ppfrc - Construction Materials Research Group (CMRG)
Transcription
ppfrc - Construction Materials Research Group (CMRG)
REPORT MECHANICAL PROPERTIES OF POLYPROPYLENE FIBRE REINFORCED CONCRETE (PPFRC) AND STRUCTURAL APPLICATIONS BY SHEHNILA FATIMA June, 2013 DEPARTMENT OF CIVIL ENGINEERING NED UNIVERSITY OF ENGINEERING AND TECHNOLOGY, KARACHI, PAKISTAN i TABLE OF CONTENTS TITLE PAGE Page i TABLE OF CONTENTS ii LIST OF TABLES vi LIST OF FIGURES vii LIST OF ACRONYMS xv LIST OF NOTATIONS xvi ABSTRACT xvii ACKNOWLEDGEMENT xviii DEDICATION xix CHAPTER 1: INTRODUCTION 1.1 BACKGROUND 1 1.2 OBJECTIVE AND SCOPE 3 1.3 RESEARCH SIGNIFICANCE 4 1.4 METHODOLOGY 4 1.5 ORGANIZATION OF THE THESIS 5 CHAPTER 2: LITERATURE REVIEW 2.1 INTRODUCTION 6 2.1.1 HISTORICAL EVOLUTION OF FRCC 6 2.1.2 CLASSIFICATION OF FIBRES 6 2.1.3 FIBRILLATED POLYPROPYLENE FIBRE 7 2.1.4 FIBRE REINFORCED CEMENTITIOUS COMPOSITES 8 2.2 FRESH (PLASTIC) PPFRC 9 ii 2.2.1 WORKABILITY 9 2.2.2 EARLY AGE AND PLASTIC SHRINKAGE 2.3 HAREDENED PPFRC 12 21 1.1.1. COMPRESSIVE STRENGTH OF PPFRC 21 1.1.2. TENSILE STRENGTH OF PPFRC 22 1.1.3. FLEXURE STRENGTH PPFRC 23 TABLES 25 FIGURES 27 CHAPTER 3: EXPERIMENTAL PROGRAM 3.1 GENERAL 30 3.2 MATERIALS 30 3.2.1 CEMENT 30 3.2.2 AGGREGATES 30 3.2.3 WATER 31 3.2.4 FIBER 31 3.2.5 ADMIXTURE 31 3.3 MIX DESIGN 31 3.4 TESTS FOR WORKABILITY OF FRESH PPFRC 32 3.4.1 STANDARD SLUMP TEST (ASTM C143) 32 3.4.2 COMPACTING FACTOR TEST (BS 1811-103) 33 3.4.3 FLOW TABLE (ASTM C1437) 34 3.4.4 J-RING TEST (ASTM1621) 35 3.4.5 L-BOX TEST 35 3.4.6 V-FUNNEL TEST 36 3.5 TESTS FOR PLASTIC SHRINKAGE OF FRESH PPFRC 37 3.6 TESTS FOR MECHANICAL PROPERTIES OF HARDENED PPFRC 38 3.6.1 COMPRESSIVE STRESS-STRAIN CURVE (ASTM C39) 39 3.6.2 SPLITTING TENSILE STRENGTH OF CONCRETE CYLINDERS (ASTM C496) 39 3.6.3 FLEXURE STRENGTH OF CONCRETE BEAMS (ASTM C78) 40 TABLES 42 FIGURES 46 iii CHAPTER 4: RESULTS AND DISCUSSION 4.1 INTRODUCTION 57 4.2 WORKABILITY OF FRESH PPFRC 57 4.3 PLASTIC SHRINKAGE OF FRESH PPFRC 59 4.4 MECHANICAL PROPERTTIES OF HARDENED PPFRC 60 4.4.1 COMPRESSION TEST RESULTS 61 4.4.2 SPLITTING CYLINDER TENSILE TEST RESULTS 62 4.4.3 FLEXURAL (INDIRECT TENSILE) TEST RESULTS 63 TABLES FIGURES CHAPTER 5: 65 68 ANALYTICAL WORK 5.1 INTRODUCTION 104 5.2 FRACTIONAL EQUATION FOR COMPRESSIVE STRESS STRAIN CURVE FOR PPFRC 104 5.3 COMPARISION BETWEEN EXPERIMENTAL RESULTS ANALYTICAL EXPRESSION 105 5.4 SIMPLIFICATION OF CONSTANTS IN FRACTIONAL EQUATION 105 TABLES FIGURES 107 108 CHAPTER 6: APPLICATIONS OF PPFRC IN CIVIL INFRASTRCUTURE 6.1 INTRODUCTION 113 6.2 APPLICATIONS IN BUILDINGS 114 6.3 APPLICATIONS IN BRIDGES 114 6.4 APPLICATIONS IN HIGHWAY PAVEMENTS 114 6.5 APPLICATIONS IN INDUSTRIAL FLOORING 115 6.6 APPLICATIONS IN DAMS AND HYDRAULIC STRUCTURES 115 6.7 APPLICATIONS IN BLAST RESISTANCE 115 6.8 APPLICATIONS IN SEWAGE AND WASTE WATER MANAGEMENT 116 6.9 OTHER APPLICATIONS 116 TABLES 117 FIGURES 118 iv CHAPTER 7: CONCLUSIONS AND RECOMMENDATIONS 7.1 CONCLUSIONS 124 7.2 RECOMMENDATIONS 125 APPENDICES 126 REFERENCES 139 v LIST OF TABLES Table 2.1 A compilation of mechanical properties of commonly used fibres in concrete materials [ACI 544.5R, (2010)] Table 2.2 Properties of different types of polypropylene fibres [S.K. Singh, (2010)] Table 3.1 Polypropylene technical data sheet (MATRIXX) Table 3.2 Mix proportion of concrete mixtures in Kg/m³ Table 3.3 Experimental matrix for workability tests Table 3.4 Experimental matrix for shrinkage tests Table 3.5 Experimental matrix for mechanical properties Table 4.1 Test results of various fresh properties tests of PC and PPFRC with different volume fraction and length of fibre Table 4.2 Shrinkage test results of PC and PPFRC Table 4.3 Weight measurements of PC and PPFRC Table 4.4 Weight loss percentage of PC and PPFRC Table 4.5 Displacement ductility calculated from experimental results for the flexure tests of PC and PPFRC with different volume fraction and length of fibre Table 5.1 Calibrated constants of the fractional equation for PC (Plain) concrete for different strengths of concrete [Ahmad and Shah (1979, 1982, 1985)] Table 5.2 Calibrated constants of the fractional equation for PPFRC with different Lf and Vf . Table 6.1 Typical dosages of PPFRC for various applications (MATRIXX Company) vi LIST OF FIGURES Figure 2.1 Main characteristics of fibres [Naaman et al, (2006)] Figure 2.2 Composite model of FRC with two main components, namely fibre and matrix [Naaman et al, (2006)] Figure 2.3 Simplified general classifications of FRC composites based on their tensile stress-strain response [Naaman et al, (2007)] Figure 2.4 Typical stress-strain or elongation curve in tension up to complete separation: (a) Conventional strain-softening FRC composites; (b) Strain-hardening FRC composites [Naaman et al, (2007)] Figure 2.5 Schematic stress-strain behaviour of cementitious matrix in tension [Gregor Fischer, (2004)] Figure 3.1 Fibrillated polypropylene fibre Figure 3.2 Polypropylene fibres of different length Figure 3.3 The average compressive strength-time curve of 2”x2” mortar cubes Figure 3.4 Pictorial view of rotary drum mixer Figure 3.5 Pictorial view of freshly prepared FFRRC Figure 3.6 Pictorial view of standard slump test apparatus [Eric et al (2003)] Figure 3.7 Types of concrete slump[Eric et al (2003)] Figure 3.8 Compacting factor test apparatus [Eric et al (2003)] Figure 3.9 Pictorial view of flow table test apparatus [Technical Bulletin 1506] Figure 3.10 Pictorial view of J-ring test apparatus [Eric et al (2003)] Figure 3.11 Pictorial view of L-box test apparatus [Eric et al (2003)] Figure 3.12 Pictorial view of V-funnel test apparatus [Eric et al (2003)] Figure 3.13 Pictorial view of shrinkage moulds lined with plastic sheets vii Figure 3.14 Pictorial view of shrinkage specimen after casting Figure 3.15 Pictorial view of length measurement instrument Figure 3.16 Schematic view of standard shrinkage specimen Figure 3.17 The universal testing machine Figure 3.18 Schematic diagram of the compressive strength test setup Figure 3.19 Schematic diagram of the tensile split test setup Figure 3.20 Flexure test beam profile and section Figure 3.21 Schematic diagram for flexure test Figure 3.22 Pictorial view of the loading assembly for two-point flexure test Figure 3.23 Pictorial view of the PPFRC beam while flexure test Figure 4.1 Pictorial view of the slump cone after the removal of the standard slump cone for PPFRC trial mix Figure 4.2 Pictorial view of measurement of the weight of partially compacted fresh concrete for evaluating Compacting factor Figure 4.3 Pictorial view of measurement of the diameter of fresh concrete after flow table test for PC. Figure 4.4 Pictorial view of J-Ring test for PC Figure 4.5 Pictorial view of J-Ring test for PPFRC 0.8-25 Figure 4.6 Pictoria view of L-Box test for PC Figure 4.7 Pictorial view of L-Box test for PPFRC 0.8-38 Figure 4.8 Pictorial view of V-Funnel test for PC Figure 4.9 Effect of fibre length (Lf ) on slump. Figure 4.10 Effect of Fibre volume fraction (Vf ) on slump Figure 4.11 Relationship between slump and compacting factor viii Figure 4.12 Relationship between slump and flow table diameter Figure 4.13 Pictorial view of length measurement for PPFRC specimen Figure 4.14 Average shrinkage-time curve for PC and PPFRC Figure 4.15 Average weight loss-time curve for PC and PPFRC Figure 4.16 Pictorial views of PPC and PPFRC specimens under compressive strength test. Figure 4.17 Pictorial views of PC and PPFRC specimens after compressive strength test. Figure 4.18 Effect of Vf on average compressive stress-strain curve for PC and PPFRC with 25 mm long fibres at 7 days. Figure 4.19 Effect of Vf on average compressive stress-strain curve for PC and PPFRC with 38 mm long fibres at 7 days Figure 4.20 Effect of Vf on average compressive stress-strain curve for PC and PPFRC with 25 mm long fibres at 14 days. Figure 4.21 Effect of Vf on average compressive stress-strain curve for PC and PPFRC with 38 mm long fibres at 14 days. Figure 4.22 Effect of Vf on average compressive stress-strain curve for PC and PPFRC with 25 mm fibres at 28 days Figure 4.23 Effect of Vf on average compressive stress-strain curve for PC and PPFRC with 38 mm fibres at 28 days Figure 4.24 Effect of Lf on average compressive stress-strain curve for PC and PPFRC with 0.4% volume fraction of PPF at 7 days Figure 4.25 Effect of Lf on average compressive stress-strain curve for PC and PPFRC with 0.6% volume fraction of PPF at 7 days. Figure 4.26 Effect of Lf on average compressive stress-strain curve for PC and PPFRC with 0.8% volume fraction of PPF at 7 days. ix Figure 4.27 Effect of Lf on average compressive stress-strain curve for PC and PPFRC with 0.4% volume fraction of PPF at 14 days. Figure 4.28 Effect of Lf on average compressive stress-strain curve for PC and PPFRC with 0.6% volume fraction of PPF at 14 days. Figure 4.29 Effect of Lf on average compressive stress-strain curve for PC and PPFRC with 0.8% volume fraction of PPF at 14 days Figure 4.30 Effect of Lf on average compressive stress-strain curve for PC and PPFRC with 0.4% volume fraction of PPF at 28 days. Figure 4.31 Effect of Lf on average compressive stress-strain curve for PC and PPFRC with 0.6% volume fraction of PPF at 28 days Figure 4.32 Effect of Lf on average compressive stress-strain curve for PC and PPFRC with 0.8% volume fraction of PPF at 28 days Figure 4.33 Effect of Vf on average compressive strength-time curve for PC and PPFRC with 25 mm long PP fibres. Figure 4.34 Effect of Vf on average compressive strength-time curve for PC and PPFRC with 38 mm long PP fibres. Figure 4.35 Effect of Lf on average compressive strength-time curve for PPFRC with 0.4% volume fraction of PP fibres. Figure 4.36 Effect of Lf on average compressive strength-time curve for PPFRC with 0.6% volume fraction of PP fibres. Figure 4.37 Effect of Lf on average compressive strength-time curve for PPFRC with 0.8% volume fraction of PP fibres. Figure 4.38 Average splitting tensile stress-displacement curve for PC at 7 days Figure 4.39 Pictorial view of PC specimen under split tensile strength test. Figure 4.40 Effect of Vf on average splitting tensile stress-displacement curve for PC and PPFRC with 25 mm long fibres at 7 days. x Figure 4.41 Effect of Vf on average splitting tensile stress-displacement curve for PC and PPFRC with 38 mm long fibres at 7 days. Figure 4.42 Effect of Vf on average splitting tensile stress-displacement curve for PC and PPFRC with 25 mm long fibres at 14 days. Figure 4.43 Effect of Vf on average splitting tensile stress-displacement curve for PC and PPFRC with 38 mm long fibres at 14 days. Figure 4.44 Effect of Vf on average splitting tensile stress-displacement curve for PC and PPFRC with 25 mm fibres at 28 days. Figure 4.45 Effect of Vf on average splitting tensile stress-displacement curve for PC and PPFRC with 38 mm fibres at 28 days. Figure 4.46 Effect of Lf on average splitting tensile stress-displacement curve for PC and PPFRC with 0.4% volume fraction of PPF at 7 days. Figure 4.47 Effect of Lf on average splitting tensile stress-displacement curve for PC and PPFRC with 0.6% volume fraction of PPF at 7 days Figure 4.48 Effect of Lf on average splitting tensile stress-displacement curve for PC and PPFRC with 0.8% volume fraction of PPF at 7 days Figure 4.49 Effect of Lf on average splitting tensile stress-displacement curve for PC and PPFRC with 0.4% volume fraction of PPF at 14 days. Figure 4.50 Effect of Lf on average splitting tensile stress-displacement curve for PC and PPFRC with 0.6% volume fraction of PPF at 14 days. Figure 4.51 Effect of Lf on average splitting tensile stress-displacement curve for PC and PPFRC with 0.8% volume fraction of PPF at 14 days. Figure 4.52 Effect of Lf on average splitting tensile stress-displacement curve for PC and PPFRC with 0.4% volume fraction of PPF at 28 days. Figure 4.53 Effect of Lf on average splitting tensile stress-displacement curve for PC and PPFRC with 0.6% volume fraction of PPF at 28 days. xi Figure 4.54 Effect of Lf on average splitting tensile stress-displacement curve for PC and PPFRC with 0.8% volume fraction of PPF at 28 days. Figure 4.55 Pictorial view of crack propagation of PPFRC cylinder under splitting tensile test. Figure 4.56 Pictorial view of the split PPFRC cylinder Figure 4.57 Effect of Vf on average splitting tensile strength-time curve for PC and PPFRC with 25 mm long PP fibres Figure 4.58 Effect of Vf on average splitting tensile strength-time curve for PC and PPFRC with 38 mm long PP fibres. Figure 4.59 Effect of Lf on average splitting tensile strength-time curve for PPFRC with 0.4% volume fraction of PP fibre Figure 4.60 Effect of Lf on average splitting tensile strength-time curve for PPFRC with 0.6% volume fraction of PP fibre Figure 4.61 Effect of Lf on average splitting tensile strength-time curve for PPFRC with 0.8% volume fraction of PP fibre Figure 4.62 Pictorial view of the loading assembly for the two-point load flexure test. Figure 4.63 Pictorial view of the PC beam after failure. Figure 4.64 Pictorial view of the PPFRC beam during flexure testing, showing wide crack and vertical displacement Figure 4.65 Pictorial view of the PPFRC beam after collapse. Figure 4.66 Pictorial view of the PC and PPFRC beam fractured surface after failure. Figure 4.67 Effect of Vf on average flexure stress-displacement curve for PC and PPFRC with 25 mm fibres at 28 days. Figure 4.68 Effect of Vf on average flexure stress-displacement curve for PC and PPFRC with 38 mm fibres at 28 days. xii Figure 4.69 Effect of Lf on average flexure stress-displacement curve for PC and PPFRC with 0.4% volume fraction of fibres at 28 days. Figure 4.70 Effect of Lf on average flexure stress-displacement curve for PC and PPFRC with 0.6% volume fraction of fibres at 28 days. Figure 4.71 Effect of Lf on average flexure stress-displacement curve for PC and PPFRC with 0.8% volume fraction of fibres at 28 days. Figure 5.1 Typical analytical stress-strain curves of plain conrete of various strengths (Ahmad and Shah, 1982) Figure 5.2 Comparison of experimental and analytical compressive stress-strain curve for PC at 28 days Figure 5.3 Comparison of experimental and analytical compressive stress-strain curve for PPFRC 0.4-25 at 28 days Figure 5.4 Comparison of experimental and analytical compressive stress-strain curve for PPFRC 0.6-25 at 28 days Figure 5.5 Comparison of experimental and analytical compressive stress-strain curve for PPFRC 0.8-25 at 28 days Figure 5.6 Comparison of experimental and analytical compressive stress-strain curve for PPFRC 0.4-38 at 28 days Figure 5.7 Comparison of experimental and analytical compressive stress-strain curve for PPFRC 0.6-38 at 28 days Figure 5.8 Comparison of experimental and analytical compressive stress-strain curve for PPFRC 0.8-38 at 28 days Figure 6.1 Application of PPFRC for plastering in multi-storeyed building, Mehrunnisa Welfare Trust, Korangi, Karachi, Pakistan Figure 6.2 Application of PPFRC in roof screeding, Creek Vista, DHA, Karachi, Pakistan Figure 6.3 Application of PPFRC in Jam Sadiq Bridge deck and expansion joint at KPT Interchange, Karachi, Pakistan xiii Figure 6.4 Application of PPFRC in steel free pavements at Shaheen Air, Jinnah Airport, Karachi, Pakistan Figure 6.5 Application of PPFRC in industrial flooring of Razi & Sons, Port Qasim, Karachi, Pakistan. Figure 6.6 Application of PPFRC in the construction of water reservoir at Diamond Terrace, Gulshan-e-Maymar, Karachi, Pakistan. Figure 6.7 Application of PPFRC for blast resistance, Military College of Engineering, Risalpur, Pakistan Figure 6.8 Applications of PPFRC for sewage channel, Khayaban-e-Jami, DHA, Karachi, Pakistan Figure 6.9 Application of PPFRC for man holes in industrial zone, Landhi, North Karachi, Pakistan Figure 6.10 Application of PPFRC to reduce shrinkage cracking in column footing, Karachi, Pakistan Figure 6.11 Application of PPFRC to reduce abrasion resistance in concrete pavement, Karachi, Pakistan. xiv LIST OF ACRONYMS RC Reinforced Concrete FRC Fibre reinforced concrete PPFRC Polypropylene Fibre Reinforced Concrete PPF Polypropylene fibres ASTM American Society for Testing Material ACI American Concrete Institute SCC Self-Consolidating Concrete MSFRSCC Micro-Synthetic Fibre Reinforced Self Consolidating Concrete PC Plain concrete SNFRC Synthetic fibrous concrete WWF Welded-wire fabric PVA Polyvinyl alcohol HDPE High-density polyethylene FMF Flexible metallic fibres MR Modulus of Rupture UTM Universal Testing Machine FMF Flexible metallic fibres xv LIST OF NOTATIONS Lf = Length of fibre Vf = Volume fraction of fibre ΔL = Length change of specimen at any age, % L= Comparator reading of the specimen at known time interval G= Gage length (initial L) T= Splitting tensile strength P= Maximum applied load indicated by the testing machine l= Length, in. (m) d= Diameter, in. (m). Ɛ'c = Peak strain (Ɛ'c) A, D = Constants for fractional equation xvi ABSTRACT The Polypropylene fibre reinforced concrete (PPFRC) contains randomly distributed short discrete Polypropylene fibres which act as internal reinforcement so as to enhance the properties of the cementitious composite (concrete). The principal reason for incorporating short discrete fibres into a cement matrix is to reduce cracking in the elastic range, increase the tensile strength and deformation capacity and increase the toughness of the resultant composite. These properties of PPFRC primarily depend upon length and volume of propylene fibres (PPF) used in the concrete mixture. In Pakistan the polypropylene fibre reinforced concrete (PPFRC) has seen limited applications in several structures. The applications are primarily to inhibit the cracking. However due to the lack of awareness, design guidelines and construction specifications, its uses are limited by the local construction industry. Therefore there is a need to develop information on the properties of Polypropylene Fibre Reinforced Concrete (PPFRC) in which indigenous polypropylene fibres are used in the concrete mixture. A combined experimental and analytical study was undertaken. For the study, fibrillated polypropylene fibres of two different lengths (lf) of 25 mm (1.00 in) and 38 mm (1.50 in) with 0.2%, 0.4% and 0.8% volume fractions (V f) of were used. The research reported in this study includes an experimental investigation for measurement of workability of PPFRC using two standard test methods to characterize consolidation and four methods for flow property of PPFRC, an experimental investigation to characterize selected mechanical properties of PPFRC and to study the effect of volume fraction of (PPF) and length of PPF on the mechanical properties and; development of an analytical model for predicting the stress-strain curves for PPFRC in compression. The comparison of the analytical model for compressive stress-strain curve of PPFRC with the experimental results is judged to be good. xvii ACKNOWLEDGEMENT Praise to Almighty Allah, the most gracious and the most merciful. Without His blessings and guidance our accomplishments would have never been possible. Financial support and sponsorship of MATRIXX Company, F-37/A, Block 4, Clifton, Karachi 75600, Pakistan, is gratefully acknowledged. Acknowledgement and gratitude is extended to all those people who lent support at various stages of this work. The author wishes to express deep gratitude and profound thanks to Prof. Dr. Shuaib H. Ahmad (Foreign Professor, Department of Civil Engineering); for his motivation encouragement & tremendous support and without whose encouragement and guidance this work would not have been possible. Acknowledgment of support is also extended to fellow graduate students and technicians in the laboratories of Civil Engineering Department at NED University of Engineering and Technology. Last but not least, the author’s wishes to thank and extend appreciation and gratitude to the members of the family & friends who supported the efforts throughout this study. xviii DEDICATION Dedicated to my loving parents Mr. and Mrs. Razi Muhammad Abidi and husband Mr. Syed Fahim Hyder Naqvi xix CHAPTER 7 CONCLUSIONS AND RECOMMENDATIONS 7.1. CONCLUSIONS Based on research work conducted in this study, following conclusions can be made. • The addition of polypropylene fibres reduces the flow characteristics and workability of the concrete mixture; however it also reduces bleeding and segregation in the concrete mixture. • The mixing, placing, finishing and consolidation of the Polypropylene fibre reinforced concrete (PPFRC) needs careful attention and control as the performance of PPFRC is greatly affected by these. • The polypropylene fibres (PPF) reduce early age shrinkage and moisture loss of the concrete mix even when low volume fractions of PPF are used. • Addition of the polypropylene fibres (PPF) has little or insignificant effect on the compressive strength of plain concrete. • Addition of the polypropylene fibres (PPF) increases the deformation capacity of concrete (in compression) and thus improves the material ductility of concrete. • Addition of the polypropylene fibres (PPF) increases the energy absorption capacity (area under the compression stress-strain curve) and thus improves the material ductility of concrete. • In compression, the mode of failure of PPFRC is different from that of plain concrete, as in the case of PPFRC, the fibres arrest the cracks, inhibit the fast growth of cracks and smear the cracks over a larger area. • In tension, the post peak behaviour of the PPFRC is very significantly improved from a perfect brittle behaviour for plain concrete to a relatively ductile behaviour. The addition of PPF fibres increase the post peak deformation capacity by bridging the cracks that appear as the concrete reaches its tensile strength. • In flexure loading (indirect tensile loading), the improvement in the behaviour due to the addition of the PPF is the similar to that in tension. The plain 124 concrete beams exhibit a very brittle behaviour, whereas PPFC beams showed ductile failure (increased deformation capacity) with formation of smeared and wide cracks. 