 2 using an Uster Evenness Tester I I I 3 following the ASTM Standard D 1 425 (ref. 24). The characteristics of the resulting slivers are given in Table I . 2.2 Methods 2.2. 1 Apparent Diameter and Yam Deformation To determine the apparent diameter and the yarn deformation of the wrapped yarns, a unique methodology was developed. The yarn was taken under constant tension over a glass slide to facilitate a continuous observation of its s tructure. The diameters de and d; were measured in the tested yarns by means of optical and electronic m icroscopy, where the hairi ness can be easily d iscarded optically (Fig. 3). One hundred measurements were made for each type of yarn. The average apparent diameter, RIV A I:l al. : STRUCTURAL & FUNCTIONAL CHARACTERISTICS OF YARNS 389 Fig. 3--S tructure of the HZNtrz yarn necessary to study the yarn deformation, was measured in the areas of little deformation. The coefficient of yarn deformation was determined using the following relationship: De = de - di d where De i s the coefficient of deformation (0 < De > I ) ; dc, the maximu m diameter of the yarn ()..I.); di, the minimum diameter of the yarn ()..I.); and d, the average apparent diameter of the yarn in non-deformed areas ()..I. ) . The closer the value of De to one, the greater i s the deformation of the resulting yarn, which will have a more pronounced " corkscrew" structure. On the other hand, as this value approaches zero, the yarn shows less deformation and is more cylindrical. Figure 4 i llustrates the meaning of the parameters indicated above. 2.2.2 Yam Evelllless, Hairilless alld Neps The yarn evenness was determined with an U ster Evenness Tester I I I 23 as per the ASTM Standard D 1 425 (ref. 24). The hairiness and neps were analysed using the method i ncorporated i n the evenness tester, which gives a value corresponding to the total hairiness and the number of neps. 2.2.3 A verage Apparellt Twist The average apparent twist of the yarns was determined using the Zweigle 0-3 1 2 S Automatic Digital Twist Counter, following the DIN Standard 53832 for twi st-backtwisting. 25 2.2.4 Tellacity alld Elongatioll Uster Automatic Dynamometer was used to determine the tenac i ty and elongation of the yarns, fol lowing the ASTM S tandard 02256 (ref. 26). Each yarn was tested 1 00 times and the average was taken . 2.2.5 Twist Vivacity Twist vivacity is the tendency of a yarn to twist as a consequence of the twist caused by the spinning process. The method to determine the twist vivaci ty Fig. 4-Wrapped yarns (a) with l i ttle deformation and (b) with pronounced deformation entai ls determining the twist produced in a thread after it is plied and hung with a small weight and left to twist until it stabilises. The backtwisting was determi ned following the ISO 206 1 (ref. 27). 2.2.6 Elongatioll due to Ulltwist-Backtwisting Effect This parameter was determined from the elongation curve that results from the untwist-backtwisting of the yarn. The method is based on the hypothesis that the lesser the degree to which the thread exhibits a corkscrew structure, the greater i s the compensation for fibri llar twisting in the group of fibres that make up the nucleus of the wrapped yarn. For this reason, the elongation curve yields i nformation on the structure of this type of yarn. The process fol lowed to determine the elongation curve is as follows: The average apparent twist was measured using an automatic twist counter and following the usual procedure. Subsequently, the elongation produced in the yarn at the following four different moments of backtwisting was measured: • When half (50%) of the apparent twist of the yarn had unwound. • When all ( 1 00%) of the apparent twist of the yarn had unwound. • When half (50%) of the apparent twist of the yarn had backtwisted. • When all ( 1 00%) of the apparent twist of the yarn had backtwisted and the yarn had reached its i n i ti al length. 