atlas syringe pump

pump
atlas syringe
pump
Atlas simply does it all
What is the Atlas Syringe Pump?
The Atlas Syringe Pump is a versatile volumetric dosing and/or sampling
system. It allows 2 independant refilling flows, one continuous flow,
reaction sampling, intelligent control of pH and temperature dependant
dosing. It consists of two syringes and multi port valves and be controlled
from the front panel, by a Reactor Master, an Atlas Base or PC software.
Atlas Syringe Pump Benefits
Examples of Operation
• Flexible: Use as 2 refilling pump channels or 1 continuous
pump channel or an autosampler
• Easy to use on its own: Twist and click control knob and
large display
Reagent 1
Reagent 2
• Automated reagent addition: Dispense simply by volume or
Automated reagent addition
flow rate over a time perod or create advanced flow profiles.
• Versatile: 10 reagents to one reactor, 1 reagent to 10 reactors,
5 reagents to 2 reactors, one continuous flow, etc.
Dosing with one syringe and
autosampling with the other
• Automated reaction sampling: Use with the Autosampler
module to regularly aspirate samples into 2ml HPCL vials.
• Wide flow rate range: 0.5μl/min to 20ml/min (up to 200ml/
min with the Atlas Syringe Pump XL)
• Intelligent: Pump to control pH or pause if a reaction
temperature is exceeded. Full data logging to a .csv file.
acid
base
Active pH control
1 continuous flow addition
•
• Excellent chemical compatibility: PTFE, PCTFE and glass.
Compact Size: Fits conveniently alongside reactor.
Watch the Atlas Videos
Watch a video online at www.syrris.com/videos of our Atlas laboratory
scale reactors that feature the Atlas Syringe Pump and its easy-to-use
"twist and click" knob, and other intuitive features.
10 reagents
to 1 reactor
(5 reagents
to 1 reactor)
x2
Left: The Atlas Syringe Pump
and Syringe Pump XL
Above: The Autosampler module
Right: The Atlas Syringe Pump
with Atlas Potassium jacketed
reactor system.
1 reagent
to 10 reactors
(1 reagent
to 5 reactors)
x2
Syringe Pumps
Atlas Specific Parts
Atlas Syringe Pumps
The Atlas Syringe Pumps (regular up to 20ml/min or XL up to 200ml/min) are
versatile volumetric dosing and/or sampling systems. They allow 2 independent
refilling flows, one continuous flow, reaction sampling, intelligent control of pH
and temperature dependant dosing. An Atlas Syringe Pump or Atlas Syringe
Pump XL consists of two syringes and multi port valves and is controlled from
the front panel, by an Atlas Base, Reactor Master or the Atlas or Reactor Master
PC software.
Both types of Atlas Syringe Pumps have 5 main modes of operation
(standalone modes shown by *):
1) Dual Dosing* allows independent control of each syringe (and associated
valve), e.g. dose with one syringe and autosample using the other.
Commands include: dose a volume, pump at a flow rate, dose one reagent
to many reactors, sophisticated profiles or autosampling (connect the
Autosampler and probe to enable automated sampling of up to 6 samples
with each syringe/valve)
2) pH control* (with an Atlas pH probe and node plugged in, dose an acid and/
or base to keep the pH within a defined range)
3) Continuous* (2 syringe pumps work together to produce 1 continuous flow,
i.e. one is refilling while the other is dispensing)
4) Atlas Base Control Mode (an Atlas Syringe Pump can be controlled from the
Atlas Base Unit or Reactor Master as part of an automated temperature and
stirrer speed profile)
5) PC Control Mode (PC software can control Dual Dosing, pH Control and
Continuous dosing in the same way as the Atlas Syringe Pump in standalone
mode)
During dosing commands a maximum temperature can be set to pause the
Atlas Syringe Pumps in the case of an exothermic reaction.
The valves are user changeable and are available in a number of different port
options. Each of the ports on each valve can be configured to be an input
or output, therefore, with a 6 port valve it is possible to pump from up to 5
sources to one reactor, etc. per syringe. The syringes are also user changeable
and come in a variety of sizes, corresponding to a variety of flow rate ranges.
Use the Atlas Pump Pressurized Input Store to enable an inert gas blanket over
the samples to be pumped and to minimize cavitation/bubbles.
Features common to the Atlas Syringe Pump and Atlas Syringe Pump XL:
• Chemical Resistance: All wetted parts made from glass, PTFE and PCFE
• Maximum Pressure: 6 bar
• Number of Syringes: 2
• Number of Valves: 2
www.syrris.com
3
Atlas Specific Parts
Syringe Pumps
Atlas Syringe Pump
2200072
Atlas Syringe Pump - without Valves or Syringes
2200100
The Atlas Syringe Pump (2200072) is supplied with two 4 port valves and two
2.5ml syringes by default. The Atlas Syringe Pump without Valves or Syringes
(2200100) allows valves and syringes to be purchased separately.