7.2. RECOMMENDATIONS • The use of Polypropylene fibres (PPF) should be encouraged in various applications in civil infrastructure. • The PPFRC should be used in combination with plain concrete to obtain cost effectiveness. • The effect of PPF on the long term shrinkage and time dependent mechanical properties should also be studied. • This study was conducted on plain concrete. Beneficial effects of PPF on reinforced concrete for structural applications should also be studied. • Similar comprehensive studies should be conducted for hybrid FRC i.e. combination of Steel and Polypropylene fibres. 125 APPENDIX-I 126 Microsoft Excel Programme for generating stress-strain curves in compression Microsoft Excel Programme for generating stress-strain curves in splitting tension 127 Microsoft Excel Programme for generating stress-displacement curves in flexure 128 APPENDIX-II 129 List of projects where PPFRC was used in Concrete Pavement (MATRIXX, 2011) Project Name CONCRETE PAVEMENT Project Address PAF-Pakistan Air Force PAF-Pakistan Air Force Gatron Industries Novatex Industries Faisal House (Faisal Bank) Siemens Factory Pakistan Refinery Limited (PRL) KANUPP, Karachi Nuclear Power Plant Lucky Cement Factory Al-Abid Silk Mills Ltd Dewan Mushtaq Group P.S.O Kohat Cement Factory Concrete Runaway, Faisal Base, Karachi. Concrete Runaway, Pasni Base, Karachi. Hub Chowki, Balochistan. Korangi Industrial Area, Karachi. Car Parking, Shahrah-e-Faisal, Karachi. Generator Concrete Foundation, S.I.T.E., Karachi. Workshop Parking Area, Korangi, Karachi. Access Road, Paradise Point, Karachi. Nooriabad, Karachi. Industrial Concrete Pavement, Manghopir Road, Karachi. Khoski Sugar Mill, Sindh Keamari Oil Terminal-A, Karachi. Kohat, Pakistan. NHA-National Highway Authority Concrete Rigid Pavement, Sibbi Toll Plaza, Balochitan. Concrete Rigid Pavement, Dera Murad Jamali, Balochistan. Multan. Pavement, S.I.T.E. Karachi. Block-3, Clifton, Karachi. NHA-National Highway Authority City Developers Futehally Chemical Pvt Ltd CDGK, Ifza Park Zaiqa Food Industries Jinnah Hospital, Post Graduate Medical Centre S.C. Johnson’s Factory Weatherford Oil Tool Middle East Ltd Marine (Pvt) Ltd Mustaqim Dyeing & Printing Industries Yunus Textile Mills Limited Snow White Colgate Palmolive Pakistan Ltd, Factory D.A. Golf Club Jet Engine Testing House (PIA) Shaheen Air International Ltd Korangi Industrial Area, Karachi. Korangi Industrial Area. F.B. Industrial Area, Karachi. F.B. Industrial Area, Karachi. S.I.T.E., Bada Board, Karachi. Landhi Industrial Area, Karachi. Korangi, Karachi Karachi Phase-8, DHA, Karachi. Karachi Jinnah International Airport, Karachi Saya Industries Loading & Unloading Area, Site, Karachi National Industrial Parks Dry Dock International Power Global Developments Ltd PC Parking Karachi. Karachi Nuclear Power Plant U. G. Foods Barma Soap Port Qasim Authority, Karachi. Manora, Kpt, Karachi Karachi. Hubco Power Station, Hub, Balochistan Near PIDC Branch. Near Paradise point, Karachi. Bin Qasim, Karachi Karachi 130 List of projects where PPFRC was used in Industrial Flooring (MATRIXX, 2011) INDUSTRIAL FLOORING Project Name Project Address Warehouse Concrete Flooring, Hub Chowki, Gatron Industries Balochistan. Warehouse Concrete Flooring, Korangi NovaTex Industries Industrial Area, Khi. Warehouse Concrete Flooring, Korangi Allied Engineering & Services Ltd Industrial Area, Khi Warehouse Concrete Flooring, Hub Chowki, Baluchistan Wheels Ltd Balochistan. Warehouse Concrete Flooring, Keamari Oil Shell Pakistan Terminal, Khi. Warehouse Concrete Flooring, Korangi P.S.O. Gas Filling Station Industrial Area, Khi. Warehouse Concrete Flooring, 14 Km, PEL Pak Elektron Limited Ferozpur Road, Lhr. Warehouse Concrete Flooring, Korangi Valika Investment Industrial Area, Khi. Marine (Pvt) Ltd Warehouse Concrete Flooring, Karachi Warehouse Concrete Flooring, S.I.T.E., Maqbool GCP Ghee Mill Karachi. Colgate Palmolive Warehouse Concrete Flooring, Kotri, Sindh. Hub Power Company Warehouse Concrete Flooring, Hub. Gul Ahmed Textile Mills Ltd Factory Flooring, Landhi, Karachi. Factory Flooring, Super Highway (50 km), Lucky Textile Mill Extension Sindh. Gulf Chemicals (Pvt) Ltd Korangi Industrial, Karachi. Tuwairqi Steel Mills Ltd Bin Qasim Karachi Khas Traders Factory Korangi Industrial Area, Karachi. High Q Pharma Insitu Terrazzo Flooring, Karachi. Concrete Flooring at Car Parking, High-rise MCB Tower building, Karachi. Aga Khan Planning & Building Services Garden Road, Karachi. Kiran Gas (Pvt) Ltd Hub Chowki, Balochistan. Afroze Textile Industries (Pvt) Ltd S.I.T.E., Super Highway, Karachi. Shindler Futehally (Pvt) Ltd Karachi. Razi & Sons Port Qasim Industrial Zone, Karachi. Snow White Pavement, Korangi, Karachi Thal Engineering Korangi Industrial Area, Karachi. Syntech Fibres Factory Korangi Industrial Area, Karachi. LUMS Sports Complex. Lucky Textile Mill Quaidabad, Karachi. 131 Yunus Textile Mills Limited Jang Press DA Sunset Club Skyways Manufacturers (Pvt) Ltd Karachi Club Annex Expo Centre Hamsons Towel Industries Warid Telecom KESC, Record Room Pilot Social Welfare Complex, Habib Group Pakistan Atomic Energy Sui Southern Gas Company Ltd., SSGC Mustaqim Dyeing & Printing Industries Gertz Pharma (Pvt) Limited Fay Motors Pharma Evo PPL Sui Purification Plant Igloo Company Derwaish, Warehouse Sadr-Uddin & Sons Meridian International (Pvt) Ltd AG Sindh Complex Huffaz Seamless Pipe Industries Limited Landhi Industrial Area, Karachi. Sultanabad Maikalachi Road, Karachi. Khayaban-e-Jami, Phase II (Ext.), DHA, Karachi A/1-A-4, S.I.T.E., Karachi Lalazar M.T.Road, Karachi University Road, Karachi Karachi. Lahore. Near Zenab Market, Karachi. Malir (Near Rangers Head Quarter), Karachi. New-2, Qayyumabad, Karachi. Regional Building, Hyderabad. D/14, A S.I.T.E., Karachi Industrial Area, Karachi Sultan Ahmed Shah Road Karachi Port Qasim Authority, Karachi. Sui, Balochistan Cold Storage Karachi Shershah, Karachi Warehouse, Rashidabad, Karachi F-10 Markaz, Islamabad Karachi Karachi List of projects where PPFRC was used in Roof Screeding (MATRIXX, 2011) ROOF SCREEDING Project Name PAF-Pakistan Air Force Pakistan Security Printing Press PARCO Pak-Arab Refinery Limited Foundation Public School DHL Head Office Building Pakistan Navy, Special Children School Kiran Cancer Hospital Horizon Pharmaceutical TCS Overland Express Centre BP Pakistan Project Address Korangi Base, Karachi. Malir, Karachi. Korangi Creek Road, Karachi. Autoban Road, Hyderabad. Shahrah-e-Faisal, Karachi. Karsaz, Karachi. A project of Pakistan Atomic Energy, Karachi. Hill Park, Karachi. Office / Warehouse, Jinnah International Airport, Karachi. Karachi. 132 Hafiz Tannery NHA-National Housing Authority PC-Pearl Continental Hotel Creek Vistas, Creek City CAA Yunus Textile Mills Limited Adamjee Enterprises Agha Khan Estate Office Hub School Falcon Masjid Memon Medical Institute, MMI Hub Marble Factory Uni Brow Industries S. M. Public Husaini School Pakistan Atomic Energy Commission Aresha City Karachi Nuclear Power Plant IBA, Existing Academic Block Dairy Land Indigo Textile (Pvt) Ltd National Industrial Parks Allied Engineering & Services Ltd Afridi Motors Zia Uddin Hospital Oncology Department Karachi Nuclear Power Plant Educational Institute charity. Meezan Bank Ltd FFBL Korangi Industrial Area, Karachi. Sassui at N-5 Toll Plaza Control Building, Karachi. Gwadar, Balochistan. Phase 8, DHA, Karachi. Radar Station, Quaid-e-Azam Airport, Karachi. Landhi Industrial Area, Karachi. Adamjee Nager, Karachi FB Area, Karachi. At Dam Road. SDH Colony, Malir Cantt, Karachi. Safoora Goth, K.D.A., Scheme 33, Karachi. Marble City, Hub. S.I.T.E. Karachi. Nazimabad, Karachi. Workshop Building, Korangi, Karachi. Gulzar-e-Hijri, Scheme 33, Karachi. Pakistan Atomic Energy Commission. Main Campus IBA, Karachi I.I. Chundrigar Road, Karachi. Joreji Bin Qasim, Karachi Shahrah-e-Faisal, Karachi Korangi Industrial Area, Karachi Peshawar Nazimabad, Karachi. Near Paradise point, Karachi. North Nazimabad, Karachi. C-25, SITE, Karachi PQA, Karachi List of projects where PPFRC was used in Concrete Plastering (MATRIXX, 2011) CEMENT CONCRETE PLASTER Project Name Project Address Indus Hospital Korangi, Karachi. KPT-Karachi Port Trust, OP1 Karachi. Aga Khan Education Service School in Gilgit & Hunza. Madarsa Fatima-tuz-Zahra Khairpur, Sindh. Mehrunnisa Welfare Trust Korangi, Karachi. Techno Pak Telecom Tipu Sultan Road, Karachi. Bahria College NORE1 Karachi. Renovation Plaster, Jinnah Intl. Airport, Mercure Grand Hotel (Accor Hotel) Karachi. Dow Medical University & Hospital Safoora Goth, Karachi. 133 Pakistan Navy, Special Children School Crescent Investment Bank Aga Khan University & Hospital Asian Pharmaceutical (CCC) Siemens Grid Station Macter International (Pvt) Limited Askari 4 Housing Tollink Pakistan (Pvt) Ltd Squash Court Faisal Base Sindh Club The Aga Khan University Indus Pharma (Pvt) Ltd Telenor Building Bosicor Pakistan Limited Uch Power Plant SOS Village Government Boys & Girls School Usmani Colony Govt Girls & Boys School Sarjani Town Girls & Boys School Aresha City Star City GSK Glaxo Smith Kline Pharma Reckitt Benckiser Pakistan Ltd Zia Uddin Hospital Oncology Department Tayyaba Mosque Stock Exchange Building ERRA-60 School Projects Civil Hospital Cotton Exchange Building King Stone U. S. Consulate Degree College, Purification Plant Inaara Garden Immigration Tower Khairpur University Girls College Boys College Byco Trade Corporation of Pakistan Karsaz, Karachi. Phase-2 Extension. Sports Complex, Karachi. Renovation Works, Tipu Sultan Road, Karachi. Hub, Balochistan. Site, Karachi. Rashid Minhas Road, Karachi. Plaster & Screed Works Karachi. Abdullah Haroon Road, Karachi. Emergency Department, Karachi. Sector-27, KIA, Karachi. Near Centrum, Gulshan-e-Iqbal, Karachi Karachi Dera Murad Jamali, Balochistan. Malir Cantt, Karachi. Yousuf Goth, Karachi. Jail Road, Karachi. Sarjani, Karachi Gulzar-e-Hijri, Scheme 33, Karachi. Garden Road, Karachi. West Wharf, Karachi. Karachi. Nazimabad, Karachi. Islamabad Islamabad Northern Area of Pakistan. Karachi. I. I. Chundrigar Road, Karachi. Phase 6 DHA, Karachi, Plaster Mia Kolachi, Karachi Dheer Kot , Bagh, AJK Dharki Near Saadi Town, Karachi Islamabad Khairpur, Miras, Sindh Bagh, AJK Bagh, AJK Near Hubco Power Plant Khairpur. 134 ISM Hospital GSK Glaxo Smith Kline Pharma Allied Bank Office Building Pfizer Laboratories Ltd Near Sobhraj Hospital Garden, Karachi. Korangi Industrial Area, Karachi. Processing Zone Landhi, Karachi Karachi. List of projects where PPFRC was used in Underground Structures (MATRIXX, 2011) BASEMENT & UNDERGROUND STRUCTURE Project Name Project Address Basement Structure Concrete work, Dera Ismail Residential Villas for UAE Govt. Khan, Punjab Karachi Gym Khana Basement Concrete works, Karachi. Basement Concrete works, Gulshan-e-Maymar, Diamond Terrace Karachi. Mercure Grand Hotel (Accor Hotel) Slab on Grade, Jinnah Intl. Airport, Karachi. Colgate Palmolive Concrete Foundation Works, Kotri, Sindh. Government S.M. Public School, Nazimabad. Education & Health Works CDGK Karachi. Grey Tower Phase 5, DHA, Karachi Aresha City Near Hamdard University, Karachi. OGDCL Hyderabad Pakistan Refinery Limited (PRL) Korangi Creek Road, Karachi. List of projects where PPFRC was used in Bridges (MATRIXX, 2011) BRIDGES Project Name KPT Interchange Bridge KPT Fly Over Hasan Square Interchange Bridge Johar Mohr Bridge Quaidabad Bridge PICT Fly Over Gizri Fly Over Shershah Bridge Project Address Korangi Road, Karachi. Near Kemari, Karachi. Civic Center, Karachi. Gulshan-e-Jauhar, Karachi Quaidabad Chawrangi, Karachi. Karachi. Kh-e-Hafiz, Gizri Commercial Area, Gizri, Karachi. SITE, Karachi List of projects where PPFRC was used in Hydraulic Structures (MATRIXX, 2011) WATER TANKS & RESERVOIRS Inter Continental Hotel Swimming Pool Concrete Works, Islamabad. Zaver Pearl-Continental Hotel Water Reservoir Concrete Works, Gwadar. 135 DHA Caltex Oil Pvt Ltd Hamson (Pvt) Ltd Maymar Housing Services (Pvt) Ltd ACACIA Country & Golf Club Waste Water Treatment Plant Sindh Club Diamond Terrace Rashid Memorial Welfare Organization Star City National Refinery Limited Nur Farm Daily Khabrian SUPARCO Rehman Dying Centre Point Karachi Nuclear Power Plant Pakistan Atomic Energy Pakistan Benazir Bhutto International Airport Sofitel Hotel Tower IBA Main Campus Textile City Water Reservoir Concrete Works, Phase-VI, Karachi Underground, Korangi Industrial Area, Karachi. Water Retaining Structure, Landhi Industrial Zone, Karachi Water Retaining Structure, P.E.C.H.S., Karachi Water Retaining Structure, Karachi. Am Textile, Jarawala Road, Faisalabad. Abdullah Haroon Road, Karachi. Gulshan-e-Maymar, Karachi. 30 Km of Hyderabad. Opp Bambino Cinema Karachi Karachi. Canal Lining, Hyderabad Multan. Head Quarter, Safoora Goth, Karachi. Normal Water Tank Super High Way Site Trakker Tower, Shaheed-e-Millat, Karachi Near Paradise point, Karachi. Lahore. Islamabad Main Clifton Road, Karachi Karachi PQA, Karachi List of projects where PPFRC was used in Sewerage Drains (MATRIXX, 2011) SEWERAGE DRAINS Project Name Project Address Pakistan Defence Officers Housing Sewage Channel, Khy-e-Jami, DHA, Karachi Authority (DHA) KWSB Manhole, Landhi Industrial Zone, Karachi. KWSB Manhole, FB Industrial Zone, Karachi. KWSB Manhole, Korangi Industrial Zone, Karachi. Manhole, North Karachi Industrial Zone, KWSB Karachi. KWSB Manhole, Sherpao Industrial Zone, Karachi. Sewage Channel, Landhi Industrial Zone, KWSB Karachi. List of projects where PPFRC was used in Marine Structures (MATRIXX, 2011) MARINE STRUCTURES 136 Project Name Korangi Fisheries Harbour Authority KPT Karachi Port Trust Zara Textile Hyeworth Reckitt Benckiser Pakistan Ltd KPT, OP3, Oil Pair 3 Project Address Rehabilitation Concrete Work of Jetty, Chasma Goth, Karachi Floating Jetty East Wharf, Karachi Beach Hut, S-96, Sandspit, Karachi. Beach Hut, S-30, Sandspit, Karachi. Beach Hut, N-49, Sandspit, Karachi. Kemari List of projects where PPFRC was used in Precast Structures (MATRIXX, 2011) PRECAST STRUCTURES Project Name Project Address Marine Cable Cover, Hawks Bay, Arabian Sea PTCL Main Fiber Optic Line (Dubai) to Khi. AL-Mohammadi Tile D.I.H. Korangi, Karachi. Randhawa Pre-Cast Factory Landhi, Karachi. Concrete Measures Exporter of Paver, Stepping Stone, Karachi. Cellpor Building Solution DHA, Phase IV, Karachi. CONEX Phase-II Ext, DHA, Karachi Concrete Wizards Factory I-9, Islamabad. Concrete Core Korangi Industrial Area, Korangi, Karachi. Kumhar TerraCotta & Concrete Gulshan-e-Mehran Malir, Karachi Envision Consulate General of the Islamic Karachi Republic of Iran List of projects where PPFRC was used in Repair Applications (MATRIXX, 2011) CRACK REPAIR APPLICATORS Project Name Project Address Burhani Impex Bhora Pir, Karachi. Con-Link International North Nazimabad, Karachi. Techno Plus Gulshan-e-Iqbal, Karachi. Concrete Technology Karachi. Protection Technology Shahrah-e-Faisal, Karachi. Pak-Binder Karachi. Dubai Palace Karachi Parco Pipri 137 List of projects where PPFRC was used in Shotcrete Rehabilitation (MATRIXX, 2011) SHOTCRETE REHABILITATION Project Name Project Address Korangi Fisheries Harbour Authority Sea Marine Structure, Karachi. 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Ying Chen, 2008, “Plastic Shrinkage Properties of Baler Twine Fiber Reinforced Concrete” Department of Civil and Geological Engineering, University of Saskatchewan, Saskatoon. Zhiguo You et al, 2011, “Ductility and strength of hybrid fiber reinforced selfconsolidating concrete beam with low reinforcement ratios”, Systems Engineering Procedia 1, 28–34, International Conference on Risk and Engineering Management (REM). Ziad Bayasi et al, 1993, “Properties of Polypropylene Fiber Reinforced Concrete”, ACI Materials Journal, V. 90, No. 6. 143 CHAPTER 1 INTRODUCTION 1.1. BACKGROUND Concrete is the most commonly used construction material worldwide. In Pakistan, reinforced concrete (RC) is extensively used in the construction of variety of civil infrastructure applications including small and large buildings, houses, bridges, storage tanks, dams and numerous other types of structures in Pakistan. Concrete is a brittle, composite material that is strong in compression and weak in tension. The tensile strength of plain concrete is about 10% of its compressive strength. Cracking occurs when the concrete tensile stress produced from the externally applied loads, temperature changes, or shrinkage in a member reaches the tensile strength of the material. Formation of tensile cracks in reinforced concrete flexural members containing conventional, non-prestress reinforcement is usually unavoidable since concrete has a low tensile straining capacity. While cracks barely wide enough to be visible may be objectionable only because of appearance, cracks of greater width can be dangerous because of the possibility of corrosive agents attacking the steel reinforcing bars. Excessively wide cracks can also result in leakage in such structures as dams, tanks, and pools. In many of the cases this cracking is so significant that it may lead to failure of the structure. The deterioration of such structures is of great concern since the repairing and rehabilitation of these structures are time consuming and costly. Hence there is an intense need to take measures that can control the cracking of concrete and thus cause overall safety of a structure and increase its useful life. Use of short discrete fibres in cementitious composites (concrete) is one approach to mitigate the cracking and increasing the tensile straining capacity. 1 The fibre reinforced concrete (FRC) contains randomly distributed short discrete fibres which act as internal reinforcement so as to enhance the properties of the cementitious composite (concrete). The principal reason for incorporating short discrete fibres into a cement matrix is to increase the toughness and tensile strength, and to improve the cracking deformation characteristics of the resultant composite. These properties of FRC primarily depend upon the type of the fibres used in the concrete. Several different types of short discrete fibres have been used to reinforce concrete. The choice of fibres varies from synthetic organic materials such as polypropylene or carbon, synthetic inorganic such as steel or glass, natural organic such as cellulose or sisal to natural inorganic asbestos. Short discrete steel, glass, polyester and polypropylene fibres are most commonly being used as reinforcement to the FRC. The selection of the type of fibres is guided by the properties of the fibres such as diameter, specific gravity, young’s modulus, tensile strength etc. and the extent these fibres affect the properties of the cement matrix. Polypropylene fibres are chemically inert, and so will not rust, corrode or rot, and will not absorb water. Little or no flame spread on the surface of polypropylene fibre reinforced panels was reported in laboratory tests. The introduction of polypropylene fibres in concrete affects its properties both in fresh and hardened state. In fresh state it may reduce the workability and the also slows down the rate of bleeding. It may also increase the setting times for the concrete. However in hardened state, polypropylene fibres act as crack arrestors. Like any secondary reinforcement, the short discrete fibres tend to mitigate the crack propagation by bridging the cracks and providing increased resistance to crack propagation. Recently, fibrillated polypropylene fibres (lattice type structure when filament is opened up) have been introduced. The structure of the fibrillated polypropylene fibres is such that it provides three dimensional reinforcement to the cementitious matrix thus; enhancing tensile strength, tensile strain capacity and the improved resistance to impact and fatigue. 