390 I N D I A N J. F I B R E TEXT. R E S . , SEPTE M B ER 2006 The average apparent twist of the yarns along with the elongation curves was determined using a Zweigle D-3 1 2 S Automatic Digital Twist Counter following the untwist-backtwisting method as per the DIN Standard 53832 (ref. 25). 2.2. 7 Residual Shrinkage This parameter was observed by determining the contraction undergone by the yarns after being boiled i n distilled water. The testing method was based on determining the length of a 2620 tex hank, prior to and fol lowing hydrothermal treatment, by suspending a 497 g weight from it for 30 s. The procedure used was as follows : Acclimate the hanks to a standard relative temperature and humidity for a m i n i mum of 24 h prior to the test. Determine the initial length of the hanks while they sustain a weight of 479 g for 30 s. Carry out the aforementioned shrinkage test. To avoid the hanks becoming tangled during the boiling process, they were introduced longitudinally into i ndividual pouches made of Marquisette fabric. The boiling time was 30 min. The hanks were subsequently allowed to cool till they reached an approxi mate temperature of 50° C . Centrifuge the hanks for 3 m i n , dry them at 3040° C and then suspend them for 2 h under forced ventilation. Re-accli mate the hanks. Re-measure the length of the hanks in the same conditions indicated before. Calculate the shrinkage using the following formula: Shri n kaae (%) = t:> I n i t i al length - Final length Initial length x 1 00 3 Results and Discussion 3.1 Apparent Diameter and Yarn Deformation The results obtained for these parameters are shown i n Table 2. While i n all the cotton/polyester blends the apparent diameters of the HZNtf yarns are smaller than the HZNtrz yarns, the significant differences do not exist among the different blends. It can be clearly observed that for all the cotton/polyester blends the deformation produced by the HZNtrz syste m is less than that of the HZNtf yarns. This reflects the difference that exists between the two spinning systems; in the HZNtrz system, as a consequence of not generating false twist, the wrapping fibres are submitted to less tension than i n the HZNtf which subsequently diminishes the corkscrew effect and, therefore, yarn deformation. Consequently, the structure of the HZNtrz yarns is closer to that of the yarns produced by conventional ring spinning. The yarns with 50:50 CO/PES blend ratio show a slightly higher degree of deformation for both the spinning systems. For the HZNtf system, the 1 00% polyester thread shows the lowest degree of deformation, while in the HZNtrz system the 75:25 CO/PES yarns show the lowest degree of deformation. The differences in deformation between samples of different cotton/polyester blends can be attributed to slight, inherent variations i n tension during the spinning process that stem from spinning different compositions of materials. 3 . 2 Yarn Evenness, Hairiness and Neps Table 3 shows the results for yarn evenness and Table 4 the results for hairiness and the number of neps for 5 different cotton/polyester blends studied. The yarns produced by the three spinning systems show CY Uster values within the 25th percentile of the Uster Standard. The HZNtf yarns yield lower values, i.e. they have a lower percentage of Tablc 2-Apparcnt d iameter (0) and yarn deformation (Dc) Composi tioll, o/(J CO PES 0 H Z Ntrz system CV % � 1 00 De � 0 HZNtf systcm CV % De 42. 