Atlas Syringe Pump Features:
• Options for Syringe Sizes: 50μl, 100μl, 250μl, 500μl, 1ml, 2.5ml or 5ml
• Options for Number of Ports per Valve: 2, 3, 4 or 6
• Minimum Flow Rate in Continuous Mode: 20% of syringe volume per
minute (e.g. 10μl/min when using 50μl syringes)
• Minimum Flow Rate in Dual Dosing Mode: 1% of syringe volume per
minute (e.g. 0.5μl/min using a 50μl syringe)
• Maximum Flow Rate in Continuous Mode: 400% of syringe volume (e.g.
20ml/min with 5ml). Note that much higher rates are possible with the
Atlas Pressurized Input Store.
• Maximum Flow Rate in Dual Dosing Mode: 400% of syringe volume (e.g.
20ml/min with 5ml). Note that much higher rates are possible with the
Atlas Pressurized Input Store.
Flow Rate range for the Atlas Syringe Pump (2200072) in μl:
Min Flow Rate μl/min
Syringe Size
(μl)
50
100
250
500
1000
2500
5000
4
www.syrris.com
Max Flow Rate μl/min
Continuous
Flow
Dual Dose
Mode
Continuous
Flow
Dual Dose
Mode
10
20
50
100
200
500
1000
0.5
1
2.5
5
10
25
50
200
400
1000
2000
4000
10000
20000
200
400
1000
2000
4000
10000
20000
Syringe Pumps
Atlas Specific Parts
Atlas Syringe Pump XL
2200376
Atlas Syringe Pump XL - without Valves or Syringes
2200316
The Atlas Syringe Pump XL (2200376) is supplied with two 4 port valves and
two 25ml syringes by default. The Atlas Syringe Pump XL without Valves or
Syringes (2200316) allows valves and syringes to be purchased separately.
Atlas Syringe Pump XL Features:
• Options for Syringe Sizes: 0.5ml, 1ml, 2.5ml, 5ml, 10ml, 25ml or 50ml
• Options for Number of Ports per Valve: 2, 3, 4, 6 or 8
• Minimum Flow Rate in Continuous Mode: 20% of syringe volume per
minute (e.g. 100μl/min when using 0.5ml syringes)
• Minimum Flow Rate in Dual Dosing Mode: 1% of syringe volume per
minute (e.g. 50μl/min using a 0.5ml syringe)
• Maximum Flow Rate in Continuous Mode: 400% of syringe volume (e.g.
200ml/min with 50ml). Note that much higher rates are possible with the
Atlas Pressurized Input Store.
• Maximum Flow Rate in Dual Dosing Mode: 400% of syringe volume (e.g.
200ml/min with 50ml). Note that much higher rates are possible with the
Atlas Pressurized Input Store.
Flow Rate range for the Atlas Syringe Pump XL (2200376) in ml:
Min Flow Rate ml/min
Syringe Size
(ml)
Max Flow Rate ml/min
Continuous
Flow
Dual Dose
Mode
Continuous
Flow
Dual Dose
Mode
0.1
0.2
0.5
1
2
5
10
0.005
0.01
0.025
0.05
0.1
0.25
0.5
2
4
10
20
40
100
200
2
4
10
20
40
100
200
0.5
1
2.5
5
10
25
50
Note that some combinations of valves and syringes on the Atlas XL Pump can make
up to 3 valve ports inaccessible. Please see the compatibility chart in the valves
section (see page 30).
www.syrris.com
5
Atlas Specific Parts
Syringe Pumps
Autosampler Module (for Atlas Syringe Pumps)
2200196
The Autosampler Module is designed for use with the Atlas Syringe Pump or
Atlas Syringe Pump XL and Autosampler Probe (2200197) to aspirate up to 6
samples (when using 6 port valves) from a reactor at user defined intervals.
The Autosampler Module, which can be mounted on the extra pair of Support
Rods provided, holds 6 x 2ml HPLC vials and is located, in a fluidic sense,
between the Atlas Syringe Pump and the Autosampler Probe. The Atlas Syringe
pumps can sequentially aspirate samples from the reactor into the vials (which
can contain a chemical quench if required).
Autosampler Probe (for Atlas Syringe Pumps)
2200197
The Autosampler Probe is designed for use with the Atlas Syringe Pump or
Atlas Syringe Pump XL and Autosampler Module (2200196) to aspirate up to
6 samples (when using 6 port valves) from a reactor into HPLC vials at user
defined intervals.
The Autosampler Probe consists of 6 PTFE pipes held in a chemically resistant
(PTFE and glass) sheath, which can be located in a Jacketed Vessel Lid port
using the probe holder included. Each of the PTFE pipes is connected to the
Autosampler Module during use.
Autosampler Probe Filter (Cap and 5 Filters)
RD2200463
The Autosampler Probe Filters fit over the end of the Autosampler Probe
(2200197) and minimizes the likelihood of blocking the pipes when aspirating
samples. The filters are manufactured from PTFE and have a pore size of 10μm.
Atlas Pump Pressurized Input Store
2200475
This module enables reagents pumped by the Atlas Syringe Pump (2200072) or
Atlas Syringe Pump XL (2200376) to be conveniently stored in up to 4 x 250ml
bottles under an inert gas blanket. The module accepts gas at pressures from
1 to 10 bar and automatically regulates the pressure inside the bottles to 1 bar.