2 In Pakistan the polypropylene fibre reinforced concrete (PPFRC) has seen limited applications in several structures including parking areas, drive ways, industrial floorings, water and other chemical storage tanks, walkways, pavements, roof screeds, mosaic flooring, structural concrete and also in pre-cast slabs. The applications are primarily to inhibit the cracking. However due to the lack of awareness, design guidelines and construction specifications, its uses are limited by the local construction industry. Therefore there is a need to develop information on the properties of Polypropylene Fibre Reinforced Concrete (PPFRC) in which indigenous polypropylene fibres are used. 1.2. OBJECTIVE AND SCOPE The objectives of this research are: 1) Conduct experimental investigation for measurement of workability of Polypropylene Fibre Reinforced Concrete (PPFRC). 2) Conduct experimental and analytical investigation to characterize principal mechanical properties of PPFRC and to study the effect of volume fraction and length of polypropylene fibres (PPF) on the mechanical properties. The scope of this research is limited to the fibrillated polypropylene fibres of length 25 mm (1.00 in.) and 38 mm (1.50 in.). For the measurement of workability of the PPFRC, two standard methods are used for characterizing workability in terms of consolidation, however; four standard test methods are used to characterize the flow property of PPFRC. For the mechanical properties, the following tests are conducted to study the effect of amount of fibres and the length of fibres on the compressive, tensile and flexure strength and the associated straining capacity. 1) Compressive Strength of concrete cylinders (ASTM C39) 2) Split Tensile Strength of concrete cylinders (ASTM C496) 3) Flexure Strength of concrete beams under two point loading (ASTM C78) 3 The shrinkage characteristics of plain and PPFRC were studied using ASTM C157 standard test method. This method is used for measuring the length change of hardened mortar or concrete specimens. 1.3. RESEARCH SIGNIFICANCE The use of PPFRC in the local construction industry is limited. The purpose of this work is to develop evidence of the engineering properties of PPFRC in which indigenous polypropylene fibres are used. This includes the properties of PPFRC such as workability in fresh state, free shrinkage and other mechanical properties in hardened state. The results of this work will be useful for the local construction industry and could be used for developing specification guidelines for the use of PPPFC in the local construction. 1.4. METHODOLOGY The research methodology was to conduct a literature review of the studies on FRC and PPFRC that have been conducted in the past two decades. On the basis of the literature review, knowledge gaps were identified. It was realized that mechanical properties of Polypropylene fibre reinforced concrete have been studied by many researchers in different areas of world; however in Pakistan there still a need to provide experimental and knowledge ground for the use of PPFRC in the local construction industry. An experimental program was developed to study the properties of PPFRC in fresh and hardened state. The experimental program included number of variables such as the length of the PPF (Lf), amount of PPF (Vf), test age etc. Concrete mixture proportions for plain and PPRC concrete were developed to maintain a target slump. Using these PPFRC concrete mixes, test specimens were cast, cured and tested as per the experimental matrix. The results of the plain and PPFRC concrete test specimens were compared to quantify the beneficial effects of PPF on concrete. The results are discussed 4 and presented along with an analytical equation for characterizing the stress-strain curve of PPFRC in compression. 1.5. ORGANIZATION OF THE THESIS This report is organized into seven chapters. Details of each chapter are described as follows. 1. Chapter 1 gives an introduction to the report. 2. Chapter 2 presents a literature review of the researches related to the workability and mechanical properties of the PPFRC conducted in the past two decades. 3. Chapter 3 presents the experimental investigation that gives a detailed description about the materials, casting and curing of the test specimens, and the test set ups for the laboratory work. 4. Chapter 4 presents the test results and discussion of the results. 5. Chapter 5 gives analytical solution of the stress-strain curves of PPFRC in compression using fractional equation. 6. Chapter 6 indicates some common applications of PPFRC in civil infrastructure in Pakistan. 7. Chapter 7 summarizes the research work, presents conclusions and offers recommendations for future research. 5 CHAPTER 2 LITERATURE REVIEW 2.1. INTRODUCTION This chapter presents the review of studies conducted on the history, performance and behaviour of FRC and the properties of different fibres that affect the performance of the composite. The studies conducted in the past two decades are mainly focused. 2.1.1. Historical Evolution of FRCC The use of randomly distributed fibres in concrete is not new. Since ancient times, fibres like straws, horse hair and other vegetable fibres have been used to reinforce brittle materials [ACI 544.1R (1996)]. However after 1960’s, a great evolution took place in this regard and a number of different fibres and other materials were introduced to enhance the most significant mechanical properties of concrete. The use of those materials was supported by an extensive number of research results showing the ability of fibres to improve the mechanical properties and durability of concrete. Modern developments and world-wide interest on the subject took off during the early 1960’s following studies by Romualdi on the use of steel fibres in concrete [Romualdi et al (1964), Romualdi et al (1969)]. Use of glass fibres in concrete was first attempted in the late 1950s by Biryukovich [Biryukovich et al (1965)]. After this initial work, a substantial amount of research, development, experimentation, and industrial application of fibre reinforced concrete has occurred. 2.1.2. Classification of fibres A wide variety of fibres have been used in concrete. For each application it needs to be determined which type of fibre is optimal in satisfying the concrete application. The different types of fibres used as concrete reinforcement are synthetic fibres and steel 6 fibres. The different types of synthetic fibres used are Polypropylene, Nylon, Polythene, Polyester and Glass Fibres. For architectural and decorative concrete products and for prevention of early age cracking, synthetic fibres may be used. Steel fibres are used for applications where properties of concrete in the hardened stage have to be modified, namely, post crack flexural strength, abrasion resistance, impact resistance and shatter resistance of concrete [Clinton Pereira (2009)]. The majority of materials used in fibre production and the typical range of mechanical properties for each fibre type are summarized in Table 2.1 [ACI 544.5R (2010)]. A more comprehensive classification “system” of these fibres (Figure 2.1) is given by Naaman[(2006)]. In this system, the characteristics of the fibres are categorised into four, namely the geometrical properties, mechanical properties, physical/chemical properties and material type. For practical utilisation of fibres in FRC applications, properties which are given significant considerations in selection of fibres are material type, tensile strength, elastic modulus and the aspect ratio (the ratio of fibre length to the diameter or equivalent diameter). 2.1.3. Fibrillated Polypropylene Fibre Previously, problems were encountered in mixing, workability and durability of fibre reinforced concrete but these have almost been overcome by the emergence of new types of synthetic fibres. Polypropylene Fibre is one amongst them. The primary advantages of polypropylene fibre over others are its easily tailoring properties and its resistance against corrosive attack of the environment. Polypropylene fibres are actually man-made synthetic fibres resulted from research and development in the petrochemical and textile industries. These fibres derived from organic polymers which are available in a variety of formulations [ACI 544.1R (1996)]. 7 Table 2.2 gives physical properties of different types of Polypropylene Fibres namely, Monofilament, Microfilament and Fibrillated fibres [S. K. Singh (2010)]. 2.1.4. Fibre Reinforced Cementitious Composites ACI 544.3R-08 defines Fibre Reinforced Concrete, (FRC) as a composite material made of hydraulic cements, water, fine and coarse aggregate, and a dispersion of discontinuous fibres [ACI 544.3R (2008)]. Naaman proposed a composite model to define FRC as a composite with two main components, namely the fibre and the matrix, as indicated in Figure 2.2. In this model, both the fibre and the matrix are assumed to work together through bond, providing synergism for an effective composite [Naaman (2006)]. Naaman classified fibre reinforced cementitious composites into two broad categories according to their tensile response, namely, either Strain-Softening or Strain- Hardening. (Figure. 2.3) Strain-softening FRC composites (Figure. 2.4a) exhibit strain softening and crack localization immediately following first cracking whereas Strain-hardening FRC composites are characterized by a stress-strain response in tension that exhibits strain hardening behaviour after first cracking, accompanied by multiple cracking (Figure. 2.4b). First cracking here implies a through the section crack or percolating crack [Naaman (2007)]. Another classification of fibre reinforced cementitious materials on the basis of structural applications is given by Stang et al [(2004)]. According to that, the general mechanical response of these materials under uniaxial state of stress can be either of the three: i. Tension softening response is so significant that it can be allowed to be taken into account in structural design, ii. The strain hardening portion is significant enough that it can be taking into account in structural contexts, or iii. Both the hardening and the softening regimes are significant enough to be taken into account in structural design. 8 2.2. FRESH (PLASTIC) PPFRC 2.2.1. Workability American Concrete Institute (ACI) Standard 116R-90 defines workability as “that property of freshly mixed concrete which determines the ease and homogeneity with which it can be mixed, placed, consolidated, and finished.” [ACI 116R (1990)] Workability is the measure of the ability of concrete to be mixed, handled, transported, placed, and consolidated. Workability plays key role in the performance of hardened product. The strength and serviceability properties of FRC are greatly affected by the mixing, dispersion, consolidation and hydration of fresh FRC. Hence it is mandatory to ensure good flowability, placeability, segregation resistance and uniform dispersion of fibres in the fibre reinforced concrete. Fresh concrete properties and workability (flowability, passing ability and segregation resistance) determined by different methods were reported for polypropylene fibre reinforced concrete having different fibre content that is percentage by volume. Most of the studies conducted to evaluate the workability of the fibre reinforced concrete deal with the flow property of Self-Consolidating Concrete (SCC), which is one kind of high performance concrete. The main character of self-compacting concrete is that there is no need of vibrating during construction process, reducing manpower demand in the construction stages of concrete structures. Among those, most of the researchers have focused on the effect of steel fibres on the rheology of SCC mixtures and the development of steel fibre-reinforced self-consolidating concrete mixture design procedures [Toutanji et al (1998), Mustafa et al (2007), Li et al (2011), Abdulkadir et al (2007), Stähli et al ( 2008), B. Krishna Rao et al (2010), Mustafa Sahmaran et al (2005)]. Fewer studies [D. Forgeron et al (2010), S.K. Singh (2010)] have been conducted on synthetic fibre reinforcement and its effect on the flow characteristics of SCC. It is therefore important to study the flow characteristics of self-consolidating concrete mixtures that incorporate this type of synthetic fibre reinforcement in order to identify and characterise the main factors affecting its flow. 9 2.2.1.1. Uniform Dispersion of Fibres Mixing of FRC can be accomplished by several methods, with the choice of method depending on the job requirements and the facilities available. It is important to have a uniform dispersion of the fibres and to prevent the segregation or balling of the fibres during mixing. Balling of the fibres during mixing is related to a number of factors. The most important factors appear to be the Aspect Ratio of the fibres, the volume percentage of fibres, the maximum size and gradation of the aggregates, and the method of adding the fibres to the mixture. As the first three of these factors increase, the tendency for balling increases [A. L. Ardeshana et al (2012)]. Therefore, before mixing the concrete, the fibre length, amount and design mix variables are adjusted to prevent the fibres from balling. The aspect ratio for the fibres are usually restricted between 100 and 200 since fibres which are too long tend to "ball" in the mix and create workability problems. There should be sufficient compaction so that the fresh concrete flows satisfactorily and the PP fibres are uniformly dispersed in the mixture [S.K. Singh (2010)]. 2.2.1.2. Setting time Addition of fibres in concrete reduces the amount of bleed water form concrete and so the rate of bleeding decreases. The use of polypropylene fibres may increase the time to initial and final set of the concrete as this led to a slower rate of drying in the concrete [S.K. Singh (2010)]. Alhozaimy (1995) investigated the effect of polypropylene fibres on the initial and final setting time of concrete and found that the initial and final setting times were decreased by 9 and 27 percent, respectively, with the addition of polypropylene fibres. This reduction is expected to reduce the period of exposure prior to setting of fresh concrete to the dry environment, which is responsible for plastic shrinkage cracking. The amount of bleed water for plain and fibrous concretes was also reduced. Due to the addition of polypropylene fibres, there was an 18 percent decrease in the amount of bleed water of concrete; the fibres possibly reduce the settlement of heavier mix constituents (e.g., 10 aggregates), thereby reducing the upward movement of water (bleeding) in concrete [Alhozaimy et al (1995)]. 2.2.1.3. Filling Ability, Flowability and/or Passing Ability The main parameter, which is often used to determine the workability of fresh concrete, is the slump test. The slump value depends mainly on the water absorption and porosity of the aggregates, water content in the mixture, amount of the aggregate and fine material in the mixture, shape of the aggregates and surface characteristics of the constituents in the mixture. The slump values decrease significantly with the addition of polypropylene fibres. The concrete mixture becomes rather clingy resulting in increasing of the adhesion and cohesiveness of fresh concrete. During mixing the movement of aggregates shears the fibrillated fibres apart, so that they open into a network of linked fibre filaments and individual fibres. These fibres anchor mechanically to the cement paste because of their large specific surface area. The concrete mixture with polypropylene fibres results in the fewer rate of bleeding and segregation as compared to plain concrete. This is because the fibres hold the concrete together and thus slow down the settlement of aggregates [S.K. Singh (2010)]. Forgeron and Omer studied the effect of length of fibre on the flow characteristics of Micro-Synthetic Fibre Reinforced Self Consolidating Concrete (MSFRSCC) by using 20 non-air entrainment self-consolidating concrete (SCC) mixtures with varying w/c ratios, self-fibrillating Polypropylene macro-synthetic fibre lengths of 38 mm (1.5 in) and 50 mm (2 in) and fibre volume fractions from 0.2% to 0.5%. The flow characteristics of each mixture were evaluated using four typical SCC workability test methods: slump flow, filling capacity, L-box, and V-funnel flow time tests. The results showed that the fibre length plays a very important role in the flow characteristics. Comparing the flow characteristics, both the fibre lengths showed acceptable slump flows but the Slump flow of concrete with 50 mm (2 in) long fibres was found the least. Concrete having 0.5% of 50 mm long fibres was found to be worst in filling and flow property as it showed a 11 minimum of 65% filling capacity and a blockage in V-Funnel Test [D. Forgeron et al (2010)]. In 2011, Zhiguo You et al compared the workability of fibre reinforced self-consolidating concretes with two steel fibres of different aspect ratio and one synthetic fibre using standard Slump Flow and J-Ring Test. The test results showed that 40 kg/m³ (2.5 lb/ft³) steel fibres and 4 kg/m³ (0.25 lb/ft³) plastic fibres can be the upper bound of the fibre content regarding the workability of SCC [Zhiguo You et al (2011)]. 2.2.1.4. Volume Stability The serviceability of portland cement concrete (PCC) and of reinforced concrete structures is closely associated with their ability to resist and control cracking. There are many causes of cracking on brittle cement concrete mixes; volume change is one of them. Volume change causes cracking in concrete both in plastic (early age) concrete and Hardened Concrete. The use of fibre reinforcement in concrete reduces cracking and shrinkage and thus ensures volume stability of the cementitious composite to a great extent [Isabel Padron et al (1990)]. 2.2.2. Early Age and Plastic Shrinkage Plastic shrinkage cracking of concrete occurs when it is exposed to drying environment while it is still in plastic form. Normally it occurs within the first few hours after the concrete is placed and before it attains any significant strength. The adverse effects of drying shrinkage at a very initial phase include an unsightly and non-uniform appearance on the concrete surface. Later, the plastic shrinkage cracks become critical weak points for aggressive substances to penetrate into the internal portion of concrete leading to the acceleration of other detrimental forms of concrete deterioration. Consequently, the performance, serviceability, durability, and aesthetic qualities of concrete structures are reduced. Controlling plastic shrinkage cracking in concrete is essential for developing more durable and longer-lasting structures at a minimum life-cycle cost [Naaman et al (2005), Shah et al (2004)]. 12 One of primary causes of plastic shrinkage cracking is the loss of water from evaporation that leads to a built-up tensile shrinkage stress when concrete is subjected to sufficient restraint. When the rate of water loss due to evaporation exceeds the rate at which the bleed water is supplied to the surface, negative capillary pressures form that result in volume changes in the concrete. Tensile stresses in the paste form due to the negative capillary pressure and the development of strength in the concrete. Cracking occurs if the tensile stresses are greater than the tensile strength of the concrete [Naaman et al (2005), Shah et al (2004)]. The most effective method to prevent the plastic shrinkage of concrete that has become more and more popular in the last two decades is to add fibres to the matrix of the concrete. Such fibres are supposed to be randomly distributed and can be of different materials and geometries. Dependent on the volume, the added fibres improve the shrinkage cracking behaviour of the concrete by either simply bridging cracks after their occurrence (lower volumes) or increasing the actual tensile strength of the matrix and thereby delaying or preventing the cracking (higher volumes) [Naaman et al (2005), Shah et al (2004)]. 