1 4 0.63 1 � 2 1 .8 42.83 0.448 1 8.2 � 75 25 22.6 3 7.34 0.277 1 8.4 34.83 0.6 1 1 50 50 22.2 34. 1 1 0.450 1 7.4 33.94 0.745 25 75 22.0 42.92 0.352 1 8.4 33.54 0.590 1 00 22.2 4 1 .03 0.33 1 1 8.2 3 5 . 25 0.5 1 8 RIVA 1'1 {[t . : STRUCTURAL & FUNCTION A L C H A R ACTE R I STICS OF Y A R N S 39 1 Table 3-Yarn evenness properties CO PES 1 00 75 SO 25 HZNtf HZNtrz 1 2.55 1 4.6 Thick places (+50%) 1 1 1 000 III Thin places (-50%) 1 1 1 000 III Uster CV % Composition % RS HZNtrz HZNtf RS HZNtrz HZNtf RS 1 3.9 IS 4 10 44 4 34 SO 15. 1 7 1 2 .53 1 4.47 31 2 12 47 5 28 1 5 .89 1 2. 6 1 1 5 .47 59 6 12 89 14 47 75 1 5 .92 1 3.82 1 5 .76 64 8 45 47 26 67 1 00 1 7.64 1 4. 1 1 1 6. 6 1 69 20 86 89 16 80 25 Table 4-Neps and hairi ness of the yarns Composition % CO PES 1 00 75 SO 25 HZNtrz Neps ( +200%) 1 1 1 000 III 29 Hairi ncss ( h ) (J Hairi ness HZNtf RS H ZNtrz HZNtf RS HZNtrz HZNtf RS IS 9 3.85 4.33 4.06 1 .07 1 .24 0.9 so 3] 13 16 3.8 4.23 3 . 89 1 .02 1.1 0.85 42 28 10 3 . 89 3 .96 3.44 0.99 1 .03 0.76 75 17 40 25 4.0 1 3.78 3 . 83 1 .04 0.94 0.85 1 00 13 \I 5 4.4 1 3.74 4.62 0.82 1 .06 25 I . 00 Table .'i-Average apparent twist and dynamometric properties of the yarns Composition. % CO PES 1 00 75 so 25 25 so 75 1 00 Average apparent twist twistS/ill HZNtrz HZNtf 374.2 472.9 1 92.4 1 83 . 4 1 77 . 8 1 1 2.3 392.0 4 1 4. 7 408.4 464.5 Elongation % Tenacity cN/tex HZNtrz HZNtf RS HZNtrz HZNtf RS 1 5.04 1 6.42 26.82 3.8 3.58 4.77 (9.97 ) ( 1 0. 3 7 ) ( 9 . 68 ) ( 1 0.05) ( 1 3.48) ( 7 .6 1 ) 1 4.94 1 7 .65 24.84 4.33 3.75 5.2 ( 1 0. 7 3 ) (9.34 ) (9.68) ( 1 1 .(8) ( 1 1 .54 ) ( 7 .29) 1 6. 3 8 1 7 .44 2 1 . 14 6.92 4.72 5.47 ( 1 2.45 ) ( 1 0. 7 3 ) (9.53) ( 1 7.3 1 ) ( 1 3.76) ( 1 0.54) 22.5 I 20.28 23 .99 1 0.36 7 .02 9.76 ( 1 3. 1 4) ( 1 1 .9 1 ) ( 1 4.92) (9.49) ( 1 3 .94) ( 1 6.03) 24.84 23.49 3 1 .29 1 0.04 9. 1 2 1 2.35 ( 1 4. 5 9 ) ( 1 3 . 89 ) ( 1 4.86) (9.57) ( 1 0.89) (7.76) Valucs i n parentheses are C V % . i rregularity. It is also these yarns that have a smaller i ncidence of thin and thick parts. The HZNtrz yarns have the highest Uster coefficients of variation, and are thus less even. They also have the highest number of thi n and thick parts. So, the HZNtrz yarns have less corkscrew structure but simultaneously are more i rregular because along the yarn length more thi n and thick places exist (Fig. 5). The yarns obtained by pneumatic spi nning show higher numbers of neps than the conventional yarns; the values for the H ZNtrz yarns are slightly h igher than those for the HZNtf yarns. Though the values for hairi ness are generally around 25% limit of the Uster S tandard, a few samples sl ightly exceeded i t . Differences between the spinning systems were not observed. a b Fig . .'i-Corkscrew and evenness ( a ) yarn without corkscrew but with bad evenness and ( b) yarn with corkscrew but w ith good evenness 3.3 Average Apparent Twist, Tenacity and Elongation The results obtained are shown i n Table 5. The HZNtf yarns uniformly show h igher twist values than the HZNtrz yarns. The yarns obtained by pneumatic spinning have lower tenacity values than the yarns INDIAN J. FIBRE TEXT. RES., SEPTEMB ER 2006 392 produced by conventional ring spinning, as expected. The inferior tenacity of pneumatic yarns with respect to conventional yarns is a well-known fact and represents one of the main disadvantages of this type of yarn. There were no differences worthy of mention between the two pneumatic spinning systems. The i ncrease in polyester