This 1 bar pressure avoids a partial vacuum forming when the pump aspirates
and therefore allows higher flow rates, the use of more viscous solvents and
eliminates bubble formation, resulting in the most accurate pumping possible.
The pressurizable bottles include PTFE filters to prolong the life of the pump
valves and syringes and a septum in the cap to enable filling/emptying via a
canula.
PTFE Input filters for 5μm for 3.2mm diameter (pack of 5)
2200594
A pack of 5 PTFE filters that push on to 3.2mm OD pipe and are ideal for
fitting on the input pipes of the Atlas Syringe Pumps. Filtering out particles can
increase the life of the syringes and valves. Due to the flow restriction caused,
these filters are best used at low flow rates or with the Atlas Pump Pressurized
Input Store (2200475).
6
www.syrris.com
Syringe Pumps
Atlas Specific Parts
2 Port Valve (PTFE/PCTFE) for Atlas Pump
2200089
3 Port Valve (PTFE/PCTFE) for Atlas Pump
2200090
4 Port Valve (PTFE/PCTFE) for Atlas Pump
2200091
6 Port Valve (PTFE/PCTFE) for Atlas Pump
2200092
Various valve types depending on number of inputs and outputs required for
Atlas Syringe Pump (2200072 and 2200100).
3 Port Valve (PTFE/PCTFE) for Atlas XL Pump
2200384
4 Port Valve (PTFE/PCTFE) for Atlas XL Pump
2200385
6 Port Valve (PTFE/PCTFE) for Atlas XL Pump
2200386
8 Port Valve (PTFE/PCTFE) for Atlas XL Pump
2200387
Various valve types depending on number of inputs and outputs required for
Atlas Syringe Pump XL (2200376 and 2200316).
The following table highlights the compatibility between syringes and valves for
the Atlas XL pump:
500μl
1ml
2.5ml
5ml
10ml
25ml
50ml
3-Way
4-Way
6-Way
8-Way
ü
ü
ü
ü
ü
ü
ü
ü
ü
ü
ü
ü
ü
1*
1*
1*
1
1
1
1
1*
1*
1*
1
1
1
3
2
Key
ü
No Conflict
n*
Number of port positions partially blocked (can be accessed with compact
fitting pipe end fitting and gripper)
n
Number of port positions totally blocked (no suitable fittings)
Syringe for Atlas Pump - 50μl 2200093
Syringe for Atlas Pump - 100μl2200094
Syringe for Atlas Pump - 250μl2200095
Syringe for Atlas Pump - 500μl2200096
www.syrris.com
7
Atlas Specific Parts
Syringe Pumps
Syringe for Atlas Pump - 1ml
2200097
Syringe for Atlas Pump - 2.5ml
2200098
Syringe for Atlas Pump - 5ml
2200099
Various sized syringes for Atlas Syringe Pump (2200072 and 2200100).
Syringes are made from glass with PTFE plungers for excellent chemical
resistance.
Syringe for Atlas XL Pump - 500μl2200377
Syringe for Atlas XL Pump - 1.0ml
2200378
Syringe for Atlas XL Pump - 2.5ml
2200379
Syringe for Atlas XL Pump - 5ml
2200380
Syringe for Atlas XL Pump - 10ml
2200381
Syringe for Atlas XL Pump - 25ml
2200382
Syringe for Atlas XL Pump - 50ml
2200383
Various sized syringes for Atlas Syringe Pump XL (2200376 and 2200316).
Syringes are made from glass with PTFE plungers for excellent chemical
resistance.
Pipe End Fittings for Atlas Syringe Pump - Tefzel 1.6mm
2200198
Pipe End Fittings for Atlas Syringe Pump - Tefzel 3.2mm
2200199
A pack of 10 pairs of flangeless ferrules and ¼-28 fittings for either 1.6mm or
3.2mm pipe.
8
www.syrris.com
PTFE Pipe 1.6mm OD x 0.5mm ID x 10mm
2200301
PTFE Pipe 1.6mm OD x 0.8mm ID x 10mm
2200302
PTFE Pipe 3.2mm OD x 1.5mm ID x 10mm
2200303
The Atlas Syringe Pumps are designed and manufactured by Syrris,
the world’s most advanced provider of laboratory scale chemistry
systems.
Syrris’ network of offices in the UK, USA, Japan, India and Brazil plus
over 35 distributors worldwide offer local service and support.
Contact us now at:
www.syrris.com
Download Syrris' Batch Chemistry Reactors Catalogue
www.syrris.com/downloads
Syrris Ltd. (Europe and Rest of World)
Syrris Inc. (North America)
T: +44 (0)1763 242555
E: info@syrris.com
W: www.syrris.com
T: 617 848 2997
E: info-usa@syrris.com
W: www.syrris.com
Syrris Japan, Inc.
Syrris India
Syrris Brasil
T: 045 263 8211
E: info@syrris.co.jp
W: www.syrris.co.jp
T: +91 22 2686 4410
E: info@syrris.com
W: www.syrris.com
T: +55 11 5083 4963
E: info@syrris.com
W: www.syrris.com.br
v1.0