2.2.2.1. Experimental and Analytical Methods to Study Plastic Shrinkage Numerous strategies have been advocated to reduce the potential for plastic shrinkage cracking in concrete through mixture proportioning, curing methods, or the use of fibre reinforcement. The effectiveness of each approach must be adequately quantified to determine whether the additional initial cost of each strategy is justified. The majority of current research to characterize plastic shrinkage cracking in concrete relies on manual crack observation and measurement that is typically only performed at selected locations. These manual measurements of crack width may provide only limited information and may be subject to operator bias. This section describes some systematic methodologies to accurately quantify the salient features of the plastic shrinkage cracking. These methodologies are developed by utilizing different techniques such as Image Analysis, 13 Modified Weibull Function, and by using Demec gauges [Santhanam et al (2006), Christopher et al (2007), C. Qi et al (2003)]. Santhanam (2006) used a simple and reproducible technique to monitor plastic shrinkage cracking in rectangular concrete slabs. This methodology was found to be successful even for the characterization of very fine cracks in hybrid fibre concrete systems. This was based upon image analysis of photographs and manual crack measurements. In this study, the crack measurements were made after 24 hours in order to ensure that cracks got fully developed and stabilized. The cracked area was then photographed using a 4x optical zoom digital camera, and the image was processed using image analysis software. In order to calibrate the original size of the image that was captured, a measuring scale was placed on the concrete specimen and the entire area was photographed. The distance between two points on the scale was calibrated in terms of pixels and the total pixels were converted to the desired unit. The very thin hairline cracks were studied manually using a crack width microscope, which can measure accurately the crack widths in the range of 0.025 to 2.5 mm. (0.00098 to 0.098 in.). Shrinkage cracks were observed in less than about 4.5 hours after casting for the control concrete and 5.5 and 7 hours for the steel fibre and hybrid fibre concretes respectively. For the control concrete, the maximum crack width obtained was 0.5 mm (0.0196 in.); this was reduced to 0.371 mm. (0.0146 in) i.e. by 25% in the case of steel fibre concrete (SFRC), and to 0.225 mm. ( 0.0088 in.) i.e. by 55% in case of hybrid fibre concrete. This corresponds to a reduced crack area of 57.6 % compared to control concrete and 43% compared to steel fibre concrete [Santhanam et al (2006)]. Christopher et al (2007) investigated a new test procedure to study the shrinkage cracking behavior for plain shotcrete and four different types of FRS (polypropylene, steel, polyvinyl alcohol, and hybrid). To introduce shrinkage restraint, specimens cut from a shotcrete panel are bonded to a steel fixture. This method utilizes the measurement of shrinkage strain of the restrained specimen at different times, the occurrence of cracking can be easily observed from a sudden “jump” in the strain values. To identify cracks, two 14 different approaches were employed. In the first approach, visual inspection was conducted and then the cracks were measured using Demec guage. To assist crack detection, acetone was applied onto the specimen surface with a small piece of cotton. This way, fine crack could be more easily revealed [Christopher et al (2007)]. Qi et al (2003) used image analysis and modified Weibull technique to measure plastic shrinkage of restrained slab specimen. This provides a systematic approach for quantifying the effect of fibre reinforcement on plastic shrinkage cracking. This method describes how an image analysis technique is implemented to rapidly extract pertinent crack width information along a predetermined grid system. Statistical interpretation of the collected crack widths is performed using either a standard or modified Weibull distribution function. The process of image analysis included image acquisition, image processing, crack feature determination, crack feature measurement and Crack width data analysis. Thus by using a semi-automated image analysis technique and statistical approach, the plastic shrinkage cracking of fibre reinforced concrete has been characterized [C. Qi et al (2003)]. 2.2.2.2. Effects of Different Fibres on Plastic Shrinkage As stated previously, there is a wide verity of fibres that are being used to control plastic shrinkage cracking of concrete. There have been significant efforts to evaluate and compare the performance of different types of fibres and their parameters tested under similar conditions. In 1990, Isabel and Zollo investigated restrained drying shrinkage of Fibre Reinforced Concrete by experimental program. Synthetic fibrous concrete (SNFRC) with polypropylene and acrylic fibres and nonfibrous (control) samples were tested. The tests were designed to demonstrate the ability of the fibres, (in this case, applied at low volume percentage) to control cracking and reduce shrinkage [Isabel Padron et al (1990)]. 15 After conducting the experimental program they concluded that the use of relatively fine (between 5 and 100 denier) polypropylene fibres 19 mm. (3/4 in.) long, and of acrylic material 10 mm. (3/8 in.) long can a) Reduce shrinkage for each of the two concrete matrixes tested, and b) Reduce the total crack area for each of the two concrete matrixes tested. The amount or percentage reduction in both shrinkage and crack surface area varies directly with the percent of fibre volume added for the mortar specimens using acrylic fibres [Isabel Padron et al (1990)]. Shah et al (2004) compared the performance of different fibre types, fibre blends, and welded-wire fabric (WWF) in their ability to prevent and control drying-shrinkage cracking. He used flat end steel, hooked end steel, crimped and profiled steel, crimped, monofilament and multifilament polypropylene fibres at volume fraction of 0.125 to 1% and steel welded-wire fabric. Among these fibres flat end 30 mm. (1.18 in.) fibre was found most efficient at all fibre percentage. The advantage of this fibre type is especially obvious for the lower fibre volumes of 0.125 and 0.25%. In the case of the fibre volume of 0.25%, no difference in cracking age can be found among the remaining fibre types. Certain reinforcement types stand out due to the fact that they do not significantly improve or increase the cracking age compared to the plain concrete mixture. These are the fibres: Profiled 20 mm (0.8 in) (in Vf = 0.125%), Crimped, PP 50 mm (2 in.) (in Vf = 0.3% and Vf = 0.6%), and the WWF. He noted that the age at which first crack are formed increases with increasing fibre volume in all cases [Shah et al (2004)]. Naaman (2005), studied the effect of four synthetic fibres and one metallic fibres (polypropylene, polyvinyl alcohol (PVA), high-density polyethylene (HDPE), carbon, and, flexible metallic fibres (FMF),) at volume fractions varied from 0.05 to 0.4% and noticed reduction in total crack area and total crack length accompanied by a significant decrease in maximum crack widths compared with plain concrete when 0.1% volume fraction of fibres was used. Increasing the fibre volume fraction from 0.1 to 0.4% 16 slightly improves the plastic shrinkage cracking resistance of fibre-reinforced cementitious composites. The direction of the cracks was generally normal to the longitudinal axis of the specimens and cracks were randomly distributed along the whole length of specimen. He also noticed that fibrillated polypropylene fibres were less effective in controlling plastic shrinkage cracking compared with monofilament polypropylene fibres when used at 0.1%, however, when the volume fraction of fibre is increased to 0.4%. The total plastic shrinkage cracking decreases from 45.432 to 5.9175 mm² (0.0704 to 0.0091 in².) when the volume fraction of fibrillated polypropylene fibre increases from 0.1 to 0.4% [Naaman et al (2005)]. Saleh H. (2006) conducted an extensive experimental program to investigate the influence of adding POF on the plastic cracks, drying shrinkage, under laboratory and actual hot-dry condition that normally prevails in the Kingdom of Saudia Arabia. After being exposed to the field condition for one hour, no cracks appeared in any of the POF prisms. This is clear evidence that POF had a great effect in arresting the plastic shrinkage cracks. It was seen that under both curing conditions, addition of POF to the concrete mix resulted in increasing the rate of shrinkage at the beginning of the measuring period and also increased the ultimate shrinkage strain. The increase in the ultimate strain under laboratory conditions was 17% whereas under field condition was 53% [Saleh H. Alsayed (2006)]. Chen (2008) studied the effectiveness of using small amounts of chopped baler twine to control the restrained plastic shrinkage cracking of portland cement mortar. To determine the influence of baler twine fibre type, length and volume fraction on their performance, two types of baler twine ( one composed of strands with circular cross section, the other composed of flat band shape strands) in two lengths; 19 mm and 38 mm. (0.748 and 1.5 in.) and three volume fractions; 0.05%, 0.1%, and 0.3% were evaluated. Test results indicate that both types of baler twine are capable of controlling restrained plastic shrinkage cracking to some extent, but are not as effective as fibrillated polypropylene. Compared with plain specimens, the total crack area was reduced by 95.3, 77.5 and 38.7% when 0.3% volume fraction of 38 mm fibrillated polypropylene, 17 band shape baler twine and circular baler twine fibres, respectively, were added. Free plastic shrinkage was significantly reduced only when long fibre lengths (38 mm) and high volume fractions (0.3%) were used [Ying Chen (2008)]. Various studies have been conducted to investigate the effect of fibre dosage on the shrinkage and drying cracking of PPFRC. All of these showed a significant reduction in cracking for smaller volume fraction of fibres. Alhozaimy et al (1995) conducted drying shrinkage test on PPPFRC specimen with 0.05%, 0.1%, and 0.2% volume content on two different lengths of fibres. He concluded that Polypropylene fibres reduce the total plastic shrinkage crack area and maximum crack width at 0.1 percent fibre volume fraction of 19 mm. (0.75 in.) fibre. On the average, 19 mm. (0.75 in) fibres had 13, 57, and 55 percent less crack areas than 13 mm. (0.5 in.) fibres at 0.05, 0.1, and 0.2 percent fibre volume fractions, respectively. The maximum crack widths with 19 mm. (0.75 in.) fibres were, on the average, 47, 33, and 36 percent less than those for 13 mm. (0.5 in.) fibres at 0.05, 0.1 and 0.2 percent fibre volume fractions, respectively [Alhozaimy et al (1995)]. Saeed Ahmed et al (2006) studied the Polypropylene fibres as a way to reduce plastic shrinkage cracking. The results showed that by using about 0.35% fibres by volume reduced plastic shrinkage cracking to such an extent that no cracks could be observed and lower volumes i.e. 0.15 to 0.20% visibly restrained the crack width compared to samples that were not fibre reinforced. The shrinkage cracking is reduced by 83 to 85% by addition of fibres upto 0.35% and 0.50 % [Saeed Ahmed et al (2006)]. Collins et al (2008) studied effects of the volume fraction of polypropylene fibres on the drying shrinkage of hardened concrete made with OPC and slag-blended cement binders. Different volume fractions of PP fibres ranging from 0.05 to 0.5% have been tested. The study showed that PP fibre specimens exhibited higher total shrinkage strains compared with the reference mixture PC with no fibre until the age of 56-days. The drying shrinkage of concrete mixture with 0.5% fibre vol. fraction, cured for 1-day and 7days 18 was higher than that of the reference mixture PC by 15% and 22% at an age of 56-days [F. Collins et al (2008)]. Naaman (2005), Alhozaimy (1995), and Wu (2001) studied the effects of different other fibres on the plastic shrinkage of PPFRC. • Effect of Fibre Length Alhozaimy concluded that longer fibres [19 mm (0.75 in.)] generally performed better than shorter ones [13 mm (0.50 in.)]; however, at certain volume fractions, the effect of fibre length was not statistically significant [Alhozaimy et al (1995)]. Naaman also investigated three different lengths of polypropylene fibres; 12.7, 19.05, and 25.4 mm (0.5, 0.75, 1 in. ) in his study and found that only a slight improvement in performance is achieved in specimens with longer fibres, that is, a higher aspect ratio [Naaman et al (2005)]. • Effect of Fibre Form Naaman found that at 0.1% fibre volume fraction, fibrillated polypropylene fibres were less effective in controlling plastic shrinkage cracking compared with monofilament polypropylene fibres. This disadvantage almost vanishes, however, when the volume fraction of fibre is increased to 0.4%. The total plastic shrinkage cracking decreases from 45.432 to 5.9175 mm² (.0704 to .0091 in²) when the volume fraction of fibrillated polypropylene fibre increases from 0.1 to 0.4% [Naaman et al (2005)]. • Effects of fibre diameter Better efficiency in reducing plastic shrinkage cracking is achieved with finer fibres. At 0.1% volume fraction, the total crack area of specimens with fibres of diameter 0.1 mm (0.0039 in.) was 32.183 mm² (0.0498 in²), while the specimen with fibres of diameter 0.04 mm (0.00157 in.) was 1.936 mm² (0.00299 in²), almost 16 times smaller. This observation was also confirmed when other small-diameter fibres were used, such as 19 carbon fibres. It is concluded that plastic shrinkage cracking depends greatly upon fibre diameter [Naaman et al (2005)]. • Effect of Elastic Modulus of fibres Naaman studied the effect of Modulus of Elasticity of fibres on plastic shrinkage and found no significant influence on the shrinkage of concrete [Naaman et al (2005)]. • Effect of Aspect Ratio of fibres The proportion between length and diameter or equivalent diameter is an important fibre parameter defined as the fibre aspect ratio. In case of Polypropylene fibres, the fibre aspect ratio does not influence plastic shrinkage cracking however for Polyvinyl Alcohol Fibres; fibre aspect ratio seems to be a significant factor for controlling plastic shrinkage cracking. The total crack area decreases drastically from 32.183 to 1.913 mm² when the fibre aspect ratio increases from 120 to 300 [Naaman et al (2005)]. • Effect of Geometry of Fibres Wu (2002) investigated the effect of geometry of fibres on the shrinkage cracking of cement mortars using three different forms of polypropylene fibres namely, fibre made in the drawing-wire technique, fibres made in fibrillated film technique and Y-shaped fibres. By using 0.05%, 0.1% and 0.15% of fibre contents it was found that the geometry (cross-section) shape of Y-PP fibre has a better effect on the drying shrinkage cracking than that of DW-PP fibre. In the present study, the order of reduction in drying shrinkage cracking is Fibrillated fibre < Y-shaped fibre < Drawing-wire fibre. Especially when 0.10% or more DW-PP fibres are added into cement mortar, drying shrinkage cracking can be avoided [Wu et al (2002)]. Shah (2004) compared the performance of four different forms of steel fibres, three different forms of polypropylene fibres and welded-wire fabric in their ability to prevent and control drying-shrinkage cracking and found that the fibre Flat End [30 mm (1.181 20 in)] is the best-performing reinforcement, concerning age of first crack and maximum crack width. This is valid for all investigated fibre volumes [Shah et al (2004)]. 2.3. HAREDENED PPFRC Concrete gains strength as it gets hardened. The process of gaining strength is accompanied by evolution of heat of hydration upon curing. The strength of concrete is a function of time. It gains strength as it gets old up to a certain specified age. The strength of the fibre reinforced concrete can be measured in terms of its maximum resistance when subjected to compressive, tensile, flexural and shear stresses either individually or combined. With the increasing use of fibre reinforced concrete as a structural material, more information on its mechanical properties was needed. Researchers have done significant work for establishing the impact of different fibres on the mechanical properties of fibre reinforced cementitious composites. Conclusions of some reports and researches on compressive strength, splitting tensile strength and flexural strength are presented under: 2.3.1. Compressive Strength of PPFRC The effect of polypropylene fibre on the compressive strength of concrete has been discussed in many studies and resulted that polypropylene fibres either decrease or increase the compressive strength of concrete, but overall effect is negligible in many cases. Many researchers have reported no or a very small influence of small volume fraction (from 0.05% to 0.5%) of polypropylene fibres on compressive strength of Fibre Reinforced Concrete, [Naaman et al (1985), Alhozaimy et al (1996), Vikrant et al (2012), Saeed Ahmed et al (2006)] while some of the researches have shown a significant increase in the compressive strength on fibre reinforced concrete. Ziad et al concluded that Polypropylene fibres had a relatively small favorable effect on compressive strength of concrete when 12 mm (1/2 in.) long fibres were used[Ziad Bayasi et al (1993)]. Song et al noted an enhancement of approximately 6% when used polypropylene fibres at a fibre content of 0.6 kg/m³ (0.037 lb/ft³)[Song et al (2005)]. Mtasher et al found increase 21 in the compressive strength of concrete because of presence of fibres in the concrete mix. The investigation resulted that the Polypropylene fibre inclusions in amount of 0.4% and 1.5% increased the compressive strength up to 11% and 56% respectively [Rana A. Mtasher et al (2011)]. Ahmed et al noted that polypropylene fibres when used in higher dosage (0.55% and 0.6%) decreased the 28 days compressive strength of concrete by 35% of that of plain concrete [Saeed Ahmed et al (2006)]. 2.3.2. Tensile Strength of PPFRC Brittle matrices, such as plain mortar and concrete, lose their tensile load-carrying capacity almost immediately after formation of the first matrix crack (Figure 2.5). The addition of fibres in conventional fibre reinforced concrete (FRC) can increase the toughness of cementitious matrices significantly; however, their tensile strength and especially strain capacity beyond first cracking are not enhanced [Gregor Fischer (2004)]. The tensile strength of concrete is only about 10 % of its compressive strength. It is clear that addition of fibres to a concrete mixture is beneficial to the tensile properties of concrete. The fibres act as crack arresters in the concrete matrix prohibiting the propagation of cracks in plastic state and propagation of cracks in hardened state. Once the splitting occurred and continued, the fibres bridging across the split portions of the matrix acted through the stress transfer from the matrix to the fibres and, thus, gradually supported the entire load. The stress transfer improved the tensile strain capacity of the fibre-reinforced concrete and, therefore, increased the splitting tensile strength of the reinforced concretes over the unreinforced control counterpart. Vikrant et al studied the effect of length of fibre on the split tensile strength of fibre reinforced concrete and observed that, the split tensile strength of fibre reinforced concrete was dependent on length of fibre used. By addition of longer length fibre, the split tensile strength increases. Use of 24 mm (0.94 in) long fibre with same volume of fraction gives maximum split tensile strength over fibre 15 mm (0.59 in) and 20 mm (0.787 in) cut length. The overall effect of 24 mm long fibre when used in fibre content 22 of 0.25% of weight of cement was that, it improved the split tensile strength of concrete by 72% [Vikrant et al (2012)]. Ahmed et al studied that the tensile strength of concrete increases linearly with addition of fibres up to about 0.40% after which the tensile strength decreases with addition of more fibres. The tensile strength increases about 65%~70% up to 0.40% after which it decreases. Tensile strength is increased due to bridging mechanism of polypropylene fibres and after certain time it reduced the bond strength between concrete ingredients so results in quick failure as compared to less volumes of fibres. Song et al noted an increase of 10% in the split tensile strength of fibre reinforced concrete at the fibre dosage of 0.6kg/m³(0.037 lb/ft³ ).