fibre percentage i ncreases the tenacity of the yarns produced on pneumatic spinning systems . There is a slight loss in tenacity of conventional yarn as the polyester percentage is i ncreased to 50%; the tenacity however increases on further i ncrease i n polyester content. For the yarns obtained by pneumatic spinning, the elongation values are lower than those obtained by conventional yarns; the HZNtf yarns have the lowest values . Thi s behaviour can be explained by their yarn structure; i n the case of the HZNtf yarns, there exists a smaller chance of sliding of fibres i n the nucleus of the yarn . blends, which indicates that these kind of yarns have a more pronounced corkscrew structure than the HZNtrz yarns. Coherent elongation values were obtained for the 1 00% polyester and 25 :75 cotton/polyester yarns . The values i ncrease when the yarn approach the total unwound and then decrease to zero once the yarn had completely backtwisted. In other cases, the behaviour was somewhat anomalous. One should take note that as the yarns did not show a uniform twist, the moment at which the yarn was completely u ntwisted cannot be determined with exactitude (even if the apparent twist had been determi ned previously). Thus, it i s possible for the yarns to begin to twist again w ithout reaching zero twist, and for this reason they have a smaller length at the end of the test than at the beginning; thi s explains w h y i n some cases negative elongation values are obtained. 3.4 Twist Vivacity of Threads The values for residual shrinkage are shown i n Table 8. I t can be observed that the HZNtrz yarns show less shrinkage than the conventional yarns and that the HZNtf yarns exhibit more shrinkage. The reason behind thi s behaviour is again the HZNtf yarns' thread composition, which is characterised by a strong wrapping configuration. This behaviour is explained by the fact that inside a hank the areas of HZNtf yarns that have a corkscrew structure are more likely to be compacted. The HZNtrz yarns have a higher apparent diameter than the HZNtf yarns, though they have an identical count (number of fibres per section). Thus, the porosity of the HZNtrz yarns is greater than that of the HZNtf yarns. Furthermore, there i s a greater incidence of yarn deformation in the HZNtf yarns than i n the HZNtrz yarns, which causes the former to be more liable to suffer shrinkage. The 1 00% cotton yarns had the least shrinkage throughout. Bearing in mind the fact that the polyester 3.6 Residual Shrinkage The values of twist vivacity (Table 6), somewhat higher in the HZNtf yarns, indicate that these yarns have a greater tendency to backtwist than the HZNtrz yarns . Once again, the values for this parameter i ndicate that the structure of the HZNtf yarns has areas where the wrapping is very pronounced. 3.5 Elongation due to Ulltwist-Backtwistillg Effect Table 7 shows that the values obtai ned for elongation due to the untwist-backtwisting effect are greater in the HZNtf yarns for all the cotton/polyester Table 6-Average twist vivacity of the yarn Twist vi vacity, twistS/ill Composition, % CO PES HZNtrz HZNtf 25 50 75 1 00 20.7 25.0 1 9. 1 1 8.2 29.4 30.6 39.6 49.8 49.9 49.8 1 00 75 50 25 Table 7-Elongation due to the untwi st-backtwisting effect Untwistbacktwisting % 0 -50 - 1 00 50 1 00 Elongation, % 1 00% CO 75:25 CO/PES 50:50 CO/PES 25:75 CO/PES HZNtrz HZNtf HZNtrz HZNtf HZNtrz HZNtf HZNtrz 0 0.24 0.36 0.2 1 -0.50 0 0.27 0.39 0.36 0.02 0 0.08 0. 1 0 -0.02 -0.48 0 0.2 1 0.32 0. 1 1 -0.39 0 0.08 0.08 -0.07 -0.44 0 0.82 0.45 0.32 -0.36 0 0. 1 1 0.22 0.2 1 0.00 HZNtf 0 0.32 0.56 0.52 0.00 1 00% PES HZNtrz 0 0.08 0. 1 2 0. 10 0.00 HZNtf 0 0.47 0.80 0.74 0.05 RIV A et al. : STRUCTURAL & FUNCTIONAL CHARACTERISTICS OF YARNS Table 8--Residual shrinkage Composition, % PES CO 1 00 25 75 50 50 25 75 1 00 Residual shrinkage, % RS HZNtf 2.30 2.07 3.03 4.4 1 3.60 4.89 3.20 4.96 2 .54 4.33 HZNtrz 1 .73 1 .93 2.34 2.27 2.4 1 yarns had not been thermofixed beforehand, it stands to reason that the polyester and the cotton/polyester blend yarns should exhibit a greater degree of shrinkage. 4 Conclusions 4.1 The real wrapping twist pneumatic spinning system gives rise to yarns that exhibit less yarn deformation and have a slightly greater apparent diameter than the yarns produced by the false twist spinning system. 4.2 The yarns obtained by the real twist pneumatic system ( HZNtrz) exhibit less evenness although have a greater number of thi n and thick places which exceed in both measures the corresponding values for the HZNtf yarns. The HZNtrz yarns also have a higher number of neps. 4.3 The average apparent twist is greater i n the HZNtf yarns than in the HZNtrz yarns for all the blends studied. 4.4 The dynamometric behaviour of the yarns produced by both pneumatic spinning systems is very similar and logically worse than that of the yarns produced by conventional ring spinning. 4.5 The HZNtrz yarns have less twist v ivacity than the HZNtf yarns. 4.6 The elongation due to untwist-backtwisting is greater i n HZNtf yarns than that in HZNtrz yarns. 4.7 The shrinkage produced by hydrothermal treatment is less in HZNtrz yarns than in HZNtf yarns. It can be concluded that the real wrapping twist pneumatic spinning system produces yarns that have a less pronounced corkscrew structure than those produced by false twist pneumatic spinning. However, the yarns produced by real twist spinning show some characteristics of irregularity and dynamometric characteri stics that situate them in an 393 inferior position to yarns produced by conventional ring spinning. References 1 Artz P, Messmer R & Maide H, Text Prax Int, 4 ( 1 987) 363. Salhotra K R, Indian J Fibre Text Res, 17 ( 1 992) 255. 2 Coll-Tortosa L, Chemiefasem Text Illd, 27 ( 1 977) 422. 3 4 Garcia E, Hilarura Ileumatica par falsa tarsi6n: relacioll elltre los parametros de hilatura y las propiedades al usa de los tejidos, Ph.D. thesis, Universidad Politecnica de Cataluiia. 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 Barcelona, Spain, 1 993. Krause H W, Mellialld Textilber, 68( I ) ( 1 987) 7. Mori S, U S Pat 5,2 1 1 ,00 1 (to Murata Kikai Kabushiki Kaisha, Kyoto, Japan), 1 8 May 1 993. Nishimura S, U S Pat 4,827,7 1 0 (to Murata Kikai Kabllshiki Kaisha, Kyoto, Japan), 9 May 1989. 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Coli L , Garcia E & Galvan F , Mellialld Textilber, 73(3) ( 1 992) 220. Artzt P, Dallmann H & Shou Tsai I, Text Prax lilt, 4 1 (5) ( 1 986) 509. Feuerlohn H, Coli L, Roig F, Weide T, Tornero J A & Schulze 0, U S Pat 6,209,304 (to W Schlafhorst AG&Co, Germany), 3 April 200 1 . Feuerlohn H , Coli L , Roig F , Weide T, Tornero J A & Schulze 0, U S Pat 6,3 1 4,7 14 (to W Schlafhorst AG&Co, Germany), 13 November 200 I . DIN Stalldards DIN 53808 (Deutshes Institut fUr Normllng e.V., Berlin), 2003. Uster Afts Catalogue - N. -L & D. -T (Zellweger Uster AG, Uster, Switzerland), 1 994. ASTM Stalldards ASTM 0 1 425 (ASTM International, West Conshohocken, PAl, 1 996. DIN Standards DIN 53832 (Deutshes Institut fUr Normung e.V., Berlin). ASTM Stalldards ASTM 02256 (ASTM International, West Conshohocken, PAl, 2002. ISO St(lIldards ISO 206 1 (International Organisation for Standardization, Geneva), 1 995. , .