[ Saeed Ahmed et al (2006), Song et al (2005)]. One the other hand, Xing et al (2004) investigated the mechanical properties of polypropylene fibre reinforced concrete and found that a low content of polypropylene fibre [0.91 Kg/m³ (0.056 lb/ft³)] slightly decreased the tensile strength of FRC than that of plain concrete [Xing et al (2004)]. 2.3.3. Flexure Strength of PPFRC Flexure strength is one of the measures of tensile strength of concrete. It is the ability of a beam or slab to resist failure in bending. It is measured by loading un-reinforced concrete beams with a span three times the depth. The flexural strength is expressed as “Modulus of Rupture” (MR) in psi. Flexural MR is about 12 to 20 percent of compressive strength. However, the best correlation for specific materials is obtained by laboratory tests. Ziad et al studied the effect of length and volume fraction of polypropylene fibre on the flexural behavior of PPFRC by characterising the post-peak flexural resistance under four point loading. It was found that, for volumes equal to or less than 0.3 percent, 19 mm (3/4 in.) long fibres were more favorable for enhancing the post-peak resistance. For 0.5 percent volume, 12 mm (1/2 in.) long fibres were more effective [Ziad Bayasi et al, (1993)]. 23 Alhozaimy et al investigated the effect of different volume fractions of polypropylene fibre and different types of binders on the flexure strength and toughness of the composite using the test procedure designed by ASTM C78 for the Two-Point Loading and found that at lower volumetric fractions, the fibre has no effect on the flexural strength of FRC; however the binder compositions has significant effect on the flexural toughness of FRC. Polypropylene fibres affect the flexural toughness significantly. On the average, the addition of 0.1%, 0.2%, and 0.3% volume fraction of fibres increases the flexural toughness by 44%, 271% and 387%, respectively [Alhozaimy et al (1996)]. Ahmed et al found that the behavior of concrete in flexure seems to be identical with polypropylene fibre reinforced concrete as that in tensile strength. There is about 80% increase in flexure strength by adding 0.20% fibres in concrete after which strength starts reducing with further increment in fibre ratios [Saeed Ahmed et al (2006)]. Mtasher et al investigated the effects of different volume fraction of polypropylene fibre on the mechanical properties of FRC and found that when polypropylene fibres was used in amount of 0.4% and 1.5% (on cement content), the increase of flexural strength 24.6% and 85% respectively [Rana A. Mtasher et al, (2011)]. 24 Table 2.1 A compilation of mechanical properties of commonly used fibres in concrete materials [ACI 544.5R (2010)] Equivalent Type of Fibre Diameter (mm)* 0.02 to 0.35 Acrylic 0.0015 to Asbestos 0.02 Cotton 0.2 to 0.6 Specific Gravity (Kg/m³)** 1100 Tensile Strength (MPa)*** 200 to 400 3200 1500 600 to 1000 400 to 700 1000 to Glass 0.005 to 0.15 2500 2600 0.008 to 1000 to Graphite 0.009 1900 2600 3500 to Aramid 0.01 1450 3600 Nylon 0.02 to 0.40 1100 760 to 820 Polyester 0.02 to 0.40 1400 720 to 860 Polypropylene 0.02 to 1.00 900 to 950 200 to 760 Polyvinyl alcohol 0.027 to 0.66 1300 900 to 1600 Carbon 1400 4000 Rayon 0.02 to 0.38 1500 400 to 600 Basalt 0.0106 2593 990 Polyethylene 0.025 to 1.0 960 200 to 300 Sisal 0.08 to 0.3 760 to 1100 228 to 800 Coconut 0.11 to 0.53 680 to 1020 108 to 250 Jute 0.1 to 0.2 1030 250 to 350 Steel 0.15 to 1.00 7840 345 to 3000 Young's Modulus (GPa) 2 Ultimate Elongation (%) 1.1 83 to 138 4.8 1.0 to 2.0 3.0 to 10.0 70 to 80 1.5 to 3.5 230 to 415 0.5 to 1.0 65 to 133 4.1 8.3 3.5 to 15 2.1 to 4.0 16 to 20 11 to 13 5.0 to 25.0 23 to 40 230 to 240 6.9 7.6 5 11 to 27 2.5 to 4.5 26 to 32 200 7 to 8 1.4 to 1.8 10 to 25 2.56 3 2.1 to 4.2 14 to 41 1.5 to 1.9 4 to 10 * 1 mm = 0.0393 in, ** 1 Kg/m³ = 0.0624 lb./ft³, ***1 MPa = 145 psi 25 Table 2.2 Properties of different types of polypropylene fibres [S.K. Singh (2010)] Fibre Type Length (mm)* Daimeter (mm)* Tensile Strength (Mpa)** Modulus of Density Elasticity (kg/m³)*** (Gpa) Monofilament Microfilament Fibrillated 30-50 12-20 19-40 0.30-0.35 0.05-0.20 0.20-0.30 547-658 330-414 500-750 3.50-7.50 3.70-5.50 5.00-10.00 * 1 mm = 0.0393 in, **1 MPa = 145 psi, *** 1 kg/m³ = 0.0624 lb./ft³ 26 0.9 0.91 0.95 Length, Diameter or Perimeter Geometrical Section Shape Fibre Characteristics Figure 2.1 Circular, elliptical, square, rectangle, triangle flat.... Smooth, deformed, indented, etched, crimped, coilled, twisted, with end paddles, end hooks, end buttons, 2D, 3D,... Mechanical Strength, elastic modulud, transverse modulud,stiffness, ductility, elongation to failure Physical/ Chemical Density, surface roughness, chemical stability, fire resistance, non-reactivity with cement... Material - Natural organic: wood, sisal, jute, bamboo... - Natural mineral: asbestos, rock, wool... - Man-made: steel, polymers (synthetic), glass, carbon, metallic,... Main characteristics of fibres [Naaman et al (2006)] Composite Fibre Matrix Cement Paste: -Cement -Water -Addditive and Admixtures Aggregates: Coarse and fine Others: Recycled wastes, unwanted materials, organics, woods Figure 2.2 Composite model of FRC with two main components, namely fibre and matrix [Naaman et al (2006)] 27 Figure 2.3 Simplified general classification of FRC composites based on their tensile stress-strain response [Naaman et al (2007)] Figure 2.4 Typical stress-strain or elongation curve in tension up to complete separation: (a) Conventional strain-softening FRC composites; (b) Strainhardening FRC composites [Naaman et al (2007)] 28 Figure 2.5 Schematic stress-strain behaviour of cementitious matrix in tension [Gregor Fischer (2004)] 29 CHAPTER 3 EXPERIMENTAL PROGRAM 3.1 GENERAL This chapter provides a detailed description of the materials used in the experimental program and experimental methods used in this study. The experimental program consisted of laboratory tests on plain concrete and polypropylene fibre reinforced concrete (PPFRC) to characterize the properties such as flow ability in fresh state, early age plastic shrinkage and mechanical properties in hardened state. For this purpose total of seven (7) concrete mixtures were cast with one control mix (plain concrete) and six PPFRC mixes. The PPFRC mixes were for two different length of fibre Lf (25 mm and 38 mm) and the different volume fraction of fibre Vf were 0.3%, 0.6% and 0.8%. The materials, mix design (mixture proportions), casting, curing, test methods and procedures for workability of PPFRC, tests for plastic shrinkage of PPFRC and tests for selected mechanical properties of hardened concrete are described in detailed in the respective sections. 3.2 MATERIALS 3.2.1. Cement Ordinary Portland (ASTM Type-I) cement is used for this study. 3.2.2. Aggregates The coarse aggregate used in this experimental program is found at Hub Chowk near Karachi and the fine aggregate is found at the Super Highway, Karachi. The coarse aggregate passing through sieve #2 and retained over sieve #3 is used. Whereas fine sand passing through sieve #16 and retained on sieve #20 was used as fine aggregate. 30 3.2.3. Water Ordinary tap water which is being supplied by Karachi Water and Sewerage Board was used for mixing of concrete ingredients and also for other experimental work including washing of equipment, curing of specimen etc. 3.2.4. Fibre Fibrillated polypropylene fibres (PPF) with two different lengths were used in different volume percentage. The fibre and the material specifications were provided by the Matrixx Company. The fibrillated polypropylene fibres are composed of film sheets which are cross linked by fine fibre along their length as shown in Figure 3.1. These fibres are manufactured in chicken mesh form and then cut into desired length. The two different lengths of PPF used in this study were 25 mm and 38 mm (see Figure 3.2). The physical and mechanical properties of PPF are shown in Table 3.1. 3.2.5. Admixture Super plasticizer was used to increase the workability of freshly prepared fibre reinforced concrete. 3.3 MIX DESIGN A suitable concrete mix design was established on the basis of preliminary testing of mortar cubes having cement to sand ratio of 1:2.75 and w/c ratio of 0.48. Twelve number of 2”x2” cubes were cast and cured in water tank and then tested under compression using Universal Testing Machine at a loading rate of 60 psi/min. The strength- time curve was developed for 28 days of curing. (See Figure 3.3) Each point on strength-time curve is an average of three replicate cube specimens. Note that the 28 day strength is in excess of 3000 psi. 31 The mixing for concrete was done in rotary drum mixer at a mixing rate of 40 rpm. Pictorial view of the mixer is shown in Figure 3.4. The drum was previously moistened by spraying just enough water to moist the inner surface of the drum. The mixing sequence used for all mixtures was as follows: • Add the fine aggregate (sand) to the mixer and mix for 30 seconds • Add the coarse aggregate to the mixer and mix for 30 seconds • Add the fibres and mix for 3 minutes (not done the plain concrete) • Add 50% of the adjusted water and mix for 30 seconds • Add all the cement to the mixer and mix for 30 seconds • Add admixture into the balance of the water, introduce into the mixer and mix for 4 minutes • Let the mixed PPFRC be idle for 2 minutes and then mix for 4 additional minutes After mixing, the concrete was placed into lubricated moulds and vibrated externally. A smooth steel trowel was used to finish the fresh concrete. The mix proportions of concrete mixtures are shown in Table 3.2. 3.4 TESTS FOR WORKABILITY OF FRESH PPFRC Six standard test methods were used to study the workability of PPFRC in terms of flow ability. These being Standard Slump test, Inverted Slump Test (Compacting Factor Test), Flow Table Test, J-Ring Test, L-Box Test and V-Funnel Test. All these tests were performed on the same batch of concrete for the purpose of homogeneity and the results obtained thus were compared and calibrated. The complete experimental matrix for workability tests is given in Table 3.3. Freshly prepared PPFRC is shown in Figure 3.5. 3.4.1. Standard Slump Test (ASTM C143) The slump test is the most well-known and widely used test method to characterize the workability of fresh concrete. The inexpensive test, which measures consistency, is used on job sites to determine rapidly whether a concrete batch should be accepted or rejected. 32 The test method is widely standardized throughout the world, including in ASTM C143 in the United States and EN 12350-2 in Europe. [Eric et al (2003), ASTM C143 (2000)] The apparatus consists of a mould in the shape of a frustum of a cone with a base diameter of 203 mm (8 inches), a top diameter of 101 mm (4 inches), and a height of 305 mm (12 inches). The assembly is shown in Figure 3.6. During this test, the mould is filled with concrete in three layers of equal volume. Each layer is compacted with 25 strokes of a tamping rod. The slump cone mould is lifted vertically upward and the change in height of the concrete is measured. Three types of slumps are commonly encountered, as shown in Figure 3.7. The only type of slump permissible under ASTM C143 is frequently referred to as the “true” slump, where the concrete remains intact and retains a symmetric shape. A zero slump and a collapsed slump are both outside the range of workability that can be measured with the slump test. Specifically, ASTM C143 advises caution in interpreting test results less than 12 mm (½ inch) and greater than 228 mm (9 inches). If part of the concrete shears from the mass, the test must be repeated with a different sample of concrete. A concrete that exhibits a shear slump in a second test is not sufficiently cohesive and should be rejected [Eric et al (2003)]. 3.4.2. Compacting Factor Test (BS 1811-103) The compaction factor test measures the degree of compaction resulting from the application of a standard amount of work. The test was developed in Britain in the late 1940s and has been standardized as British Standard 1881-103 [Eric et al (2003), BS 1881-103 (1993)]. The apparatus, which is commercially available, consist of a rigid frame that supports two conical hoppers vertically aligned above each other and mounted above a cylinder, as shown in Figure 3.8. The top hopper is slightly larger than the bottom hopper, while the cylinder is smaller in volume than both hoppers. To perform the test, the top hopper is filled with concrete but not compacted. The door on the bottom of the top hopper is 33 opened and the concrete is allowed to drop into the lower hopper. Once all of the concrete has fallen from the top hopper, the door on the lower hopper is opened to allow the concrete to fall to the bottom cylinder. A tamping rod can be used to force especially cohesive concretes through the hoppers. The excess concrete is carefully struck off the top of the cylinder and the mass of the concrete in the cylinder is recorded. This mass is compared to the mass of fully compacted concrete in the same cylinder achieved with hand rodding or vibration. The compaction factor is defined as the ratio of the mass of the concrete compacted in the compaction factor apparatus to the mass of the fully compacted concrete. The standard test apparatus, described above, is appropriate for maximum aggregate sizes of up to 20 mm. A larger apparatus is available for concretes with maximum aggregate sizes of up to 40 mm [Eric et al (2003)]. 3.4.3. Flow Table (ASTM C1437) This test provides information on filling ability (flowability) and passing ability (for a stable mix, high flowability tracks with passing ability) [ASTM C1437 (1999), Technical Bulletin 1506]. The apparatus consists of standard Abram’s cone [ASTM C143 (2000)] and Slump flow board which is a non-absorbent rigid plate (coated plywood, plastic, metal or similar material) measuring at least 1 meter square (39 in. per side) as shown in Figure 3.9. In general, the slump flow test is very similar to the standard slump test but it is used to measure the horizontal spread of concrete cone specimen. The Abram’s cone is placed in the centre of the slump flow board, either in the normal orientation (large opening down) or inverted (small opening down). It is filled in one lift (no rodding or other consolidation) and then the cone is then raised in 3 ±1 seconds to a height of 230 ±75 mm (9 ±3 in.), allowing the fluid concrete to flow onto the slump flow board. The slump flow is the diameter of the resulting concrete “patty” obtained from the average of measuring the greatest diameter and diameter perpendicular to this direction. Large differences between the two diameters indicate a non-level surface, which must be corrected [ASTM C1437 (1999), Technical Bulletin 1506]. 34 3.4.4. J-Ring Test (ASTM1621) The J-ring test extends common filling ability test methods to also characterize passing ability. The J-ring test device can be used with the slump flow test. The J-ring, as shown in Figure 3.10, is a rectangular section (30 mm by 25 mm) open steel ring with a 300 mm diameter. Vertical holes drilled in the ring allow standard reinforcing bars to be attached to the ring. Each reinforcing bar is 100 mm long. The spacing of the bars is adjustable, although 3 times the maximum aggregate size is typically recommended. For fibrereinforced concrete, the bars should be placed 1 to 3 times the maximum fibre length [Eric et al (2003)]. To conduct the J-ring test in conjunction with the slump flow test, the slump cone is placed in the centre of the J-ring and filled with concrete. The slump cone is lifted and concrete is allowed to spread horizontally through the gaps between the bars [Eric et al (2003), ASTM 162 (2011)]. Various interpretations of the test results have been suggested. The measures of passing ability and filling ability are not independent. To characterize filling ability and passing ability, the horizontal spread of the concrete sample is measured after the concrete passes through the gaps in the bars of the J-ring and comes to rest. Also, the difference in height of the concrete just inside the bars and just outside the bars is measured at four locations. The smaller this difference in heights is, the greater the passing ability of the concrete will be. Alternatively, the horizontal spread with and without the J-ring can be compared as a measure of passing ability [Eric et al (2003), ASTM 162 (2011)]. 3.4.5. L-Box Test The L-box test measures the filling and passing ability of self-compacting concrete. Originally developed in Japan for underwater concrete, the test is also applicable for highly flowable concrete [Eric et al (2003)]. 35 As the test name implies, the apparatus consists of an L-shaped box, shown in Figure 3.11. Concrete is initially placed in the vertical portion of the box, which measures 600 mm in height and 100 mm by 200 mm in section. A door between the vertical or horizontal portions of the box is opened and the concrete is allowed to flow through a line of vertical reinforcing bars and into the 700 mm long, 200 mm wide, and 150 mm tall horizontal portion of the box. In the most common arrangement of reinforcing bars, three 12 mm bars are spaced with a clear spacing of 35 mm. Generally, the spacing of the reinforcing bars should be three times the maximum aggregate size. It should be noted that various dimensions for the L-box have been used and no one set of dimensions is considered official; however, the dimensions described above seem to be the most common [Eric et al (2003)]. After the concrete comes to rest in the apparatus, the heights of the concrete at the end of the horizontal portion, H2, and in the vertical section, H1, are measured. The blocking ratio, H2/H1, for most tests should be 0.80 to 0.85. If the concrete being tested is truly self-levelling, like water, then the value of the blocking ratio will be unity. Segregation resistance can be evaluated visually. A concrete sample with coarse aggregate particles that reach the far end of the horizontal part of the box exhibits good resistance to segregation. The L-box can be disassembled after the concrete has hardened [Eric et al (2003)]. While the test does give valuable information about filling and passing ability, and to a lesser extent, segregation resistance, the test is not as simple as the slump flow test. Since there are no standardized dimensions, results from different test apparatuses cannot be compared directly [Eric et al (2003)]. 3.4.6. V-Funnel Test The V-funnel test is used to measure the filling ability of concrete and can also be used to judge segregation resistance. The test method is similar to the concept of the flow cone test used for cement paste. 36 The test apparatus, shown in Figure 3.12 consists of a V-shaped funnel with a height of 425 mm (16.75 inches) a top width of 490 mm (19.29 inches), a bottom width of 65 mm (2.55 inches), and a thickness of 75 mm (3 inches). At the bottom of the V-shape, a rectangular section extends downward 150 mm ( inches). The entire funnel is filled with concrete without tamping or vibration. The door at the bottom of the funnel is opened and concrete is allowed to flow out of the funnel and into a bucket. The flow time for all of the concrete to exit the funnel is recoded as a measure of filling ability. Further, nonuniform flow of concrete from the funnel suggests a lack of segregation resistance [Eric et al (2003)]. 3.5 TESTS FOR PLASTIC SHRINKAGE OF FRESH PPFRC A standard test method for measuring the length change of hardened mortar or concrete specimens was introduced in ASTM C157. However, it is still a challenge to measure the early-age shrinkage of concrete, while it is still in a plastic state, and no standardized method exists to evaluate free (unrestrained) plastic shrinkage [ASTM C157 (1999), ASTM C596 (2000)]. This test gives a measure of the amount of drying shrinkage of hardened mortar and concrete in terms of change in length. The standard specimen size is 4”x4”x11 ¼”. Before casting, the polyethylene sheets were placed on the inside of the moulds to prevent any loss of water from the mix (see Figure 3.13). After casting, two identification marks were drawn on the top surface of the specimen at some suitable distance in order to measure length changes at the required time intervals. This was done by embedding two metallic nails or pins on the longitudinal axis of each specimen’s top surface, separated longitudinally by a distance of approximate 8 inches (200 mm).[ Chen (2008)]. Figure 3.14 shows the standard shrinkage prism with thumb tacks over it. A digital calliper with a precision of 0.01 mm (0.000393 in) was used to measure the distance between the indentations on the thumb tacks initially and after the required time intervals (See Figure 3.15). [ASTM C157 (1999)] A schematic diagram of shrinkage specimen is shown in Figure 3.16. 37 The initial reading is taken after 24 hours of mixing water with cement and then the specimen were exposed to natural environment at room temperature. The calliper readings are taken after 48, 72 and 96 hours. The length change of any specimen at any age after the initial calliper reading is computed using the Eq. 3.1 and noted as a percent increase or decrease in linear dimension to the nearest 0.001 % of the gage length based on the initial measurement made at the time of removal from moulds. [ASTM C157 (1999)] ∆L = (L – previous L)/G x100 {Eq. 3.1} Where, ∆L = length change of specimen at any age, % L = comparator reading of the specimen at known time interval, and G = the gage length (initial L) The moisture loss measurements were also done by measuring the weight of 4'' x 4'' x 11 ¼'' specimens at the same time interval. The complete experimental matrix is given in Table 3.4. 3.6 TESTS FOR MECHANICAL PROPERTIES OF HARDENED PPFRC Some of the mechanical properties of PPFRC are considered in this study. These include Compressive strength, splitting tensile strength and flexure strength. Standard methods of test for each of the property are described in the following sections. The complete experimental matrix is given in Table 3.5. 38 3.6.1. Compressive Stress-Strain Curve (ASTM C39) This test method covers the determination of cylindrical compressive strength of concrete specimen. The specimens are prepared by pouring freshly mixed concrete into lubricated cylinders. The mixing procedure is the same as described in Section 3.3 of this report. Consolidation is done externally over vibrating table for 3-5 minutes. After vibration and finishing, the moulds are kept at normal atmospheric conditions for 23 ½ ± ½ hours after which de moulding is done. The specimens are then cured in water tank [ASTM C39 (2001)]. The test is conducted at surface dry condition. The specimens are capped, placed and seated in the testing machine as described by section 7 of ASTM C39. The specimens are tested at the age of 7, 14 and 28 days of curing under the Universal Testing Machine shown in Figure 3.17. This machine applies compressive stress on the cylinder due to the downward movement of the platen at a constant displacement rate of 0.1 mm/sec. Figure 3.18 shows schematic diagram of the compressive strength test. The load and stroke measurements are noted from which stress and longitudinal strain values are computed and plotted for each set of tests [ASTM C39 (2001)]. The strength-time curves for plain concrete and PPFRC were also obtained for an average of three values and then compared to each other. 3.6.2. Splitting Tensile Strength of Concrete Cylinders (ASTM C496) This test method covers the determination of splitting tensile strength of concrete cylinders. The procedure for preparation of specimens for split cylinder testing is similar to the procedure described in the Section 3.6.1 of this report. Figure 3.19 shows schematic diagram of the split tensile strength test. This test method consists of applying a diametric compressive force along the length of a cylindrical concrete specimen at a rate that is within a prescribed range until failure occurs. This loading induces tensile stresses on the plane containing the applied load and relatively high compressive stresses in the area immediately around the applied load. Tensile failure 39 occurs rather than compressive failure because the areas of load application are in a state of multi axial compression, thereby having a much higher resistance as compared to uniaxial compressive strength test result. [ASTM C496 (1996)] The test was performed in the Universal Testing Machine (see Figure 3.17). The load and stroke values are recorded by the test machine and the split tensile stresses were calculated by using the Eq. 3.2. T=2P/πld (Eq. 3.2) Where, T = splitting tensile strength, psi (kPa), P = maximum applied load indicated by the testing machine, lbf (kN), l = length, in. (m), and d = diameter, in.(m). Tensile stress-strain and strength-time curves were plotted for plain and PPFRC and then compared. 3.6.3. Flexure Strength of Concrete Beams (ASTM C78) This test method covers the determination of the flexural strength of concrete by the use of a simple beam with third-point loading. The preparation of sample is the same as described in ASTM C42 [ASTM C42 (1999)]. For the purpose of finding indirect tensile strength of plain concrete and PPFRC, a total fourteen (14) - 3''x 6''x72'' beams specimens were cast and tested under two point loads. The section and span of the beam specimens is shown in Figure 3.20. The testing procedure as described in ASTM C78 implies that the third point loading method shall be used in the testing and concrete bearing blocks will be employed, which will ensure that 40 forces applied to the beam will be perpendicular to the face of the specimen and applied without eccentricity. A schematic diagram of test set-up and loading is shown in Figure 3.21 [ASTM C78 (2001)]. The test was performed in the Universal Testing Machine. The load was applied by the downward movement of the platen. The loading assembly is shown in Figure 3.22. The load and displacement data were obtained for each beam specimen and the average values of replicate specimen were calculated and load-deflection (P-δ) curves were plotted. From the P-δ curves, the effect of various amount of PPF with different fibre length on the strength and the post peak deformation capacity was studied. 41 Table 3.1 Polypropylene technical data sheet (MATRIXX) Compressive Strength (psi) Flexural strength (psi) Tensile strength at break (psi) Elongation at break (%) Water absorption (%) Specific gravity Ignition point Melting point Heat & UV stabilization Thermal conductivity 5,500-8,000 6,000-8,000 4,500-6,000 100-600 Negligible (0.01-0.03) 0.90-0.91 593°C 160 - 170°C Long Term 2.8 10-4 cal cm/sec cm² °C Tensile modulus (ksi) 165-225 Compressive modulus (ksi) 150-300 Flexural modulus (ksi @ 170-250 25°C.) Electrical conductivity Low Salt resistance High Acid resistance High Alkali resistance 100% (alkali proof) 42 ASTM D695 ASTM D790 ASTM D638 ASTM D638 ASTM D570 ASTM C177 ASTM D638 ASTM D695 ASTM D790 Table 3.2 Mix No. PCC PPFRC 0.4-25 PPFRC 0.6-25 PPFRC 0.8-25 PPFRC 0.4-38 PPFRC 0.6-38 PPFRC 0.8-38 Mix proportion of concrete mixtures in Kg/m³ Fibre Content Fibre (Kg/m³) Volume Fraction (%) 0 3.6 5.4 7.2 3.6 5.4 7.2 0 0.4 0.6 0.8 0.4 0.6 0.8 Fibre Length Cement mm (Kg/m³) 25 25 25 38 38 38 Fine Coarse Agg. Agg. (Kg/m³) (Kg/m³) 440 760 970 0.6 525 788 920 0.55 585 788 920 0.55 *added to increase slump value after fibre was added into the concrete PPFRC Vf (%)-Length of PPF (mm) 1 Kg/m³ = 1.68 lb/ft³ 43 w/c Ratio SuperPlasticizer (L/m³) 2.2 5.25 5.25 5.25 5.85 5.85 5.85 Table 3.3 Experimental matrix for workability tests Standard Slump Test Mix No. Vertical Slump Slump Type (in) Compacting Factor Test Flow Table J-Ring Test C.F Diameter Diameter (kg/kg) (in) (in) L- Box Test VFunnel Blocking Ratio H₂₂/H₁₁ (in/in) Flow Time (sec.) PCC PPFRC 0.425 PPFRC 0.625 PPFRC 0.825 PPFRC 0.438 PPFRC 0.638 PPFRC 0.838 Table 3.4 Description A B Plastic Shrinkage Moisture Loss Experimental matrix for shrinkage tests Spacimen Size 4"x4"x11 1/4" Specimen 4"x4"x11 1/4" Specimen Testing Age No. of Samples for Vf=0% No. of Samples for Vf=0.2% No. of Samples for Vf=0.4% Total specimens 24 hr 3 6 6 15 48 hr - - - 0 72 hr - - - 0 96 hr 24 hr - - - 0 3 6 6 15 48 hr - - - 0 72 hr - - - 0 96 hr - - - 0 44 Results Length Change (∆L) Weight loss (%) Table 3.5 Description A B1 B2 Compressive Strength Experimental matrix for mechanical properties Spacimen Testing No. of No. of Size Age Samples Samples for for Vf=0% Vf=0.4 % 7 Days 3 6 4"x8" Cylinders Indirect Tension Split Cylinder 4"x8" Cylinders Indirect TensionBeams 3"x6" x72" Beams 14 Days 28 Days 7 Days 14 Days 28 Days 28 Days Total No. of No. of Samples Samples specimen for for Vf=0.6% Vf=0.8% 6 6 21 3 6 6 6 21 3 6 6 6 21 3 6 6 6 21 3 6 6 6 21 3 6 6 6 21 2 4 45 4 4 Results 14 StressStrain property StressStrain property P-δ curves Figure 3.1 Fibrillated polypropylene fibre Figure 3.2 Polypropylene fibres of different length 46 Avg. Compressive Strength(psi) 4000 3500 3 days 28 days 14 days 3000 3046 2500 3372.03 3147 2000 1500 Average of 3 replicate specimen 1000 500 0 0 5 10 15 20 25 30 Time(days) Figure 3.3 The average compressive strength-time curve of 2”x2” mortar cubes Figure 3.4 Pictorial view of rotary drum mixer 47 Figure 3.5 Pictorial view of freshly prepared FFRRC Figure 3.6 Pictorial view of standard slump test apparatus [Eric et al (2003)] 48 Figure 3.7 Types of concrete slump [Eric et al (2003)] Figure 3.8 Compacting factor test apparatus [Eric et al (2003)] 49 Figure 3.9 Pictorial view of flow table test apparatus [Technical Bulletin 1506] Figure 3.10 Pictorial view of J-ring test apparatus [Eric et al (2003)] 50 Figure 3.11 Pictorial view of L-box test apparatus [Eric et al (2003)] Figure 3.12 Pictorial view of V-funnel test apparatus [Eric et al (2003)] 51 Figure 3.13 Pictorial view of shrinkage moulds lined with plastic sheets Figure 3.14 Pictorial view of shrinkage specimen after casting 52 Figure 3.15 Pictorial view of length measurement instrument Figure 3.16 Schematic view of standard shrinkage specimen 53 Figure 3.17 The universal testing machine Figure 3.18 Schematic diagram of the compressive strength test setup 54 Figure 3.19 Schematic diagram of the tensile split test setup Figure 3.20 Flexure test beam profile and section 55 Figure 3.21 Schematic diagram for flexure test Figure 3.22 Pictorial view of the loading assembly for two-point flexure test 56 CHAPTER 4 RESULTS AND DISCUSSION 4.1. INTRODUCTION The fabrication, curing of the test specimens was presented in Chapter 3. In this chapter, the results of laboratory tests are presented and discussed. These include results of workability tests of fresh concrete using six (6) different test procedures, results of early age shrinkage tests, results of compression tests at test ages of 7, 14 and 28 days respectively, results of split cylinder tests at test ages of 7, 14 and 28 days respectively, and results of beam flexural tests at 28 days. 4.2. WORKABILITY OF FRESH PPFRC For the workability of fresh concrete, the six (6) tests used were traditional Slump Cone Test, Compacting Factor, Flow Table diameter, J-Ring Diameter, L-Box blockage ratio and V-funnel time tests. These tests were performed on concrete without polypropylene fibres (PPF) termed as “control” specimens and on polypropylene fibre reinforced concrete (PPFRC) specimens. For the PPFRC specimens, variables included length of polypropylene fibres (lf) and the volume fraction (Vf) of polypropylene fibres. The tests results of various fresh properties tests of Plain Concrete (PC) and polypropylene fibre reinforced concrete (PPFRC) with different volume fraction (Vf) and length of fibre (Lf) are presented in the Table 4.1. The PPFRC mixtures were proportioned to give slump values which are needed to ascertain adequate workability of the fresh concrete to be placed and finished. For all the concrete mixes having different fibre contents and with different lengths of fibres, the measured slump is greater than 3 in. (76 mm), which is an acceptable slump values for the ease of construction and finsishability. For the PPFRC mixtures, in order to maintain reasonable slump, and approximately similar w/c, the quantity of cement was increased with increase in amount of chemical admixture as segregation 57 was observed to occur when only water content was increased in order to increase the workability of the PPFRC mixtures. Pictorial view of various workability tests are shown in Figure 4.1-4.8. The addition of polypropylene fibres (PPF) reduced the flow characteristics when L-Box and VFunnel tests were performed for the different mixtures. This is because during mixing of the concrete, the coarse aggregates damage the fibrillated PPF fibres to some degree and perhaps do not permit the PPF to fully open into a lattice structure, instead the PPF open into a network of linked fibre filaments and individual fibres. These fibres adhere to the cement paste because of their large specific surface area. The concrete mixtures with polypropylene fibres (PPF) result in lower (reduced) bleeding and segregation as compared to plain concrete. This is because the PPF help in maintaining the continuum (holding the concrete together or increasing the cohesiveness of concrete) and thus reduces the segregation of the coarse aggregates. The effect of fibre length (Lf) on the vertical slump for different fibre volume fractions (Vf) is shown in Figure 4.9. It can be seen that greater the fibre length (Lf), greater is the measured slump. This is because for a fixed volume fraction of PPF in PPF mixtures, in the concrete, less number of longer fibres will be present as compared to the shorter length fibres. Fibre population will be smaller in case of longer fibres which results in larger slumps for the case of longer fibres. The effect of fibre volume fraction (Vf) on the slump for the two different lengths of fibres is shown in Figure 4.10. The results indicate an inverse relationship between the two parameters i.e. the slump (or the workability) decreases with increase in fibre volume fraction (Vf). This re-affirms the trends reported in the literature in Chapter 2 of this report. The experimental results show that a relationship does exist between the slump flow and the compacting factor (Figure 4.11). The compaction factor is parameter which gives the degree of compaction of the fresh concrete resulting from the application of a standard amount of work. From regression analysis the coefficient of determination (R²), is found to be 0.8382, which indicates that high degree of correlation between the between the slump flow and the compacting factor. 58 The relationship between the slump and diameters from J-Ring and the flow table tests are shown in Figure 4.12. The straight line regression equation with a coefficient of correlation of 0.9099 for the data of slump and the J Ring diameter is also shown in the Figure 4.12. The exponential line equation with a coefficient of correlation of 0.8242 for the data of slump and flow table diameter is also shown in the Figure 4.12. This indicates that the relationship of slump with J ring diameter is seemingly stronger than the relationship between slump and the flow table diameter. 4.3. PLASTIC SHRINKAGE OF FRESH PPFRC The test procedure for shrinkage test is described in the Chapter 3. The results of the shrinkage tests performed on the control specimen PC and four different PPFRC mixtures are shown in Table 4.2. The length measurement was done using a digital calliper (see Figure 4.13) and then the results were computed using Eq. 3.1. The results were then plotted against time and then compared. The graphical representation of the results is given in Figure 4.14. In general it can be noted that the shrinkage of both PC and PPFRC mixtures varies greatly in the initial 24 hours and then gradually reduces with the passage of time. From Figure 4.14, it is evident that the shrinkage of PC specimens is larger than shrinkage of PPFRC specimens and that addition of PPF reduces the early age plastic shrinkage of concrete. Among the four PPFRC mixtures, the PPFRC 0.4-25 is found to be the most efficient in controlling early age shrinkage as it showed the maximum average shrinkage of 0.106% at 72 hours. The other three mixtures i.e. PPFRC 0.2-25, PPFRC 0.2-38 and PPFRC 0.4-38 showed the maximum average shrinkage of 0.378%, 0.165% and 0.312% respectively. Here it can be noted that for 25 mm long PP fibre, higher Vf (0.4%) showed better performance in controlling plastic shrinkage than that of smaller Vf (0.2%). Thus for 25 mm long PP fibre, the early age shrinkage reduces with the increasing Vf. For the case of 38 mm long PP fibres, plastic shrinkage for the Vf of 0.4% was greater than for Vf of 0.2%. Higher Vf showed greater plastic shrinkage. A similar trend was also reported by Collins [F. Collins et al (2008)]. The drying shrinkage of concrete mixture with 0.5% fiber volume fraction, cured for 1-day and 7days was higher than that of the plain concrete [F. Collins et al (2008)]. 59 The moisture loss rate was also determined for the control PC and four PPFRC mixtures. The readings of weight of 4” x 4” x 11 ¼” specimens were taken at the same time interval, when the shrinkage readings were recorded. The results of weight loss test are presented in Table 4.3 and Table 4.4. The graphical representation of moisture loss with time is shown in Figure 4.15, which shows the same trend for all the mixtures as that of shrinkage. The moisture loss is greater for the first 24 hours and then gradually slows down. It is also clear that the PC showed the least weight loss of 1.86% at 72 hours as compared to the PPFRC, which may be because of hydrophobic property of the fibres which enable the water from being absorbed and so it evaporates at higher rate for the PPFRC. Among the four PPFRC mixtures, the PPFRC 0.4-38 showed the greatest loss of water i.e. 3.169% at 72 hours. The other three mixtures, i.e. PPFRC 0.2-25, PPFRC 0.4-25 and PPFRC 0.2-38 showed 2.091%, 1.863% and 2.895% moisture loss at 72 hours respectively. The slower rate of moisture loss in PPFRC is primarily because of the reason that presence of fibres in the concrete increase the time to initial and final set of the concrete and so a slower rate of drying of water from the mix. [S.K.Singh (2010)] To be more precise, the fibrillated fibres, when mixed in concrete, open into a network of linked fibre filament which possibly reduce the settlement of heavier mix constituents (e.g., aggregates), thereby reducing the upward movement of water (bleeding) in concrete and also the rate of moisture loss from the exposed surface on concrete. [Alhozaimy et al (1995)]. 4.4. MECHANICAL PROPERTTIES OF HARDENED PPFRC The addition of the PPF to the concrete mixtures has beneficial effects on the mechanical properties of hardened concrete. The effect of volume of fibres (Vf) and the length of fibres (Lf) on the mechanical properties such as compressive strength, split cylinder tensile strength, flexural tensile strength at different test ages are reported. 60 4.4.1. Compression Test Results The compressive strength tests were performed on one plain concrete mixture “Control” concrete and six (6) polypropylene fibre reinforced concrete (PPFRC) mixtures. The seven different mixtures were PPC, PPFRC 0.4-25, PPFRC 0.6-25, PPFRC 0.8-25, PPFRC 0.4-38, PPFRC 0.6-38, and PPFRC 0.8-38 respectively. These were tested at the ages of 7, 14 and 28 days. Three replicate specimens were tested at each test age for each type of mixture. At each of the test age, three (3) specimen were taken out from curing, dried and then caped with sulphur and were tested to get the load-stroke data. From the load-stroke data, stress-strain data was computed. From the stress-strain data of each of the 3 specimens, an average stress-strain data was obtained, which was plotted. Microsoft Excel design sheet is attached in Appendix-I. The The resulting average compressive stress-vertical displacement curves are shown in the figures. The pictorial views of the failure surface of PC and PPFRC specimen are shown in Figure 4.16 and Figure 4.17 respectively. The effect of volume fraction of fibre (Vf) on the compressive stress- strain at different test ages is shown in Figure 4.18 – Figure 4.23. From figures it is clear that the fibres tend to increase the ductility of the mix by increasing the failure strains however these have varying effect on the compressive strength. The smaller strain of PC is because of the fact that after the concrete reaches its peak stress; cracks appear and as the loading continues the failure is occurred by the crushing of the concrete specimen at a relatively lower value of strain. However in PPFRC mixtures the increase in strains is due to the fact that these fibres have an interlocking capability which allows these to hold the mixture together even after cracking and so prevents the effect of shattering force. In PPFRC specimens, the bulging of specimens was observed without any significant deterioration of the test specimen. The effect of length of fibre (Lf) on the compressive stress- strain of concrete mixture tested at different test ages is shown in and Figure 4.24 – Figure 4.32. The figures show that the 28 day strengths of PPFRC with 25 mm long fibres are greater than that 61 on the respective PPFRC with 38 mm long fibres. This is true for all the volume fractions used. The strength-time curve for PC and the six (6) PPFRC mixtures are shown in Figure 4.33 – Figure 4.37. The compressive strengths of PPFRC mixtures are found to be less than that of PC except for the PPFRC 0.6-25 which showed an increase of 19.4% in 28 day strength. The decrease in compressive strength may be because the presence of fibres introduces more air voids in the composite and also create consolidation and compaction problems and hence reduces the compressive strength of the mix. 4.4.2. Splitting Cylinder Tensile Test Results The splitting cylinder tensile tests were performed on one plain concrete mixture “Control” concrete and six (6) polypropylene fibre reinforced concrete (PPFRC) mixtures as described in the Section 4.4.1 of the report. The seven different mixtures were PPC, PPFRC 0.4-25, PPFRC 0.6-25, PPFRC 0.8-25, PPFRC 0.4-38, PPFRC 0.6-38, and PPFRC 0.8-38 respectively. These were tested at the ages of 7, 14 and 28 days. Three replicate specimens were tested at each test age for each type of mixture. At each of the test age, the specimens were tested and the load-stroke data was obtained from which stress-displacement data was computed. From the stress- displacement data of each of the 3 specimens, an average stress-displacement data was obtained, which was plotted. The Microsoft Excel design sheet is attached in Appendix-I. The resulting average splitting tensile stress-vertical displacement curves are shown in the Figures. The average stress-displacement behaviour of PC shows a linear trend up to the cracking (Figure 4.38). After the first crack occurs, the strength of the PC reduces immediately and the crack widening leads to the splitting of the cylinder. (See Figure 4.39) The average stress-displacement behaviour of PC and PPFRC with different Vf and Lf at different test ages are shown in Figure 4.40- Figure 4.54. From these figures, it can 62 be seen that the stress-displacement behaviour up to first crack is almost the similar for both PC and PPFRC; however the post-peak behaviour is different and the addition of PP fibres to concrete helps in increasing the post peak deformation capacity and enhancing the post-cracking strength of PPFRC in tension. In the case of PPFRC, the PP fibres come into action after the first crack. The PP fibres bridge these cracks and restrain them from further opening and hence improve the load-carrying capacity of structural member beyond cracking. After the first crack, a drop in the stress is noted which shows the stress transfer from concrete to the randomly distributer fibres, which further take the applied load by elongating. (See Figure 4.55) The failure or the splitting on the cylinder occurred when the fibres elongation exceed the allowable i.e. the breaking of the fibres under axial tension. (See Figure 4.56) The effect of Vf on average strength-time curves for these concrete mixtures is shown in Figure 4.57 and Figure 4.58 and the effect of Lf on the average splitting tensile strength-time curves is shown in Figure 4.59-Figure 4.61. 4.4.3. Flexural (Indirect Tensile) Test Results The flexural tests were performed on beam specimen prepared from the same seven (7) of mixtures as mentioned in Section 4.1 and the tests were performed at test age of 28 days only. At the test age, three (3) replicate specimens were tested with the Universal Testing Machine (UTM) following the procedure described in the Chapter 3 of the report. The loading assembly and test set –up is shown in Figure 4.62. The behaviour of the PC and six (6) different PPFRC beams under flexure test were similar to that under splitting tensile strength test as both the tests indicate the indirect tensile behaviour (strength) of the material. Before the occurrence of the first crack, the load-deflection behaviour of all PPFRC beams was found to be similar to that of the plain concrete “control” beams. Just after the appearance of the first crack, “control” beams suddenly failed and the load-defection behaviour showed a steep and 63 sharp drop after the peak (maximum) load and thus exhibited little or no post-cracking deformation capacity (Figure 4.63). However in PPFRC beams, after the occurrence of the first crack, a drop is observed in the load-deflection curve as the load is released and transferred from the matrix to the fibres, and afterwards that the beams continues to withstand a portion of the load with increasing deformations and widening of the cracks (Figure 4.64) The PPFRC beams continue to resist load with increasing deformations by virtue of the elongation of the randomly distributed discrete fibres and ultimately fails at large deformations as the fibres reach their maximum elongation (Figure 4.65) The fractured surfaces of the PC and the PPFRC beams are shown in Figure 4.66. The load-stroke data was obtained from which strength-displacement data was computed and plotted. The Microsoft Excel design sheet is attached in Appendix-I. The effect of Vf on the average flexure strength-displacement curves of the concrete mixtures is shown in Figure 4.67 and Figure 4.68. The peak flexure strength of PC beams is higher than that of PPFRC beams however PPFRC beams showed greater displacement capacity. Among the PPFRC beams with different Vf of PPF, the beams with Vf 0.8% (7.2 Kg/m3) of both the 25 mm and 38 mm long PPF showed greatest deformation (vertical displacement). The effect of Lf on the average flexure strengthdisplacement curves is shown in Figure 4.69 to Figure 4.71. The PPFRC with 38 mm long PPF showed greater deformation (vertical displacement) capacity as compared to the PPFRC with 25 mm long PPF. The combined effect of Vf and Lf on the average flexure strength-displacement behaviour is that the PPFRC with the greatest Vf and Lf showed the greatest vertical displacement. Numerically the PPFRC 0.8-38 beams showed the average vertical displacement of about 20 times greater than that of control beams. The displacement ductility is improved by the introduction of PPF (see Table 4.2). 64 Table 4.1 Test results of various fresh properties tests of PC and PPFRC with different volume fraction and length of fibre Standard Slump Test Mix No. Vertical Slump Slump Type (in) PC PPFRC 0.4-25 PPFRC 0.6-25 PPFRC 0.8-25 PPFRC 0.4-38 PPFRC 0.6-38 PPFRC 0.8-38 Compacting Factor Test Flow Table Test J-Ring Test L- Box Test V-Funnel Test C.F (computed) Dia. Dia. Blocking Ratio H₂/H₁ Flow Time (kg/kg) (in) (in) (in/in) (sec.) 8.0 True 0.987 15.35 14.0 0.58 3.79 6.5 True 0.957 15.0 12.5 Blockage Blockage 6.0 True True 0.944 13.5 12.0 Blockage Blockage 0.919 12.0 11.0 Blockage Blockage 3.8 9.0 Collapse 0.986 15.5 15.3 Blockage Blockage 7.5 Collapse 0.956 14.0 13.0 Blockage Blockage 6.8 Collapse 0.94 14.35 13.35 Blockage Blockage 65 Table 4.2 Time Shrinkage test results of PC and PPFRC Mix ID (hour) 0 24 48 72 0 24 48 72 0 24 48 72 0 24 48 72 0 24 48 72 PC PPFRC 0.2-25 PPFRC 0.4-25 PPFRC 0.2-38 PPFRC 0.4-38 ΔL ΔL ΔL Average ΔL (%) (%) (%) (%) 0.000 -0.5562 -0.6985 0.000 -0.407 -0.420 0.000 -0.630 -0.643 0.000 -0.531 -0.587 -0.6985 0.0000 -0.2119 -0.3841 -0.512 0.000 -0.473 -0.578 -0.746 0.000 -0.080 -0.133 -0.652 0.000 -0.255 -0.365 -0.4106 0.0000 -0.0137 -0.0684 -0.591 0.000 -0.013 -0.026 -0.133 0.000 -0.013 -0.025 -0.378 0.000 -0.013 -0.040 -0.1643 - -0.078 0.000 -0.039 -0.064 -0.076 0.000 -0.101 -0.127 -0.106 0.000 -0.070 -0.096 - -0.103 0.000 -0.107 -0.413 -0.228 0.000 -0.099 -0.149 -0.165 0.000 -0.103 -0.281 - -0.426 -0.199 -0.313 66 Table 4.3 Weight measurements of PC and PPFRC Time Weight (gms.) (hours) PC PPFRC 0.2-25 PPFRC 0.4-25 PPFRC 0.2-38 PPFRC 0.4-38 0 6740 6838 6.762 6.806 6.816 24 6660 6744 6.672 6.620 6.607 48 6631 6712 6.645 6.616 6.603 72 6618 6695 6.636 6.609 6.600 Table 4.4 Weight loss percentage of PC and PPFRC Time Weight loss (%) (hours) PC PPFRC 0.2-25 PPFRC 0.4-25 PPFRC 0.2-38 PPFRC 0.4-38 0 0 0 0 0 0 24 -1.187 -1.375 -1.331 -2.733 -3.066 48 -1.617 -1.843 -1.730 -2.792 -3.125 72 -1.810 -2.091 -1.863 -2.895 -3.169 Table 4.5 Displacement ductility calculated from experimental results for the flexure tests of PC and PPFRC with different volume fraction and length of fibre Concrete Mix PC PPFRC 0.4-25 PPFRC 0.6-25 PPFRC 0.8-25 PPFRC 0.4-38 PPFRC 0.6-38 PPFRC 0.8-38 Displacement at Yield δy (in) 0.039094 0.039685 0.037205 0.042756 0.044488 0.036220 0.044961 Displacement at Ultimate δu (in) 0.042598 0.490866 0.440000 0.538228 0.680394 0.841417 0.924094 67 Displacement Ductility µ (in/in) 1.089627 12.369048 11.826455 12.588398 15.293805 23.230435 20.553246 Figure 4.1 Pictorial view of the slump cone after the removal of the standard slump cone for PPFRC trial mix. Figure 4.2 Pictorial view of measurement of the weight of partially compacted fresh concrete for evaluating Compacting factor 68 Figure 4.3 Pictorial view of measurement of the diameter of fresh concrete after flow table test for PC Figure 4.4 Pictorial view of J-Ring test for PC 69 Figure 4.5 Pictorial view of J-Ring test for PPFRC 0.8-25 Figure 4.6 Pictoria view of L-Box test for PC 70 Figure 4.7 Pictorial view of L-Box test for PPFRC 0.8-38. Figure 4.8 Pictorial view of V-Funnel test for PC 71 Figure 4.9 Effect of Fibre length (Lf ) on slump Figure 4.10 Effect of fibre volume fraction (Vf ) on slump 72 Figure 4.11 Relationship between slump and compacting factor Figure 4.12 Relationship between slump and flow table diameter 73 Figure 4.13 Pictorial view of length measurement for PPFRC specimen Figure 4.14 Average shrinkage-time curve for PC and PPFRC 74 Figure 4.15 Average weight loss-time curve for PC and PPFRC 75 Figure 4.16 Pictorial views of PPC and PPFRC specimens under compressive strength test. Figure 4.17 Pictorial views of PCC and PPFRC specimens after compressive strength test. 76 3000 PCC PPFRC 0.4-25 PPFRC 0.6-25 2500 PPFRC 0.6-25 PCC PPFRC 0.8-25 Avg. Stress (psi) 2000 PPFRC 0.4-25 1500 1000 PPFRC 0.8-25 500 0 0 0.001 0.002 0.003 0.004 0.005 0.006 0.007 0.008 Avg. Strain (in/in) Figure 4.18 Effect of Vf on average compressive stress-strain curve for PCC and PPFRC with 25 mm long fibres at 7 days. 3000 PCC PPFRC 0.4-38 PPFRC 0.4-38 2500 PPFRC 0.6-38 Avg. Stress (psi) PCC 2000 PPFRC 0.8-38 PPFRC 0.6-38 1500 PPFRC 0.8-38 1000 500 0 0 0.001 0.002 0.003 0.004 0.005 Avg. Strain (in/in) 0.006 0.007 Figure 4.19 Effect of Vf on average compressive stress-strain curve for PCC and PPFRC with 38 mm long fibres at 7 days 77 0.008 3000 PCC PPFRC 0.4-25 PPFRC 0.6-25 PPFRC 0.8-25 PPFRC 0.6-25 2500 PPFRC 0.4-25 Avg. Stress (psi) 2000 PPFRC 0.8-25 PCC 1500 1000 500 0 0 0.001 0.002 0.003 0.004 0.005 Avg. Strain (in/in) 0.006 0.007 0.008 0.009 Figure 4.20 Effect of Vf on average compressive stress-strain curve for PCC and PPFRC with 25 mm long fibres at 14 days. 3000 PCC PPFRC 0.4-38 2500 PPFRC 0.6-38 PPFRC 0.6-38 Avg. Stress (psi) PPFRC 0.8-38 PCC 2000 PPFRC 0.4-38 1500 1000 500 PPFRC 0.8-38 0 0 0.001 0.002 0.003 0.004 0.005 Avg. Strain (in/in) 0.006 0.007 0.008 Figure 4.21 Effect of Vf on average compressive stress-strain curve for PCC and PPFRC with 38 mm long fibres at 14 days. 78 0.009 4500 Avg. Stress (pssi) PCC 4000 PPFRC 0.6-25 3500 PCC PPFRC 0.4-25 PPFRC 0.6-25 PPFRC 0.8-25 PPFRC 0.4-25 3000 2500 PPFRC 0.8-25 2000 1500 1000 500 0 0 0.002 0.004 0.006 Avg. Strain (in/in) 0.008 0.01 0.012 Figure 4.22 Effect of Vf on average compressive stress-strain curve for PCC and PPFRC with 25 mm fibres at 28 days. 4500 PCC 4000 PPFRC 0.4-38 PCC Avg. Stress (psi) 3500 PPFRC 0.6-38 PPFRC 0.8-38 PPFRC 0.6-38 3000 2500 PPFRC 0.4-38 2000 PPFRC 0.8-38 1500 1000 500 0 0 0.002 0.004 0.006 Avg. Strain (in/in) 0.008 0.01 Figure 4.23 Effect of Vf on average compressive stress-strain curve for PCC and PPFRC with 38 mm fibres at 28 days. 79 0.012 3000 PCC PPFRC 0.4-25 2500 PPFRC 0.4-38 PPFRC 0.4-38 Avg. Stress (psi) 2000 PCC 1500 1000 500 PPFRC 0.4-25 0 0 0.001 0.002 0.003 0.004 0.005 Avg. Strain (in/in) 0.006 0.007 0.008 Figure 4.24 Effect of Lf on average compressive stress-strain curve for PCC and PPFRC with 0.4% volume fraction of PPF at 7 days. 3000 PCC PPFRC 0.6-25 PPFRC 0.6-38 PPFRC 0.6-25 2500 Avg. Stress (psi) 2000 PCC PPFRC 0.6-38 1500 1000 500 0 0 0.001 0.002 0.003 0.004 0.005 Avg. Strain (in/in) 0.006 0.007 Figure 4.25 Effect of Lf on average compressive stress-strain curve for PCC and PPFRC with 0.6% volume fraction of PPF at 7 days. 80 0.008 3000 PCC PPFRC 0.8-25 2500 PPFRC 0.8-38 Avg. Stress (psi) 2000 PCC PPFRC 0.8-25 1500 PPFRC 0.8-38 1000 500 -0.001 0 1E-17 0.001 0.002 0.003 0.004 Avg. Strain (in/in) 0.005 0.006 0.007 0.008 Figure 4.26 Effect of Lf on average compressive stress-strain curve for PCC and PPFRC with 0.8% volume fraction of PPF at 7 days. 3000 PCC Avg. Stress (psi) 2500 PPFRC 0.4-25 PPFRC 0.4-25 PCC PPFRC 0.4-38 PPFRC 0.4-38 2000 1500 1000 500 0 0 0.001 0.002 0.003 0.004 0.005 0.006 0.007 0.008 Avg. Strain (in/in) Figure 4.27 Effect of Lf on average compressive stress-strain curve for PCC and PPFRC with 0.4% volume fraction of PPF at 14 days. 81 0.009 3000 PCC 2500 PPFRC 0.6-25 PPFRC 0.6-25 Avg. Stress (psi) PPFRC 0.6-38 2000 PCC 1500 1000 PPFRC 0.6-38 500 0 0 0.001 0.002 0.003 0.004 0.005 0.006 0.007 0.008 0.009 Avg. Strain (in/in) Figure 4.28 Effect of Lf on average compressive stress-strain curve for PCC and PPFRC with 0.6% volume fraction of PPF at 14 days. 3000 PCC PPFRC 0.8-25 2500 PPFRC 0.8-38 PCC Avg. Stress (psi) 2000 PPFRC 0.8-25 1500 PPFRC 0.8-38 1000 500 0 0 0.001 0.002 0.003 0.004 0.005 0.006 0.007 0.008 Avg. Strain (in/in) Figure 4.29 Effect of Lf on average compressive stress-strain curve for PCC and PPFRC with 0.8% volume fraction of PPF at 14 days. 82 0.009 4500 PCC 4000 PPFRC 0.4-25 PCC 3500 PPFRC 0.4-38 PPFRC 0.4-25 Avg. Stress (pssi) 3000 2500 PPFRC 0.4-38 2000 1500 1000 500 0 0 0.002 0.004 0.006 0.008 0.01 0.012 Avg. Strain (in/in) Figure 4.30 Effect of Lf on average compressive stress-strain curve for PCC and PPFRC with 0.4% volume fraction of PPF at 28 days. 4500 PCC PPFRC 0.6-25 4000 3500 PPFRC 0.6-25 PCC PPFRC 0.6-38 Avg. Stress (pssi) 3000 PPFRC 0.6-38 2500 2000 1500 1000 500 0 0 0.002 0.004 0.006 0.008 0.01 Avg. Strain (in/in) Figure 4.31 Effect of Lf on average compressive stress-strain curve for PCC and PPFRC with 0.6% volume fraction of PPF at 28 days. 83 0.012 4500 PCC 4000 PPFRC 0.8-25 3500 PCC PPFRC 0.8-38 Avg. Stress (pssi) 3000 2500 PPFRC 0.8-25 2000 PPFRC 0.8-38 1500 1000 500 0 0 0.002 0.004 0.006 0.008 0.01 0.012 Avg. Strain (in/in) Figure 4.32 Effect of Lf on average compressive stress-strain curve for PCC and PPFRC with 0.8% volume fraction of PPF at 28 days. 4500 Avg. Compressive Strength (psi) 4000 3500 3000 2500 2000 1500 PCC 1000 PPFRC 0.4-25 500 PPFRC 0.6-25 PPFRC 0.8-25 0 0 7 14 21 28 Days Figure 4.33 Effect of Vf on average compressive strength-time curve for PCC and PPFRC with 25 mm long PP fibres. 84 35 4000 Avg. Compressive Strength (psi) 3500 3000 2500 2000 1500 PCC 1000 PPFRC 0.4-38 PPFRC 0.6-38 500 PPFRC 0.8-38 0 0 7 14 21 28 35 Days Figure 4.34 Effect of Vf on average compressive strength-time curve for PCC and PPFRC with 38 mm long PP fibres. Avg. Compressive Strength (psi) 3500 3000 2500 2000 1500 PPFRC 0.4-25 PPFRC 0.4-38 1000 0 7 14 21 28 Days Figure 4.35 Effect of Lf on average compressive strength-time curve for PPFRC with 0.4% volume fraction of PP fibres. 85 35 Avg. Compressive Strength (psi) 4500 4000 3500 3000 2500 2000 PPFRC 0.6-25 1500 PPFRC 0.6-38 1000 0 7 14 21 28 35 Days Figure 4.36 Effect of Lf on average compressive strength-time curve for PPFRC with 0.6% volume fraction of PP fibres. 4500 Avg. Compressive Strength (psi) PPFRC 0.8-25 4000 PPFRC 0.8-38 3500 3000 2500 2000 1500 1000 0 7 14 21 28 Days Figure 4.37 Effect of Lf on average compressive strength-time curve for PPFRC with 0.8% volume fraction of PP fibres. 86 35 400.00 350.00 PCC Avg. Splitting Stress (psi) PC 300.00 250.00 200.00 150.00 100.00 50.00 0.00 0 0.05 0.1 0.15 0.2 0.25 0.3 Vertical Displacement (in) Figure 4.38 Average splitting tensile stress-displacement curve for PC at 7 days. Figure 4.39 Pictorial view of failure surface of PC specimen under split tensile strength test. 87 400.00 Avg. Splitting Stress (psi) 350.00 PCC PPFRC 0.4-25 PPFRC 0.6-25 PPFRC 0.8-25 PC 300.00 PPFRC 0.8-25 250.00 PPFRC 0.6-25 PPFRC 0.4-25 200.00 150.00 100.00 50.00 0.00 0 0.05 0.1 0.15 0.2 0.25 0.3 Vertical Displacement (in) Figure 4.40 Effect of Vf on average splitting tensile stress-displacement curve for PC and PPFRC with 25 mm long fibres at 7 days. 400.00 Avg. Splitting Stress (psi) 350.00 PCC PPFRC 0.4-38 PPFRC 0.6-38 PPFRC 0.8-38 PC PPFRC 0.4-38 300.00 PPFRC 0.6-38 250.00 PPFRC 0.8-38 200.00 150.00 100.00 50.00 0.00 0 0.05 0.1 0.15 0.2 0.25 0.3 Vertical Displacement (in) Figure 4.41 Effect of Vf on average splitting tensile stress-displacement curve for PC and PPFRC with 38 mm long fibres at 7 days. 88 500 PCC PPFRC 0.4-25 PPFRC 0.6-25 PPFRC 0.8-25 450 PPFRC 0.6-25 Splitting Stress (psi) 400 350 PPFRC 0.4-25 300 250 200 PPFRC 0.8-25 150 PC 100 50 0 0 0.05 0.1 0.15 Vertical Displacement (in) 0.2 0.25 Figure 4.42 Effect of Vf on average splitting tensile stress-displacement curve for PC and PPFRC with 25 mm long fibres at 14 days. 400 PCC PPFRC 0.6-38 PPFCR 0.4-38 350 PPFRC 0.4-38 PPFRC 0.6-38 Splitting Stress (psi) 300 PPFRC 0.8-38 250 PPFRC 0.8-38 200 PC 150 100 50 0 0 0.05 0.1 0.15 Vertical Displacement (in) 0.2 0.25 Figure 4.43 Effect of Vf on average splitting tensile stress-displacement curve for PC and PPFRC with 38 mm long fibres at 14 days. 89 500 PCC PC 450 PPFRC 0.4-25 PPFRC 0.4 -25 Splitting Stress (psi) 400 PPFRC 0.6-25 PPFRC 0.6-25 350 300 PPFRC 0.8-25 PPFRC 0.8-25 250 200 150 100 50 0 0 0.05 0.1 0.15 0.2 0.25 Vertical Displacement (in) Figure 4.44 Effect of Vf on average splitting tensile stress-displacement curve for PC and PPFRC with 25 mm fibres at 28 days. 500 PPFRC 0.4 -38 PC 450 Avg. Splitting Stress (psi) 400 350 PPFRC 0.6 -38 300 250 PPFRC 0.8 -38 200 PCC 150 PPFRC 0.4-38 100 PPFRC 0.6-38 50 PPFRC 0.8-38 0 0 0.05 0.1 0.15 0.2 0.25 0.3 0.35 Vertical Displacement (in) Figure 4.45 Effect of Vf on average splitting tensile stress-displacement curve for PC and PPFRC with 38 mm fibres at 28 days. 90 0.4 400.00 PCC PPFRC 0.4-25 PPFRC 0.4-38 350.00 PC Splitting Stress (psi) 300.00 PPFRC 0.4-25 250.00 PPFRC 0.4-38 200.00 150.00 100.00 50.00 0.00 0 0.05 0.1 0.15 0.2 0.25 Vertical Displacement (in) Figure 4.46 Effect of Lf on average splitting tensile stress-displacement curve for PC and PPFRC with 0.4% volume fraction of PPF at 7 days. 400.00 PCC PC 350.00 PPFRC 0.6-25 PPFRC 0.6-38 Splitting Stress (psi) 300.00 PPFRC 0.6-25 250.00 PPFRC 0.6-38 200.00 150.00 100.00 50.00 0.00 0 0.05 0.1 0.15 0.2 Vertical Displacement (in) Figure 4.47 Effect of Lf on average splitting tensile stress-displacement curve for PC and PPFRC with 0.6% volume fraction of PPF at 7 days. 91 0.25 400.00 PCC PPFRC 0.8-25 PPFRC 0.8-38 350.00 PC 300.00 Splitting Stress (ksi) PPFRC 0.8-25 250.00 PPFRC 0.8-38 200.00 150.00 100.00 50.00 0.00 0 0.05 0.1 0.15 0.2 0.25 Vertical Displacement (in) Figure 4.48 Effect of Lf on average splitting tensile stress-displacement curve for PC and PPFRC with 0.8% volume fraction of PPF at 7 days. 500 Avg. Splitting Stress (psi) PCC 450 PPFRC 0.4-25 400 PPFRC 0.4-38 350 PPFRC 0.4-25 300 PPFRC 0.4-38 250 PC 200 150 100 50 0 0 0.05 0.1 0.15 Vertical Displacement (in) 0.2 Figure 4.49 Effect of Lf on average splitting tensile stress-displacement curve for PC and PPFRC with 0.4% volume fraction of PPF at 14 days. 92 0.25 400 PCC PPFRC 0.6-25 350 Avg. Splitting Stress (psi) PPFRC 0.6-38 300 PPFRC 0.6-38 PPFRC 0.6-25 250 PC 200 150 100 50 0 0 0.05 0.1 0.15 Vertical Displacement (in) 0.2 0.25 Figure 4.50 Effect of Lf on average splitting tensile stress-displacement curve for PC and PPFRC with 0.6% volume fraction of PPF at 14 days. 350 PC 300 Avg. Splitting Stress (psi) PCC PPFRC 0.8-25 PPFRC 0.8-38 PPFRC 0.8-25 250 PPFRC 0.8-38 200 150 100 50 0 0 0.05 0.1 0.15 Vertical Displacement (in) 0.2 Figure 4.51 Effect of Lf on average splitting tensile stress-displacement curve for PC and PPFRC with 0.8% volume fraction of PPF at 14 days. 93 0.25 500 PC 450 PPFRC 0.4-38 Avg. Splitting Stress (psi) 400 350 300 PPFRC 0.4 -25 250 200 150 PCC 100 PPFRC 0.4-25 50 PPFRC 0.4-38 0 0 0.05 0.1 0.15 0.2 0.25 Vertical Displacement (in) 0.3 0.35 0.4 Figure 4.52 Effect of Lf on average splitting tensile stress-displacement curve for PC and PPFRC with 0.4% volume fraction of PPF at 28 days. 500 PCC PPFRC 0.6-25 PPFRC 0.6-38 PC 450 Avg. Splitting Stress (psi) 400 PPFRC 0.6-38 350 300 PPFRC 0.6-25 250 200 150 100 50 0 0 0.05 0.1 0.15 0.2 0.25 Vertical Displacement (in) 0.3 0.35 Figure 4.53 Effect of Lf on average splitting tensile stress-displacement curve for PC and PPFRC with 0.6% volume fraction of PPF at 28 days. 94 0.4 500 PCC 450 PPFRC 0.8-25 PC PPFRC 0.8-38 Avg. Splitting Stress (psi) 400 350 PPFRC 0.8-25 300 PPFRC 0.8-38 250 200 150 100 50 0 0 0.05 0.1 0.15 0.2 0.25 Vertical Displacement (in) 0.3 0.35 Figure 4.54 Effect of Lf on average splitting tensile stress-displacement curve for PC and PPFRC with 0.8% volume fraction of PPF at 28 days. Figure 4.55 tensile test. Pictorial view of crack propagation of PPFRC cylinder under splitting 95 0.4 Figure 4.56 Pictorial view of the split PPFRC cylinder Avg. Splitting Tensile Strength (psi) 500 450 400 350 300 250 PCC 200 PPFRC 0.4-25 150 PPFRC 0.6-25 PPFRC 0.8-25 100 0 7 14 21 28 Days Figure 4.57 Effect of Vf on average splitting tensile strength-time curve for PC and PPFRC with 25 mm long PP fibres. 96 35 Avg. Splitting Tensiole Strength (psi) 500 450 400 350 300 250 PCC 200 PPFRC 0.4-38 150 PPFRC 0.6-38 PPFRC 0.8-38 100 0 7 14 21 28 35 Days Figure 4.58 Effect of Vf on average splitting tensile strength-time curve for PC and PPFRC with 38 mm long PP fibres. Avg. Splitting Tensile Strength (psi) 500 450 400 350 300 PPFRC 0.4-25 250 PPFRC 0.4-38 200 0 7 14 21 28 Days Figure 4.59 Effect of Lf on average splitting tensile strength-time curve for PPFRC with 0.4% volume fraction of PP fibre 97 35 Avg. Splitting Tensile Strength (psi) 500 450 400 350 300 PPFRC 0.6-25 250 PPFRC 0.6-38 200 0 7 14 21 28 35 Days Figure 4.60 Effect of Lf on average splitting tensile strength-time curve for PPFRC with 0.6% volume fraction of PP fibre Avg. Splitting Tensile Strength (psi) 500 450 400 350 300 250 PPFRC 0.8-25 PPFRC 0.8-38 200 0 7 14 21 28 Days Figure 4.61 Effect of Lf on average splitting tensile strength-time curve for PPFRC with 0.8% volume fraction of PP fibre 98 35 Figure 4.62 test. Pictorial view of the loading assembly for the two-point load flexure Figure 4.63 Pictorial view of the PC beam after failure. 99 Figure 4.64 Pictorial view of the PPFRC beam during flexure testing, showing wide crack and vertical displacement. Figure 4.65 Pictorial view of the PPFRC beam after collapse. 100 Figure 4.66 failure. Pictorial view of the PC and PPFRC beam fractured surface after 10 PCC PPFRC 0.4-25 PPFRC 0.6-25 PPFRC 0.8-25 9 PC 8 7 fr (ksi) 6 5 4 PPFRC 0.4-25 PPFRC 0.6-25 PPFRC 0.8-25 3 2 1 0 0 0.2 0.4 0.6 Displacement (in) 0.8 1 Figure 4.67 Effect of Vf on average flexure stress-displacement curve for PC and PPFRC with 25 mm fibres at 28 days. 101 1.2 10 PCC PPFRC 0.4-38 PPFRC 0.6-38 PPFRC 0.8-38 9 PC 8 7 fr (ksi) 6 5 PPFRC 0.4 -38 4 3 PPFRC 0.6 -38 2 PPFRC 0.8 -38 1 0 0 0.2 0.4 0.6 Displacement (in) 0.8 1 1.2 Figure 4.68 Effect of Vf on average flexure stress-displacement curve for PC and PPFRC with 38 mm fibres at 28 days. 10 PCC 9 PPFRC 0.4-25 PC 8 PPFRC 0.4-38 7 fr (ksi) 6 5 4 PPFRC 0.4-25 3 PPFRC 0.4-38 2 1 0 0 0.2 0.4 0.6 Displacement (in) 0.8 1 Figure 4.69 Effect of Lf on average flexure stress-displacement curve for PC and PPFRC with 0.4% volume fraction of fibres at 28 days. 102 1.2 10 PCC PPFRC 0.6-25 PPFRC 0.6-38 9 PC 8 7 fr (ksi) 6 5 4 PPFRC 0.6-25 3 PPFRC 0.6-38 2 1 0 0 0.2 0.4 0.6 Displacement (in) 0.8 1 1.2 Figure 4.70 Effect of Lf on average flexure stress-displacement curve for PC and PPFRC with 0.6% volume fraction of fibres at 28 days. 10 9 PCC PPFRC 0.8-25 PPFRC 0.8-38 PC 8 7 fr (ksi) 6 5 4 PPFRC 0.8-25 3 2 PPFRC 0.8-38 1 0 0 0.2 0.4 0.6 Displacement (in) 0.8 1 Figure 4.71 Effect of Lf on average flexure stress-displacement curve for PC and PPFRC with 0.8% volume fraction of fibres at 28 days. 103 1.2 CHAPTER 5 ANALYTICAL WORK 5.1. INTRODUCTION The chapter presents the analytical solution for stress-strain curves for PPFRC under compression using fractional equation. This model is developed in order to calibrate the compressive stress-strain curves obtained after testing the cylindrical specimen at the Material Testing Laboratory of the NED University of Engineering and Technology. The fractional equations used for this work are described in the next section followed by the analytical solution for the PC and PPFRC mixtures used in this study. 5.2. FRACTIONAL EQUATION FOR COMPRESSIVE STRESS STRAIN CURVE FOR PPFRC A fractional equation developed by Ahmad and Shah (1979, 1982, 1985) is used for analytically predicting the compressive stress-strain curve of plain and polypropylene fiber reinforced concrete (PPFRC). The fractional equation is expressed as Y= ( ) (Eq. 5.1) ( –) Where Y = fc/fc ' ' X = Ɛ c/ Ɛc For Plain Concrete Ɛ'c = 0.001648+0.000114 (f’c) (Eq. 5.2) 104 ' The Equation for peak strain (Ɛ c ) and constants for plain concrete were calibrated from a large data base by Ahmad and Shah (1-5). For pre-peak portion of the curve ' ' (Ɛc < Ɛ c ), the constants are A1, D1 are for the post-peak curve (Ɛc > Ɛ c ), the constants are A2, D2.. The calibrated constants for plain concrete of various strengths are shown in Table 5-1. For a given strength of plain concrete, the complete stressstrain curve can be obtained by using appropriate constants in the fractional equation and different values of strain as input and obtaining the corresponding values of stress. For the PPFRC, the fractional equation for plain concrete is used and the constants A and D were calibrated from the experimental test results for various length (Lf) of the PPF and various volume fractions (Vf) of PPF. The calibrated constants for PPFRC with different various lengths (Lf) of the PPF and different volume fractions of PPF (Vf) are shown in Table 5.2. 5.3. COMPARISION BETWEEN EXPERIMENTAL RESULTS AND ANALYTICAL EXPRESSION The comparison of the experimental compressive stress strain curves and the analytical curves predicted by the use of fractional equation and the calibrated constants are shown in Figures 5.2 – 5.8. The comparisons are for the test age of 28 days. Figures 5.2-5.8 show that the analytical equation with calibrated constants adequately predicts the compressive stress strain curve of PPFRC and captures the effects of different various lengths (Lf) of the PPF and different volume fractions of PPF (Vf) on the stress strain curve. 5.4. SIMPLIFICATION OF CONSTANTS IN FRACTIONAL EQUATION For simplification of the constants in the fractional equation, a regression analysis was done for the values of the calibrated constants. The constants A1 and D1 and A2 and D2 can be expressed in terms of fc’, Vf and Lf. 105 The resulting expressions are: A1 = 1.37+0.01Lf-1.25Vf R2 = 0.704 (Eq. 5.3) D1 = 0.10-0.02Lf+3.13Vf R2 = 0.517 (Eq. 5.4) A2 = 0.12+0.001Lf+0.59Vf R2 = 0.458 (Eq. 5.5) D2= 1.13-0.00038Lf-0.28Vf R2 = 0.4189 (Eq. 5.6) And, For generating the analytical compressive stress-strain curve of plain and PPFRC concrete, the constants of Eq. 5.3-5.6 will facilitate the computations for the compressive stress strain curve. The values of the constants were computed using these equation and the values are presented in table 5.2. 106 Table 5-1 Calibrated constants of the fractional equation for PC (Plain) concrete for different strengths of concrete [Ahmad and Shah (1979, 1982, 1985) ]. fc' A1 D1 A2 D2 4 8 12 1.6003 1.3768 1.3244 0.6551 0.2581 0.1913 1.5045 0.283 0.1156 0.8801 0.9869 0.9964 Table 5-2 Calibrated constants of the fractional equation for PPFRC with different Lf and Vf . Lf Vf (mm) (%) A1 0.000 0.000 1.500 25.000 0.400 1.000 25.000 0.600 0.800 25.000 0.800 0.500 38.000 0.400 1.200 38.000 0.600 1.080 38.000 0.800 1.100 Average of Error Square Lf (mm) Vf A2 (%) 0.000 0.000 0.000 25.000 0.400 0.050 25.000 0.600 0.200 25.000 0.800 0.200 38.000 0.400 0.100 38.000 0.600 0.200 38.000 0.800 0.800 Average of Error Square A1 Error Square (computed) 1.370 1.120 0.870 0.620 1.250 1.000 0.750 A2 (computed) 0.017 0.014 0.005 0.014 0.003 0.006 0.123 0.03 Error Square 0.120 0.381 0.499 0.617 0.394 0.512 0.630 0.014 0.110 0.089 0.174 0.086 0.097 0.029 0.09 107 D1 0.500 0.700 0.500 2.000 0.600 0.700 3.000 D2 1.060 1.050 1.050 0.930 1.000 1.000 0.700 D1 (computed) 0.100 0.852 1.478 2.104 0.592 1.218 1.844 D2 (computed) 1.130 1.009 0.953 0.897 1.004 0.948 0.892 Error Square 0.160 0.023 0.956 0.011 0.000 0.268 1.336 0.39 Error Square 0.005 0.002 0.010 0.001 0.000 0.003 0.037 0.01 14 Stress (f'c = 4ksi) Stress (f'c = 8ksi) 12 12 ksi Stress (f'c = 12ksi) Compressive Stress (ksi) 10 8 ksi 8 6 4 ksi 4 2 0 0 0.001 0.002 0.003 0.004 0.005 0.006 0.007 0.008 strain (in/in) Figure 5.1 Typical analytical stress-strain curves of plain conrete of various strengths (Ahmad and Shah, 1982) 108 0.009 Avg. Compressive Stress (psi) 4000 PCC (NED Analytical) PC (Experimental) 3500 PCC (Experimental) 3000 PC (NED Analytical) 2500 2000 1500 1000 500 0 0 0.001 0.002 0.003 0.004 0.005 0.006 Avg. Strains (in/in) Figure 5.2 Comparison of experimental and analytical compressive stress-strain curve for PC at 28 days 3500 Avg. Compressive Stress (psi) 3000 PPFRC 04-25 (NED Analytical) PPFRC 04-25 (Experimental) PPFRC 0.4-25 (Experimental) 2500 PPFRC 0.4-25 (NED Analytical) 2000 1500 1000 500 0 0 0.001 0.002 0.003 Avg. Strains (in/in) 0.004 Figure 5.3 Comparison of experimental and analytical compressive stress-strain curve for PPFRC 0.4-25 at 28 days 109 0.005 4500 Avg. Compressive Stress (psi) PPFRC 06-25 (NED Analytical) PPFRC 06-25 (Experimental) PPFRC 0.6-25 (Experimental) 4000 3500 3000 PPFRC 0.6-25 (NED Analytical) 2500 2000 1500 1000 500 0 0.000 0.002 0.004 0.006 0.008 0.010 0.012 Avg. Strains (in/in) Figure 5.4 Comparison of experimental and analytical compressive stress-strain curve for PPFRC 0.6-25 at 28 days 3000 PPFRC 08-25 (NED Analytical) PPFRC 08-25 (Experimental) Avg. Compressive Stress (psi) 2500 2000 PPFRC 0.8-25 (NED Analytical) 1500 1000 PPFRC 0.8-25 (Experimental) 500 0 0.000 0.001 0.002 Avg. Strains (in/in) 0.003 0.004 Figure 5.5 Comparison of experimental and analytical compressive stress-strain curve for PPFRC 0.8-25 at 28 days 110 Avg. Compressive Stress (psi) 3000 PPFRC 0.4-38 (Experimental ) 2500 2000 PPFRC 0.4-38 (Experimental) PPFRC 0.4-38 (NED ANALYTICAL) PPFRC 0.4-38 (NED Analytical) 1500 1000 500 0 0.000 0.001 0.002 0.003 0.004 0.005 Avg. Strains (in/in) Figure 5.6 Comparison of experimental and analytical compressive stress-strain curve for PPFRC 0.4-38 at 28 days 3500 Avg. Compressive Stress (psi) 3000 PPFRC 0.6-38 (NED Analytical) PPFRC 0.6-38 (Experimental) PPFRC 0.6-38 (Experimental) 2500 2000 PPFRC 0.6-38 (NED Analytical) 1500 1000 500 0 0.000 0.001 0.002 0.003 0.004 0.005 0.006 0.007 Avg. Strains (in/in) 0.008 0.009 0.010 0.011 Figure 5.7 Comparison of experimental and analytical compressive stress-strain curve for PPFRC 0.6-38 at 28 days 111 2000 PPFRC 0.8-38 (NED Analytical) Avg. Compressive Stress (psi) 1800 1600 PPFRC 08-38 (Experimental) PPFRC 08-38 (NED ANALYTICAL) 1400 PPFRC 0.8-38 (Experimental) 1200 1000 800 600 400 200 0 0.000 0.001 0.002 0.003 Avg. Strains (in/in) 0.004 Figure 5.8 Comparison of experimental and analytical compressive stress-strain curve for PPFRC 0.8-38 at 28 days 112 0.005 CHAPTER 6 APPLICATIONS OF PPFRC IN CIVIL INFRASTRCUTURE 6.1. INTRODUCTION In this chapter, the applications of Polypropylene fibre reinforced concrete (PPFRC) in civil infrastructure are described. The uniform dispersion of fibres throughout the concrete mix provides near isotropic properties not common to conventionally reinforced concrete. The use of PPFRC in concrete construction and other applications is driven by the enhanced properties of PPFRC exhibits as compared to conventional concrete. Polypropylene fibre reinforced concrete (PPFRC) is recommended in all types of concretes which demonstrate a need for enhanced toughness characteristics, resistance to intrinsic cracking and improved water tightness. The main area of PPFRC applications includes buildings, bridges, highway pavements, industrial floorings, hydraulic structures, blast resistance, sewage and waste management and other applications. The major benefits of PPFRC include • Inhibits plastic settlement cracking. • Control plastic shrinkage cracking up to 80%. • Lowers water migration in concrete and control bleeding. • Improves flexural properties of concrete up to 30%. • Resist impact /shatter forces up to 14 times more than plain concrete. • Increase abrasion resistance significantly. • Provide fatigue endurance in fibre reinforced concrete not available in plain concrete. • Improve fire resistances of concrete 113 The typical dosages of PPF in concrete for various applications are shown in Table 6.1. Some of the examples of applications of PPFRC in civil infrastructure in Pakistan are presented next. 6.2. APPLICATIONS IN BUILDINGS The application of PPFRC in buildings include slabs, beams, balconies, overhangs and ledges, driveways, sidewalks, screed toppings and overlays, rooftop screeding, water storage tanks (both overhead and underground) pool construction, basements, architectural finishes, cement tiles and plastering, coloured concrete, foundations, drainage etc. Being wholly synthetic there is no corrosion risk. The possibility of increased tensile strength and impact resistance offers potential reductions in the weight and thickness of structural components and should also reduce the damage resulting from shipping and handling. The application of PPFRC for plastering in multi-storeyed building of Korangi is shown in Figure 6.1 and that of roof screeding of a building in DHA is shown in Figure 6.2. 6.3. APPLICATIONS IN BRIDGES In order to enhance the seismic performance and serviceability of bridges, focus has been on the development and implementation of innovative materials. PPFRC has the potential for seismic applications due to its increased strain capacity and reduced cracking i.e. its crack arresting capability. PPFRC is widely being used to control early age cracking on bridge decks and overlays. The addition of micro-fibres in amounts as small as 0.1% by volume is an effective method to control plastic shrinkage cracking in bridges. For controlling shrinkage cracking in bridge decks, PPFRC is commonly used in expansion joints. Its application in one of the bridges in Karachi is shown in Figure 6.3. 6.4. APPLICATIONS IN HIGHWAY PAVEMENTS Polypropylene fibre reinforced concrete (PPFRC) has been used in concrete slabs and pavements to reduce the amount of required shrinkage-and-temperature reinforcement. For the same wheel loads, the thickness of slabs with PPFRC could also be reduced and PPFRC slab of about ½ the thickness of conventional PCC slab would have about the same load carrying capacity. PPFRC paved aircraft parking are 114 now in service in severe and mild environments. Example of use of in Shaheen Air, Jinnah Airport Karachi, is shown in Figure 6.4 6.5. APPLICATIONS IN INDUSTRIAL FLOORING In industrial flooring, one of the main reasons of using polypropylene fibres in concrete slab is for crack control (inhibition of cracks or arresting of cracks). Better resistance to impact and other suddenly applied loads is also one of enhancements that provided by the use of PPF in concrete. Fibres help in distributing the impact forces to the entire body of concrete, thus reducing the concentration of the impact forces. Example of application of PPFRC in industrial flooring is shown in Figure 6.5. 6.6. APPLICATIONS IN DAMS AND HYDRAULIC STRUCTURES PPFRC is being used for the construction and repair of dams and other hydraulic Structures to provide better resistance to cavitation and severe erosion. The addition of polypropylene fibres in concrete has significant beneficial effects on reducing the deterioration of concrete surface skin subjected to sea water attack. Application of PPFRC in hydraulic structures is shown in the construction of water reservoir at Diamond Terrace, Gulshan-e-Maymar, Karachi (Figure 6.6). 6.7. APPLICATIONS IN BLAST RESISTANCE Since PPFRC exhibits superior impact resistance properties, its use in structures exposed to sudden impact or blast loading has advantages. The use of PPFRC in blast resistant structures can also have an additional benefit as it exhibits better fire resistance properties, in case fire accompanies the blast loading. Use of PPF in concrete cement plaster and concrete works provide significant improvement, reduction to spill-damage and better structural integrity. The effectiveness of PPFC in withstanding the blast forces was studied in the Military College of Engineering, Risalpur, Pakistan. (Figure 6.7) 115 6.8. APPLICATIONS IN SEWAGE AND WASTE WATER MANAGEMENT Polypropylene fibres are nonmagnetic and non-corrosive, as well as chemically inert. These fibres can withstand the chemical environment inside concrete. Because these fibres are unaffected by the alkaline environment of concrete, and are stable under long-term heat exposure, these fibres do not degrade and provide durable concrete reinforcement. These properties of fibres make them suitable for concrete application in sewage, manholes and waste water treatment plants. (Figure 6.8-6.9) 6.9. OTHER APPLICATIONS The other applications of PPFRC include applications in plaster to reduce plastic shrinkage cracking, applications to reduce plastic shrinkage cracking, and applications to increase abrasion resistance, increase freeze and thaw durability, control plastic settlement cracking etc. (Figure 6.10-6.11) The lists of some projects where PPFRC is used for different applications are attached in Appendix-II. 116 Table 6.1 Company) Typical dosages of PPFRC for various applications (MATRIXX Fibre Length (mm) Type of Work Minimum Dosage (gms/50 Kg cement bag) 100 Plaster Works (Including Colour Crete) 6 External Plaster Works, Precast Concrete and Repair of Plaster Works Residential and Commercial Roof Screed and Roof Slab, Industrial Flooring and Pavement, RCC Structure for Water Tank, Basement Walls, Manhole and Canal Lining Water Reservoir, Sewerage Drain, Storm Water Drain and Residential Roof Screed (Over Flexible Insulation Base) Heavy Duty Industrial Floor, Hanger Floor, Runway, Quay Wall, Sea Block, Bridge Deck Screed, Expansion Joint and 13 100 25+13 300 25+13 450 25 600 117 Figure 6.1 Application of PPFRC for plastering in Multistoried Building, Mehrunnisa Welfare Trust, Korangi, Karachi, Pakistan. Figure 6.2 Pakistan. Application of PPFRC in Roof Screeding, Creek Vista, DHA, Karachi, 118 Figure 6.3 Application of PPFRC in Jam Sadiq Bridge Deck and Expansion Joint at KPT Interchange, Karachi, Pakistan. NIP, PQA Figure 6.4 Application of PPFRC in steel free pavements at Shaheen Air, Jinnah Airport, Karachi, Pakistan. 119 Figure 6.5 Application of PPFRC in Industrial Flooring of Razi & Sons, Suppliers of Toyota Motors, Port Qasim, Karachi, Pakistan. Figure 6.6 Application of PPFRC in the construction of water reservoir at Diamond Terrace, Gulshan-e-Maymar, Karachi, Pakistan. 120 With Fibre Without Fibre Figure 6.7 Application of PPFRC for blast resistance, Military College of Engineering, Risalpur, Pakistan. Figure 6.8 Applications of PPFRC for Sewage Channel, Khayaban-e-Jami, DHA, Karachi, Pakistan. 121 Depth: 8 to 30 ft KWSB Figure 6.9 Application of PPFRC for Man holes in industrial zone, Landhi, North Karachi, Pakistan. Without Fibre Without Duracrete Fibres WithFibres Duracrete Fibre With Figure 6.10 Application of PPFRC to reduce shrinkage cracking in column footing, Karachi, Pakistan. 122 Abrasion Resistance Without Fibre Duracrete Fibre Without WithFibre Duracrete Fibre With Figure 6.11 Application of PPFRC to reduce abrasion resistance in concrete pavement, Karachi, Pakistan. 123